Appendix 1 List Of BSI And ISO Standards Relating To .
Appendix 1 List of BSI and ISO Standards relatingto surfactant analysisBritish Standards BS 3762 and 6829 deal respectively with the analysis offormulated detergent products and raw materials. Some parts areidentical with ISO Standards. Conversely some of the ISO Standardsrelating to surfactant analysis correspond with parts of these BritishStandards. The following list shows which Standards from either organisation correspond with those of the other. The words given here describethe subject matter but are only occasionally the official title of eitherStandard.BS 3762: Analysis of formulated productsPart 1Methods of sample divisionPart 2, Tests Qualitative tests for type of surface active matter3.2 and 3.3Part 2, TestQualitative test for nonionic surfactants3.4cobaltothiocyanatePart 3.1Anionic-active matter by two-phase titrationAlkali-hydrolysable and non-hydrolysable activePart 3.2matterAcid-hydrolysable and non-hydrolysable activePart 3.3matterCationic-active matter by two-phase titrationPart 3.4Total organic matter by ethanol extractionPart 3.5Non-detergent organic matter (neutral oil,Part 3.6petroleum ether solubles)Total nonionic matter by ion exchangePart 3.7Part 3.8Alkanolamides-Kjeldahl nitrogenPart 3.9Soap contentShort-chain alkylbenzene sulphonatesPart 3.10BS 6829: Analysis of raw materialsPart 1.1Inorganic sulphate-volumetricPart 2.1Total alkane sulphonatesPart 2.2Mean molecular weight and alkanemonosulphonate content by extractionPart 2.3Alkane monosulphonate content by 12268456121
APPENDIX 1Part 3.1Part 4.1Part 4.2Part 4.3Part 4.4Part 4.6Part 5.1Part 5.2Part 5.3Mean molecular weight of alkylbenzenesulphonates by gas chromatographyCloud point of nonionicsTotal nonionic active and polyethylene glycolsWeibull methodTotal ethylene oxide groups-iodometric methodCloud point-volumetric methodHydroxyl value-acetic anhydrideAlkylether and alkylphenylether sulphates-totalactive matterAlkylether and alkylphenylether sulphatesmean molecular weightAlkylether and alkylphenylether sulphatesunsulphated matterOther ISO Standards relating to surfactant analysishaving no corresponding British StandardTechnical alkane sulphonates-Methods ofanalysisTechnical primary alkyl sulphates-analysisTechnical secondary alkyl sulphates-analysisTechnical alkylarylsulphonates excludingbenzene derivatives-analysisAnion-active stable to acid hydrolysis-traceamountsHydroxyl value-phthalic anhydrideTechnical ethoxylated fatty amines-methods SO8938948951104286843276384Other Standards dealing with the analysis of soaps and soap products andthe determination of non-surfactant components of detergent productsare omitted.
Appendix 2List of relevant ASTM MethodsAll ASTM Methods have titles of the form 'Standard Test Method(s) for. '. These words are omitted in the following list, which includes allmethods for the analysis of surfactants, excluding soaps and soapproducts and the determination of non-surfactant constituents. All theseMethods are in the Annual Book of ASTM Methods, Section 15, Volume15.04, apart from Methods D 2071 to D 2080 inclusive, which are in thesame Book, Section 6, Volume 6.03.Method No.D 500-89D 1568-63D 1570-89D 1681-83D 1768-89DDDD2023-892024-652071-872073-66D 2074-66D 2075-89D 2076-64D 2078-86D 2080-64D 2357-74D 2358-89TitleChemical Analysis of Sulfonated and Sulfated oilsSampling and Analysis of Alkylbenzene SulfonatesSampling and Chemical Analysis of Fatty AlcoholSulfatesSynthetic Anionic Active Ingredient in Detergents byCationic Titration ProcedureSodium Alkylbenzene Sulfonates in Synthetic Detergentsby Ultraviolet AbsorptionAnalysis for Sodium Toluene Sulfonate in DetergentsCloud Point of Nonionic SurfactantsFatty Nitrogen Products(Reapproved 1987) Total, Primary, Secondary andTertiary Amine Values of Fatty Amines, Amidoaminesand Diamines by Referee Potentiometric Method(Reapproved 1987) Total, Primary, Secondary andTertiary Amines by Alternative Indicator MethodIodine Value of Fatty Amines, Amidoamines andDiamines(Reapproved 1987) Acid Value and Amine Value ofFatty Quaternary Ammonium ChloridesIodine Value of Fatty Quaternary Ammonium ChloridesAverage Molecular Weight of Fatty QuaternaryAmmonium ChloridesQualitative Classification of Surfactants by Infra-redSpectroscopySeparation of Active Ingredient from Surfactants andSyndet Compositions
APPENDIX 2D 2959-89DDDD3049-893673-894224-894251-89D 4252-89D 4337-89D 5070-90345Ethylene Oxide Content of Polyethoxylated NonionicSurfactantsSynthetic Anionic Ingredient by Cationic TitrationChemical Analysis of Alpha Olefin SulfonatesAnionic Detergent by p-Toluidine HydrochlorideActive Matter in Anionic Surfactants by PotentiometricTitrationChemical Analysis of Alcohol Ethoxylates andAlkylphenol EthoxylatesAnalysis of Linear Detergent AlkylatesSynthetic Quaternary Ammonium Salt in FabricSofteners by Potentiometric TitrationASTM publications may be obtained from: American Society for Testingand Materials, 1916 Race Street, Philadelphia, PA 19103, USA.
