DISTILLATION/ABSORPTION COLUMN DESIGN

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DISTILLATION/ABSORPTION COLUMN DESIGN1800 or earlierNowChE 4253 - Design I

DISTILLATION/ABSORPTION COLUMN DESIGNDistillationChE 4253 - Design IAbsorption

DISTILLATION/ABSORPTION COLUMN DESIGNPacked TowerChE 4253 - Design ITray tower

DISTILLATION/ABSORPTION COLUMN DESIGNComplex ColumnsChE 4253 - Design I

DISTILLATION/ABSORPTION COLUMN DESIGNComplex ColumnsHeat Integrated Distillation Columns (HIDiC)ChE 4253 - Design I

DISTILLATION/ABSORPTION COLUMN DESIGNComplex ColumnsPetroleum FractionationChE 4253 - Design I

DISTILLATION/ABSORPTION COLUMN DESIGNComplex ColumnsPervaporation distillationChE 4253 - Design I

DISTILLATION/ABSORPTION COLUMN DESIGNComplex ColumnsDouble EffectChE 4253 - Design I

DISTILLATION/ABSORPTION COLUMN DESIGNComplex ColumnsPressure Swing DistillationChE 4253 - Design I

DISTILLATION/ABSORPTION COLUMN DESIGNComplex Columns Multicomponent casesSimple SequencesChE 4253 - Design I

DISTILLATION/ABSORPTION COLUMN DESIGNComplex Columns Multicomponent casesSimple SequencesChE 4253 - Design I

DISTILLATION/ABSORPTION COLUMN DESIGNComplex ColumnsPetlyuk Colums (circa 1960)ChE 4253 - Design IDivided wall column

DISTILLATION/ABSORPTION COLUMN DESIGNComplex Columns Multicomponent casesComplex SequencesChE 4253 - Design I

DISTILLATION/ABSORPTION COLUMN DESIGNAbsorber/stripper typical arrangement.ChE 4253 - Design I

DISTILLATION/ABSORPTION COLUMN DESIGNDistillation ControlChE 4253 - Design I

DISTILLATION/ABSORPTION COLUMN DESIGNBINARY SYSTEMS: Use McCabe ThieleÆ DesignGiven xB and xDÎ calculate RR, #trays, Feed tray, D, BGiven xD and RR (for fixed #trays and feed tray) Æ xB , D, BÆ OperationsGiven 2 operating values (for fixed #trays and feed tray) Æ the rest Æ OperationsChE 4253 - Design I

DISTILLATION/ABSORPTION COLUMN DESIGNMULTICOMPONENT SYSTEMS : Use Computers!!!Degree of Freedom Number of unknowns – Number of equationsOne per each condenser, reboiler or draw. See notes.11S2S22233445S15S166778899T110S410S3T1S32ChE 4253 - Design I1

DISTILLATION/ABSORPTION COLUMN DESIGNMULTICOMPONENT SYSTEMS : Use Pro IICase 2: You know number of trays and feed tray locationYou need to fix variables or add equations. Add Equations (The easiest ), e.g. Reflux ratio and Recovery ratioFix variables, e.g. Compositions, temperatures, flows, etc.ChE 4253 - Design I

DISTILLATION/ABSORPTION COLUMN DESIGNMULTICOMPONENT SYSTEMS :Case 2: You know nothing, not even the number of trays needed.Use Fenske-Underwood Gilliland (see Separation Class Book) to get an idea x 1 xb log d 1 xd xb N log α avgPro II has this shortcut . or if you are too lazy use Pro II as follows1. Do not try blindly specs and number of trays. it won’t work most of the time.2. If you have many components do not include them all at the beginning. start with afew of the most abundant components.3. Put an adiabatic flash first. if the feed is not two phase at the desired pressure,use an isothermal flash. Change the temperature until you get some separation in thedirection you want.S2S1To do this list the components in increasing boiling point and determine keycomponents. Light key goes mostly to the top. Heavy key goes mostly to bottom.F1S3ChE 4253 - Design IContinues in next slide

DISTILLATION/ABSORPTION COLUMN DESIGNMULTICOMPONENT SYSTEMS : Use Pro IICase 2: You know nothing, not even the number of trays needed.Continued 4. Replace the flash by a three plates column, with similar specs as those given by theflash outlet streams. It should not be a big problem to get it.5. Add the components that are missing. Do it slowly, increasing their concentrationuntil you reach the desired values.6. Keep tightening the specs and increasing the number of plates accordingly, so thatyou meet the separation you want.ChE 4253 - Design I

ChE 4253 - Design I MULTICOMPONENT SYSTEMS : Use Pro II Case 2: You know number of trays and feed tray location You need to fix variables or add equations. Add Equations (The easiest ), e.g. Reflux ratio and Recovery ratio Fix variables, e.g. Compositions, temperatures, flows, etc.

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