Appendix VI: Minimum Levels And Test Methods
Appendix VI: Minimum Levels and Test MethodsPARAMETER- CAS No. -M inimum Levels and Test M ethods1, 2, 3GC 4G CM S 5LC 6FAA 7Other1. Total Suspended Solids (TSS)5 mg /lM etho d 16 0.22. Total Residual Chlorine (TRC)20 u g/lM etho d 33 0.53. Total Petroleum Hydrocarbons (TPH)5 mg /lM ethod 16644. Cyan ide (to tal)- 57125 10 u g/lM etho d 33 5.45. Benzene (B)- 71432 0.5 u g/lMethod 6022 ug/lMethod 624Method 8260C 26. Toluene (T)- 108883 0.5 u g/lMethod 8260C 2Method 6022 ug /lMethod 6247. Ethylbenzene (E)- 100414 0.5 u g/lMethod 6022 ug /lMethod 624Method 8260C 28. (m,p,o) Xylenes (X)- 108383;106423; 95476 0.5 u g/lMethod 60210 u g/lMethod 1624Method 8260C 29. Total BTEX0.5 u g/lMethod 6022 ug /lMethod 624Method 8260C 210. Ethylene D ibromide (ED B)(1,2- Dibromoethane) - 106934 1.0 u g/lMethod 6180.01 ug/lMethod 504 .10.1 u g/lMethods 524.2Method 8260C 2Rem ediation General Pe rmit - Ap pend ix VI1
PARAMETER- CAS No. -M inimum L evels and Test M ethods (40 CFR 136)GCG CM SLCFAAOther11. Methyl-tert-Butyl Ether (M tBE)0.5 u g/lMethod 602 85.0 u g/lM etho d 52 4.2Method 8260C 212. tert-Butyl Alcoh ol (TBA )(Tertiary-Butanol) - 75650 0.5 u g/lMethod 602 8100 ug/lM ethod 1666Method 8260C 213. tert-Amyl M ethyl Ether (TA M E)-994058 0.5 u g/lMethod 602 814. Naphthalene- 91203 10 u g/lMethod 610GC/FID2 ug /lMethod 6255.0 u g/lM etho d 52 4.215. Carbon Tetrachloride- 56235 -0.5 u g/lMethod 6012 ug /lMethods 624, 1624Method 8260C 216. 1,4 Dichlorob enzene (p-D CB )- 106467 0.5 u g/lMethods 601, 6022 ug /lMethods 624, 625Method 8260C 217. 1,2 Dichlorob enzene (o-D CB )- 95501 0.5 u g/lMethods 601, 6022 ug /lMethods 624, 625Method 8260C 218. 1,3 Dichlorobenzene (m-DCB) - 541731 0.5 u g/lMethods 601, 6022 ug /lMethods 624, 625Method 8260C 219. 1,1 Dichloroeth ane (DC A) - 7534 3 -0.5 u g/lMethod 6011 ug /lMethod 624Method 8260C 220. 1,2 Dichloroethane (DCA)- 107062 0.5 u g/lMethod 6012 ug /lMethod 624Method 8260C 2Method 8260C 2Rem ediation General Pe rmit - Ap pend ix VI20.2 u g/lMethod 610 HPLCMethod 8270D 3
PARAMETER- CAS No. -M inimum Levels and Test M ethods (40 CFR 136)GCG CM S21. 1,1 Dichloroeth ylene (DC E)- 75354 0.5 u g/lMethod 6012 ug /lMethod 624Method 8260C 222. cis-1,2 Dichloro-ethylene (DCE)-156592 0.5 u g/lMethod 6012 ug /lMethod 624Method 8260C 223. Dichloromethane (M ethylene Ch loride) 75092 0.5 u g/lMethod 6012 ug /lMethod 624Method 8260C 224. Tetrachloro ethylene (PC E)- 127184 0.5 u g/lMethod 6012 ug /lMethod 624Method 8260C 225. 1,1,1 Trichloro-ethan e (TCA )- 71556 0.5 u g/lMethod 6012 ug /lMethod 624Method 8260C 226. 1,1,2 Trichloro-ethan e (TCA )- 79005 0.5 u g/lMethod 6012 ug /lMethod 624Method 8260C 227. Trichloroethy lene (TCE )- 79016 0.5 u g/lMethod 6012 ug /lMethod 624Method 8260C 228. Vinyl Chloride- 75014 0.5 u g/lMethod 6012 ug /lMethod 624Method 8260C 229. Acetone- 67641 1.0 u g/lMethod 524 .250 u g/lMethod 1624Method 8260C 250 u g/lMethod 1624Method 8260C 21 ug /lMethods 625, 1625Method 8260C 2Method 8270D 35 ug /lMethods 625, 1625Method 8270D 330. 1,4 Dioxane-123911 31. T otal Phe nols- 1089521.0 u g/lM ethod 624LCFAAOtherMethod 8260 232. Pentachlorophenol (PCP)- 87865 -1.0 u g/lMethod 604GCF IDRem ediation General Pe rmit - Ap pend ix VI3
