Supplier Quality Requirements For Powder Bed Additive .

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JPL D-101742Initial Release, July 13, 2018Supplier Quality Requirements for Powder Bed Additive ManufacturingJPL D-101742Supplier Quality Requirements for Powder Bed AdditiveManufacturingInitial ReleaseDocument Owner: Sarah ZergaPaper copies of this document may not be current and should not be relied on for official purposes. The current versionis in EPDM: https://epdm.jpl.nasa.gov/awc/ 2018 California Institute of Technology. Government sponsorship acknowledged.July 13, 2018

JPL D-101742Initial Release, July 13, 2018Supplier Quality Requirements for Powder Bed Additive ManufacturingChange LogDateJuly 13, 2018Sections ChangedDescriptionReviewed and approved forunlimited release –CL#18-4827RevisionInitial Release 2018 California Institute of Technology. Government sponsorship acknowledged.

JPL D-101742Initial Release, July 13, 2018Supplier Quality Requirements for Powder Bed Additive ManufacturingTable of ContentsDefinitions . i1.Purpose. 12.Applicability . 13.Applicable Documents . 13.1.ASTM Publications . 13.2.ISO Publications . 23.3.MSFC Standard . 23.4.NFPA Publications. 23.5.SAE Publications . 24.General . 35.Powder . 36.7.8.5.1.General Powder Requirements for Supplier and Powder Manufacturer . 35.2.Powder Manufacturer Requirements . 55.3.Supplier Powder Requirements . 55.4.Reuse . 6Machine Requirements . 76.1.Machine Identification . 76.2.Environmental Parameters . 76.3.Machine Selection . 76.4.Machine Qualification. 76.5.Machine Calibration. 86.6.Machine Maintenance . 86.7.Cleaning . 9Build. 97.1.Support Structure and Part Orientation . 97.2.Build Configuration Management . 97.3.Pre-Build Setup . 97.4.Build Record . 107.5.Process Interruptions . 117.6.Part Handling . 117.7.Part and Witness Coupon Identification . 11Secondary Processing . 118.1.Part Separation . 118.2.Heat Treatment. 12 2018 California Institute of Technology. Government sponsorship acknowledged.

JPL D-101742Initial Release, July 13, 20189.Supplier Quality Requirements for Powder Bed Additive ManufacturingInspection . 129.1.Source Inspection . 129.2.Visual Inspection . 129.3.Dimensional Inspection. 1210.Testing. 1310.1.Mechanical Testing . 1310.2.Chemical Composition . 1310.3.Radiographic Inspection . 1310.4.Density . 1310.5.Surface Finish . 1311.Packaging, Handling, and Shipping . 1412.Traceability . 1413.Deliverable Matrix . 14 2018 California Institute of Technology. Government sponsorship acknowledged.

JPL D-101742Initial Release, July 13, 2018Supplier Quality Requirements for Powder Bed Additive ManufacturingDefinitionsAdditive Manufacturing (AM) – Process of joining materials to make objects from 3D modeldata, usually layer upon layer, as opposed to subtractive manufacturing methods.As-built – The part’s form after it has been built but before secondary processingBuild Strategy – The AM machine’s strategy for building the partCondensate – Vaporized material, created while the laser is firing, that condenses intonanometer-sized particlesFirst Article Inspection (FAI) – Qualification report of the first part produced that ensures thespecifications are metITAR – International Traffic in Arms Regulations. Regulation of the export and import ofdefense related partsPowder Lot – Powder produced by a certified supplier in one production run, using the sameprocess, equipment, and one type of powderManufacturing Plan – The supplier’s plan to manufacturer a JPL part, including all stepsperformed to the part from start to finishMelting Device – The device used to fuse the powder together to form layers, often an electronbeam or a laserPart Cake – The combination of sintered powder and part on the build plate after the part hasfinished buildingPowder Bed – The build area in an additive manufacturing process in which the powder isdeposited and selectively melted with a heat source to build up componentsPowder Manufacturer – The organization that produces the powderRecoater Blade – The part of the powder distribution system that spreads a thin, level layer ofpowder across the build platformSupplier – Additive manufacturing vendor producing parts or providing post-processing for JPLSupport Structure – Supplementary, sacrificial material built along with a part to providethermal management within the powder bed, dimensional stability, and overhanginggeometry supportUsed Powder – Powder that has been processed in at least one previous build cycleVirgin Powder – Unused powder from a single powder lot 2018 California Institute of Technology. Government sponsorship acknowledged.i