Indexaccuracy 12acid-base titration 48Acid Blue 1 59, 60acid hydrolysis 113amides 113amidopropylbetaines 179determination of fattyacid 140determination of fattyamine 140determination ofmethyltaurine 140determination ofsulphosuccinic acid 140determination oftaurine 140glyceride see acidhydrolysissulphates see alkylsulphates; alkylethersulphates; alkylphenylethersulphatesacid mixed indicator 61, 106,172acid value 53, 54acyl isethionates 19, 129, 1%determination of activecontent 129determination of sodiumisethionate 130acyl methyltaurates 20, 194,196determination of fattyacids 140determination ofmethyltaurine 140determination of soap 141determination oftaurine 140methyltaurates 139acyl sarcosinates 20acyl taurates 139, 194determination of fattyacid 140determination ofmethyltaurine 140determination of soap 141determination oftaurine 140alcohol ethoxylates 216, 224,322,324alcohol sulphates 216alcohols 269alkali value 55alkaline mixed indicator 61alkane monosulphonates224alkane sulphonates 19, 109,119,229determination of alkanemono- anddisulphonates 121determination of meanmolecular weight 120determination of totalalkane sulphonate 119alkanolamides 21, 29, 164,275,340amide diester 165amide ester 165, 168amide monoester 165composition 164di(N-hydroxyethyl)piperazine 165diester amine 165ester amine 165, 167ethanolamide 168ethoxylated 164, 198free ethanolamine 167free fatty acid 167glycerides 168glycerol 167methyl ester 168monoester amine 165total amide 166total ethanolamide 165total fatty acid 165alkene monosulphonates seealpha-olefin sulphonatesalkoxylates 269alkylamidobetaines 23alkyl amidopropyl betaine,infrared spectrum mmonium chloride 226alkylamines 22alkylaminodipropionates 23alkylaminopropionates 23alkylbenzene sulphates 109alkylbenzene sulphonates 19,116, 231' 275desulphonation 116infrared spectrum 279in sewage effluents 331short -chaindetermination 118alkylbenzene sulphuric acidsdetermination of sulphuricacids 117alkyl betaines 280alkyl diethanolamide, infraredspectrum 278alkyldiglycinates 23alkyldimethyl betaines 23alkylether phosphates 20, 29,143see also phosphate estersalkylether sulphates 19, 27,110,193,196,217,223,226,229,280,331acid hydrolysis 110determination of sulphateion 112extraction of activematter 113extraction of alcoholethoxylates 111infrared spectrum 283alkyl ethoxy carboxylates20alkylethoxylatedsulphates 216alkylglycinates 23alkyl group, identified by massspectrometry 322alkyl monoethanolamide,infrared spectrum 277alkylnaphthalenesulphonates 19, 129alkyl phenols 269alkyl phenol ethoxylates 20,216,225,229,269,324infrared spectrum 274in drinking water 330alkylphenylethersulphates 110, 193acid hydrolysis 110determination of sulphateion 112extraction of activematter 113extraction of alkylphenolethoxylates 111alkyl phosphate mixtures by31 P-NMR 314alkyl phosphates 20, 29, 143see also phosphate estersalkyl polyglycosides 21, 164,198alkylpyridinium salts 22, 198alkyl sulphates 19, 27, 110,193,224,229,230,280,325,331acid hydrolysis 110determination of sulphateion 112extraction of fattyalcohol 111alkyl sulphonates 231, 275,331infrared spectrum 281 , 282alkyl sulphosuccinamates 20determination of fattyamine 140determination ofsulphosuccinic acid 140alkylsulphosuccinatesdetermination of free fattyamine 141determination of soap 141alkyl (C 10-C 14)sulphosuccinates 224alkyltrimethylammoniumcationics 216alpha-olefin sulphonates19,24,109,218,224,331alpha-olefin sulphonic acids325composition 124determination ofdisulphonate 128determination ofsultones 128