M inimum Levels and Test M ethods (40 CFR 136)PARAMETER- CAS No. -GC33. To tal Phth alates(Phthalate esthers)934. Bis (2-Ethylhexyl) Phthalate[Di- (ethylhexyl) Phthalate] - 117817 10 u g/lMethod 606G CM SLCFAAOther10 u g/l*Method 625Method 8270D 35 ug /lMethod 625Method 8270D 3Method 8270D 335. T otal Gro up I P olyn uclea r Arom aticHydrocarbons (PAH)5 ug /lMethod 6250.05 ug/lMethod 610 HPLCMethod 8270D 3b. Benzo(a) Pyrene-50328 10 u g/lMethod 6252 ug /lMethod 610 HPLCMethod 8270D 3c. Benzo(b)Fluoranthene- 205992 10 u g/lMethod 6250.1 u g/lMethod 610 HPLCMethod 8270D 3d. Benzo(k)Fluoranthene- 207089 10 u g/lMethod 6252 ug /lMethod 610 HPLCMethod 8270D 3e. Chrysene- 218019 -10 u g/lMethod 6255 ug /lMethod 610 HPLCMethod 8270D 3f. Dibenzo(a,h)anthracene10 u g/lMethod 6250.1 u g/lMethod 610 HPLCMethod 8270D 3g. Indeno(1,2,3-cd) Pyrene- 193395 10 u g/lMethod 6250.15 ug/lMethod 610Method 8270D 3a. Benzo(a) Anthracene-56553 10 u g/lMethod 610 GCMethod 8270D 336. T otal Gro up II P olyn uclea r Arom aticHydrocarbons (PAH)Minor Modification on Remediation General Permit (RGP):On March 22, 2007, EPA made a minor modification to the RGP to correct the Minimum Level, (ML) for total phthalates (Phthalates and esthers). using Gas Chromatography/Mass Spectrometry(GCMS) from 5ug/l, Method 625 to 10 ug/l, Method 625. This change is just in Row 33 on Page 4 of Appendix VI.Remediation General Permit - Appendix VI4
h. Acenaphthene- 83329 1 ug /lMethod 610GC/FIDi. Acenaphthylene- 208968 PARAMETER- CAS No. -1 ug /lMethod 6250.5 u g/lMethod 610 HPLCMethod 8270D 310 u g/lMethod 6250.2 u g/lMethod 610 HPLCMethod 8270D 3M inimum Levels and Test M ethods (40 CFR 136)GCG CM SLCj. Anthracene- 120127 10 u g/lMethod 6252 ug /lMethod 610 HPLCMethod 8270D 3k. Benzo(ghi) Perylene- 191242 5 ug /lMethod 6250.1 u g/lMethod 610 HPLCMethod 8270D 31 ug /lMethod 6250.5 u g/lMethod 610 HPLCMethod 8270D 310 u g/lMethod 6250.1 u g/lMethod 610 HPLCMethod 8270D 32 ug /lMethod 6255.0 u g/lM etho d 52 4.20.2 u g/lMethod 610 HPLCMethod 8270D 3o. Phenanthrene- 85018 5 ug /lMethod 6250.05 ug/lMethod 610 HPLCMethod 8270D 3p. Pyrene- 129000 10 u g/lMethod 6250.05 ug/lMethod 610 HPLCMethod 8270D 3l. Fluoranthene- 206440 10 u g/lMethod 610GC/FIDm. Fluorene- 86737 n. Naphthalene- 91203 37. To tal Poly chlorina ted B ipheny ls (PCB s) 1010 u g/lMethod 610GC/FIDFAAOther0.00005 ug/lMethod 1668a110.5 u g/lMethod 608Remediation General Permit - Appendix VI5
Inorg anic pa rameters:38. AntimonyM inimum L evels (ug/l) and Te st M ethod sFlame A tomicAbsorptionInductively CoupledPlasmaFurnaceAto micAbsorption200 ug/l50 u g/l5 ug /l5 ug /l2 ug /l5 ug /l0.5 u g/l39. A rsenic40. Cadmium10 u g/lInorg anic pa rameters:41. C hro mium (tota l)M inimum L evels (ug/l) and Te st M ethod sFlame A tomicAbsorptionInductively CoupledPlasmaFurnaceAto micAbsorptionOtherM etho d 21 8.110 u g/lM etho ds 20 0.7 11,200.8, 200.15, 16205 ug /lM etho d 20 0.950 u g/l42. Chro mium (hexava lent)10 u g/lM etho d 21 8.6M ethod 163643. Copper20 u g/l5 ug /l3 ug /l44. Lead100 ug/l40 u g/l3 ug /l45. M ercury46. NickelOther0.2 u g/l30 u g/l47. Selenium10 u g/l5 ug /l50 u g/l5 ug /l2 ug /l48. Silver50 u g/l10 u g/l49. Zinc30 u g/l10 u g/l50. IronM ethods 6010b200 .7 12Remediation General Permit - Appendix VI6