JPL D-101742Initial Release, July 13, 2018Supplier Quality Requirements for Powder Bed Additive Manufacturing1. PurposeThe purpose of this document is to provide the supplier quality requirements for additivemanufacturing space-flight parts using powder bed fusion technologies. This document doesnot apply to any other additive manufacturing methods.2. ApplicabilityThis document applies to any suppliers who conduct activities involving additivelymanufacturing JPL flight parts using powder bed fusion technologies. A separate documentwill exist for internal production parts. For the purpose of this document, “supplier” refers tothe subcontracted organization delivering additively manufactured parts to JPL. In thisdocument, “contract” refers to the contract between JPL and the supplier, not the contractbetween NASA and JPL. JPL approved suppliers are responsible for flowing downrequirements as stated in this document to the powder manufacturer, mill, and postprocessing facilities.3. Applicable DocumentsThe following documents, of the issue specified in the contractual instrument, or as specifiedfor use within JPL, form a part of this specification to the extent specified herein.3.1. ASTM PublicationsASTM B213 – Standard Test Methods for Flow Rate of Metal Powders Using the HallFlowmeter FunnelASTM B214 – Standard Test Method for Sieve Analysis of Metal PowdersASTM B215 – Standard Practices for Sampling Metal PowdersASTM B243 – Standard Terminology of Powder MetallurgyASTM B311 – Standard Test Method for Density of Powder Metallurgy (PM) MaterialsContaining Less Than Two Percent PorosityASTM B946 – Standard Test Method for Surface Finish of Powder Metallurgy ProductsASTM E8 – Standard Test Methods for Tension Testing of Metallic MaterialsASTM E9 – Standard Test Methods of Compression Testing of Metallic Materials atRoom TemperatureASTM E539 – Standard Test Method for Analysis of Titanium Alloys by X-RayFluorescence SpectrometryASTM E1409 – Standard Test Method for Determination of Oxygen and Nitrogen inTitanium and Titanium Alloys by Inert Gas Fusion1 2018 California Institute of Technology. Government sponsorship acknowledged.

JPL D-101742Initial Release, July 13, 2018Supplier Quality Requirements for Powder Bed Additive ManufacturingASTM E1447 – Standard Test Method for Determination of Hydrogen in Titanium andTitanium Alloys by Inert Gas Fusion Thermal Conductivity/Infrared DetectionMethodASTM E1742 – Standard Practice for Radiographic ExaminationASTM E2371 – Standard Test Method for Analysis of Titanium and Titanium Alloys byDirect Current Plasma and Inductively Coupled Plasma Atomic EmissionSpectrometryASTM E2465 – Standard Test Method for Analysis of Ni-Base Alloys by WavelengthDispersive X-Ray Fluorescence SpectrometryASTM E2594 – Standard Test Method for Analysis of Nickel Alloys by InductivelyCoupled Plasma Atomic Emission Spectrometry (Performance-Based Method)ASTM E3061 – Standard Test Method for Analysis of Aluminum and Aluminum Alloysby Inductively Coupled Plasma Atomic Emission SpectrometryASTM E606 – Standard Test Method for Strain-Controlled Fatigue TestingASTM F2924 – Standard Specification for Additive Manufacturing Titanium-6Aluminum-4 Vanadium with Powder Bed FusionASTM F3056 – Standard Specification for Additive Manufacturing Nickel Alloy withPowder Bed FusionASTM F3122 – Standard Guide for Evaluating Mechanical properties of Metal MaterialsMade via Additive Manufacturing Processes3.2. ISO PublicationsISO 52900 – Standard Terminology for Additive Manufacturing3.3. MSFC StandardMSFC-STD-3716 – Standard for Additively Manufactured Spaceflight Hardware byLaser Powder Bed Fusion in Metals3.4. NFPA PublicationsNFPA 484 – Standard for Combustible Metals3.5. SAE PublicationsAMS 2750 – Pyrometry2 2018 California Institute of Technology. Government sponsorship acknowledged.