347INDEXdetermination of totalsulphonate 125disulphonate(sulphatosulphonate) 124alpha-sulphonated fattyester 194, 195, 1%Amberlite XAD-2 121amidopropyl betaines 179,280amine oxides 22, 182, 189,280,335free tertiary amine 189infrared spectrum 285titration with sodiumdodecyl sulphate 189titration with sodiumtetraphenylborate 189amines 183, 335apparent molecular(equivalent) weight 184ethoxylated amines 22molecular weight 183primary amine 183, 184secondary amine 183, 184tertiary amine 183, 184total amine 183, 184amines, ethoxylateddetermination of primaryplus secondary amine 187determination of equivalentweight 187determination of ethyleneoxide chain length 188determination ofpolyethylene glycol 188determination of totalamine 187see also diamines,ethoxylatedammonium salts ofanionics 324amphopropyl sulphonates 23amphoteric surfactant seesurfactant, definitionamphoteric surfactantscommon types 22FAB/LSIMS 337amphoterics 30, 180, 324acid-base titration 180titration with benzethoniumchloride 180titration with NaTPB 180titration with sodiumdodecyl sulphate 180analysis of mixtures 325anion-exchange resins 78anionic surfactant seesurfactant, definitionanionic surfactants 275common types 18mass spectrometry 323anionics 325analysis by GC 214analysis by HPLC 222analysis by HPTLC 229analysis of mixtures 193para-toluidine method 107potentiometrictitration 106two-phase titration 106anionics and cationics, analysisof mixtures 202Antarox C0-430 153apodisation 243array detector 328ASTM methods, list 344attenuated totalreflectance 251A TR crystals 252A TR effect 252A TR spectrum 252autotitrator 69average alkyl chain length by1 H-NMR310in environmentalbase value 55beam splitter, infrared 239,245benzalkonium salts 22, 198benzethonium chloride 59,60,61benzylic cleavage 334, 340betaines 226determination of freeamine 179potentiometric acid-basetitration 178titration with sodiumdodecyl sulphate 178titration with sodiumtetraphenylborate 178two-dimensional (2D)NMR 304biguanidinium 173block copolymers 21, 161Boltzmann energy levels 299branched-chain alkylbenzenesulphonate 331bromocresol green 63, 161bromophenol blue 64, 106BSI and ISO standards,list 342samples 330mass spectrometry 323quantitation 335cationics 229, 324analysis by GC 216analysis by HPLC 225cationics and amphoterics,analysis of mixtures 198chain length distribution 334determination by massspectrometry 319chemical noise in massspectrometry 323chromatography 38gas liquidchromatography 38high-performance liquidchromatography 38ion chromatography 38open-columnchromatography 40, 73thin-layerchromatography 38CID 331cocoamidopropylbetaine 178, 337mass spectrum 339cocodimethylbetaine 178collisionally induceddecomposition 328competitors' products 13date codes 14samples 15Coones advantage 243contaminantsdetermination by GC 217determination byHPLC 226continuous flow FAB 331in LC-MS 323COSY spectrum 305, 306cross-peaks 307calcium palmitate 266calculations 9molecular weight 10, 11volumetric 9see also directpotentiometrycalibration curves 70capillary zoneelectrophoresis 231carboxybetaines 177, 182see also betainescarboxylates 20, 29, 142acid-base titration 142solvent extraction 142titration with benzethoniumchloride 142carboxylic acid/ester mixtureby 13 C-NMR 314cation attachment 323cation-exchange resins 78cationic surfactant seesurfactant, definitioncationic surfactants 325common types 21FAB/LSIMS 325data-reduction techniquesfactor loadings 290in infraredspectroscopy 290scores matrix 290deconvolution of infraredspectra 262degree of ethoxylation 334determined by massspectrometry 322del(ree of polymerisation by13C-NMR 312deionisation 96derivatisation 222detectors, infrareddeuterated triglycinesulphate 245mercury cadmiumtelluride 245determination of equivalentweight 187determination of homologuedistribution 330determination of totalamine 187
348deuterated NMR solvents,costs 302dialkanolamides 21dialkylammonium salts 198dialkyl aspartate 136isolation anddetermination 138dialkyl dimethyl ammoniumchloride, infraredspectrum 284dialkyldimethylammoniumcationics 216dialkyldimethylammoniumsalts 22dialkylmethylammoniumquaternaries 225, 226dialkylmethylamines 22dialkylsulphonates 109dialkylsulphosuccinates 20,136alkaline hydrolysis 137anion-active matter andaspartate 136composition 136extraction of fattyalcohols 137dialkyltetralinsulphonates 215, 338dialkyltetralins 226, 227diamines, ethoxylatedsee also amines,ethoxylateddetermination of equivalentweight 187determination of totalamine 187diethanolamides 165, 275see also alkanolamidesdiffuse