1.Min im um Leve l (M L ) is th e lo we st leve l at w hic h the a na lytic al syste m gives a re cogniz able signa l a nd ac ceptable calibration point for the analyte. The MLrepresents the lowest concentration at which an analyte can be measured with a kno wn leve l of confidence. Th e M L is calculated by multiplying the laboratorydetermined method detection limit by 3.18 (see 40 CFR Part 136, Appendix B). Where a minimum level (ML) is listed but a test method is not specified,permittee may use any of the available methods approved for use under 40 CFR 136, including alternatives approved by this permit, that meets that ML. SeeEP A’s “M ethod s and Guid ance for the A nalysis of W ater” at www.e pa.go v/water/owrccatalog.nsf. Where test method is specified but ML not listed for thatmethod, the lowest ML for listed methods must be used before concentration can be considered as “non-detect.”2.For measuring volatile organic com pou nds, M ethod 826 0C (or the latest version) m ay be used as a substitute for C W A M ethod s 524 .2, 60 2, 62 4, or 1 624 .Method 826 0C must be preceded by Method 503 0 as the prep aration method. H owever, any metho d cha nges m ust be accompa nied b y documented q ualityassurance q uality con trol (Q A/Q C) test re sults to prove that the analytical process can achieve the lower detection limits of M ethod 826 0C.3. For measuring semi-volatile organic compounds, Method 8270D may be used as a substitute for Methods 610, 625, or 1625. Method 8270D must bepreceded by Method 3535 or Method 3520C as the sample preparation method. In either case, the quality control requirements of Method 3500B must be takeninto account. The sample preparation method must be specified with data analysis records. Method 82 70D may be modified to provide lower detection andquantitation limits using Selected Ion Monitoring (SIM). Any method changes must be accompanied by documented quality assurance quality control (QA/QC)test results to prove that the analytical proc ess can achiev e the lower detection limits of M ethod 827 0D .4.GC - gas chromatography5. GCM S - gas chromatography/mass spectrometry6. LC - high pressure liquid chromatography7. Flame Atomic Absorption8. For measuring fuel oxygenates, Method 602 must be modified to include a heated purge.9.The sum of individual phthalate com pound s.10.In the No vember 200 2 W QC , EPA has revised the definition of Total P CB s for aquatic life as “tota l PCBs is the sum of all hom olog ue, all isomer, allcongener, or all Aroclor analyses”.11.Method 1668a (HR GC/HRM S) has been proposed by EPA and is currently being validated. When approval of the method is finalized, it will be approvedfor use with this general permit.12. Methods 6010b and 200.7 for metals may only be used when sample prepared with SW-846 digestion method, Method 3010.Remediation General Permit - Appendix VI7
method, the lowest ML for listed methods must be used before concentration can be considered as “non-detect.” 2.For measuring volatile organic compounds, Method 8260C (or the latest version) may be used as a substitute for CWA Methods 524.2, 602, 624, or 1624. Method 8260C must be preceded by Method 5030 as the preparation method.