JPL D-101742Initial Release, July 13, 2018Supplier Quality Requirements for Powder Bed Additive Manufacturing4. GeneralAll JPL requirements and specifications shall take precedence over manufacturerrecommendations and supplier processes. Supplier processes should be in accordance withthe machine manufacturer’s machine recommendations. The supplier will maintaindocumented information of the machine manufacturer’s recommendations. The supplier mayestablish their own processes that differ from manufacturer’s recommendations, butjustification and rationale may be required. If manufacturer’s recommendations areunavailable, the supplier will be responsible for establishing processes to meet requirements.In regards to requirements listed in the contract, the drawing, and the Statement of Work(SOW), the contract will always supersede the drawing and the drawing will supersede theSOW. Supplementary specifications or standards that are required in addition to this standardwill be referenced in the drawing, contract, or SOW.5. Powder5.1. General Powder Requirements for Supplier and Powder Manufacturer5.1.1. Powder QualityThe powder shall be uniform in color and quality, dry, and free from agglomeratedmasses, foreign materials, and imperfections detrimental to its performance.5.1.2. Powder SamplingUnless otherwise stated by JPL, all powder sample collecting shall be inaccordance with ASTM B215.5.1.2.1.Particle Size DistributionIf required on the contract, particle size distribution testing shall beperformed in accordance with ASTM B214.5.1.2.2.Powder CompositionPowder chemical composition results shall conform to the materialspecification that is listed in the contract or drawing, see Section 5.2.1 and10.2. In the case where the compositional requirements differ between thedrawing and the contract, the contract shall supersede the drawing3 2018 California Institute of Technology. Government sponsorship acknowledged.

JPL D-101742Initial Release, July 13, 20185.1.2.3.Supplier Quality Requirements for Powder Bed Additive ManufacturingRheologyIf required by contract, the rheology measurement shall be delivered withthe shipment. Rheology measurement methods include hall flowmeters,used in accordance with ASTM B213, and Revolution Powder Analyzers.Additional methods may also be used if approved on the contract.5.1.3. Powder IdentificationAll material used for production, including raw material and powder, should haveidentification that includes, at a minimum:-Manufacturer identificationPurchase order numberProduction methodMaterial type and gradeLot number5.1.4. StorageSupplier shall have a process that ensures the powder is stored in a sealed moistureresistant container that permits long term storage without affecting itscharacteristics or properties. Supplier will use methods of reducing moisture insidethe containers e.g. desiccant packs or inert gas.The powder should be stored in a cool, dry area. The supplier and powdermanufacturer should have documented processes in place to address possiblemoisture contamination and prevention of electro static discharge (ESD) duringstorage and handling. Any powder found in damaged packages or that has been wetshall be segregated and properly disposed of. See 6.2 for additional information onEnvironmental Parameters.Documentation of the safe processing and storage of reactive materials, such astitanium or aluminum, shall be maintained to prevent accidental ignition and theproper PPE should be used for handling the reactive materials. See NFPA 484 forfurther reactive material handling information.4 2018 California Institute of Technology. Government sponsorship acknowledged.

JPL D-101742Initial Release, July 13, 2018Supplier Quality Requirements for Powder Bed Additive ManufacturingIdentification and traceability of the powder should be maintained throughout thetransferring of packages. The supplier should have a documented process tominimize the time that unused powder is exposed to open air in order to reducepossible contamination of the stored powders.5.2. Powder Manufacturer RequirementsSuppliers shall have a process to determine a powder manufacturer’s ability to providepowder that meets all requirements of this standard and any other required by thesupplier. As part of that process, the supplier should ensure that the powdermanufacturer maintains a documented process for:-Procurement of raw material for powderSampling and testingIdentificationStorage5.2.1. Procurement of Raw Material for PowderProcured raw material used to produce powder shall meet the compositionalrequirements specified in the contract or the engineering drawing. In the casewhere the compositional requirements differ between the drawing and the contract,the contract requirements shall supersede the drawing. A powder lot shall bedesignated as powder produced by a certified supplier in one production run, usingthe same process, equipment, and one type of powder. In addition, all procurementsshall comply with the most current JPL Designated Countries List.5.3. Supplier Powder Requirements5.3.1. Documentation VerificationBefore releasing the powder for production, the supplier should verify that thepowder is in accordance with the data provided in the CoC from the powdermanufacturer. All powder verification should be retained as documentedinformation.5 2018 California Institute of Technology. Government sponsorship acknowledged.

JPL D-101742Initial Release, July 13, 2018Supplier Quality Requirements for Powder Bed Additive Manufacturing5.3.2. Virgin PowderAll virgin powder should be conditioned by the supplier such that it is suitable foruse in their manufacturing process, including but not limited to: sieving, filtering,mixing, and powder recovery, etc. If the conditioning procedure changes, the JPLpurchaser must be notified.5.4. Reuse5.4.1. Powder RecoveryPowder shall not be reused, unless approved on the contract. Applicable methodsof powder removal include, but are not limited to:- Dry

ASTM B243 – Standard Terminology of Powder Metallurgy ASTM B311 – Standard Test Method for Density of Powder Metallurgy (PM) Materials Containing Less Than Two Percent Porosity . JPL D-101742 Supplier Quality Requirements for Powder Bed Additive Manufacturing Initial Release, July 13, 2018 .

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