Issue of orders 69 : Publication of misleading information 69 : Attending Committees, etc. 69 : Responsibility 69-71 : APPENDICES : Appendix I : 72-74 Appendix II : 75 Appendix III : 76 Appendix IV-A : 77-78 Appendix IV-B : 79 Appendix VI : 79-80 Appendix VII : 80 Appendix VIII-A : 80-81 Appendix VIII-B : 81-82 Appendix IX : 82-83 Appendix X .
Appendix G Children's Response Log 45 Appendix H Teacher's Journal 46 Appendix I Thought Tree 47 Appendix J Venn Diagram 48 Appendix K Mind Map 49. Appendix L WEB. 50. Appendix M Time Line. 51. Appendix N KWL. 52. Appendix 0 Life Cycle. 53. Appendix P Parent Social Studies Survey (Form B) 54
Appendix H Forklift Operator Daily Checklist Appendix I Office Safety Inspection Appendix J Refusal of Workers Compensation Appendix K Warehouse/Yard Inspection Checklist Appendix L Incident Investigation Report Appendix M Incident Investigation Tips Appendix N Employee Disciplinary Warning Notice Appendix O Hazardous Substance List
Appendix 1 - School Food and Beverage Policy 66 Appendix 2 - Trans Fat Standards (O.Reg. 200/08) 83 Appendix 3 - Calculating Trans Fat 84 Appendix 4 - A-Z Food and Beverage List 86 Appendix 5 - Cafeteria Food Service Provider Checklist 92 Appendix 6 - Caterer Checklist 93 Appendix 7 - School Event Menu Ideas 94
Appendix#10 Pre-Job Briefing and Post-Job Review Attendance Form Appendix#11 Safety Task Assignment (STA) Appendix#12 Physiological Monitoring for Heat Stress Appendix#13 Weekly Hour Usage Report Appendix#14 Project - Training Matrix A or B Appendix#15 Excavation Trench Inspection Form Appendix#16 Inbound Equipment Inspection Form
Appendix E: DD Form 577 for Appointing a Certifying Officer 57 Appendix F: Sample GPC Appointment Letters 58 Appendix G: Formal Reporting Requirements 66 Appendix H: Semi-Annual Surveillance Report Template 70 Appendix I: GPC Thresholds 73 Appendix J: Glossary – Sections I and II 75 Chapter 1: The Government Purchase Card Program 1-1. Purpose a.
Port Side. Appendix D . Appendix D . Page D-3. Changed to below 280 PSI and above 350 PSI. Appendix D . Page D-4. Changed to any fuel leak. Appendix E . Appendix E . Page E-3. Line item 10.C, added will not close completely. Appendix E . Page E-4. Line item 12.A, added grade 5 or better mounting . bolts. Appendix E . Page E-4.
The Need for Adult High School Programs 1 G.E.D.: The High School Equivalency Alternative 9 An Emerging Alternative: The Adult High School Ciploma 12 Conclusion 23 Appendix A -- Virginia 25 Appendix B -- North Carolina 35 Appendix C -- Texas 42 Appendix 0 -- Kansas 45 Appendix E -- Wyoming 48 Appendix F -- Idaho 56 Appendix G -- New Hampshire .