reflectance,infrared 253digitisation 243diglycerides 275dimethyl yellow 64dimidium blue 61dimidium bromide 24, 59,601, 4-dioxane 217,226direct potentiometry 70see also calibration curves,standard additionsdiscrimination 323, 325, 329,335disulphine blue 61disulphine blue V 24disulphine blue VN 59, 60ElMS of anionicsurfactants 338EI spectra 329electron impact ionisation(EI) 321electrospray 323, 329electrospray MSlimit of detection 325sensitivityelution 80, 94empirical formulae by massspectrometry 319environmental samples 334ester value 53, 54INDEXesters 21, 275nonionic esters 29ethanolamides 21, 164ethoxylate numberdetermination by1H-NMR310ethoxylate-propoxylatecopolymer, infraredspectrum 273ethoxylate/propoxylate ratio by1H-NMR311ethoxylated alcohols 149,197,231, 340ethoxylated alkylamines 340ethoxylated alkylphenols 149,197,340ethoxylateddialkanolamides 21ethoxylated fatty acids 20,149,225,341free fatty acid 160mono- and diester 160polyethylene glycols 160ethoxylated fatty alcohols 338ethoxylated fatty amines 340ethoxylatedmonoalkanolamidesulphate 194ethoxylatedmonoalkanolamides 21ethoxylated quaternaryamines 335"thoxylatessee also ethoxylatedalcohols, ethoxylatedalkylphenols, ethoxylatedfatty acidscobaltothiocyanatemethod 154composition 149determination ofoxyethylene groups 157direct potentiometry 153polyethylene glycols,volumetric determinationof 157pseudocationiccomplexes 150, 151spot test 156total nonionics andpolyethylene glycols 156two-phase titration 150Weibull method 156ethylene oxide 217in alcohol ethoxylates 217evaporative light scatteringdetector 222extraction 37liquid-liquid extraction 38,45,47liquid-solid extraction 37,42extraction columns 47FAB 329,330FAB/LSIMS of anionicsurfactants 330fatty acids 226, 324, 325, 331,337infrared spectroscopy 266fatty alcohol ethoxylates 20infrared spectrum 272fatty alcohols 20, 324fatty diaminesdetermination 186equivalent weight 187fatty ester a-sulphonates 19,130composition 130determination of asulphonated ester 133determination of lowmolecular-weight alkylsulphate 134determination of soap 131determination ofsulphonated surfactantspecies 132determination of totalunesterifiedcarboxylate 134determination ofunsulphonated ester 131saponification 133Fellgett advantage 240fingerprinting see infraredspectra, fingerprint regionflowFAB 334Fourier transformation 238free induction decay 300FT process 299gas cells, infrared 255gas chromatography 207, 209column temperature 212columns 210detectors 212injection 211resolution 209solid supports 210stationary phase 211gas chromatography detectorsFT infrared 213mass spectrometer 213gas chromatography-massspectrometry (GC-MS) 320,327, 329quantitation 330gel permeationchromatography 207, 231glyceride sulphate 115, 194,196acid hydrolysis 115determination ofglycerol 115determination ofsulphate 115extraction of fatty acid 115glycerides 324glycerol 269infrared spectrum 271glycerol trioleate, infraredspectrum 276glycolic acid, inamphoterics 179, 180heavy atom effect 236HECfOR spectrum 306,307
349INDEXhigh performance liquidchromatography (HPLC)207,218column packings 219columns 219detectors 221diode array detector 221electrochemicaldetectors 222fluorescence detectors 222injection 221mass spectrometricdetection 225mass spectrometry 222, 226mobile phase 220pumps 220refractive index 221UV photometric 221HPTLC 227developing solvents 228quantitation 228visualisation 228Hyamine 1622 60hydrobe distribution ofLAS 223hydroxyalkanesulphonates 109, 124hydroxyl value 55phthalic anhydridemethod 57hydroxypropylsulphonates 23hydroxysultaines 23imidazoline 24imidazoline derivatives 23imidazoline-typecationics 226imidazolinium 24, 280imidazolinium quats 198imidazolinium salts 22,30,229,324infrared spectrum 288infrared absorptions,origin 235infrared spectracurve-fitting 260differentiation 260fingerprint region 264infrared spectroscopybaseline corrections 256buying a spectrometer 293instrumentation 239liquids 249mulls 249pressed halide discmethod 248source 244iodine value 57ion chromatography 78,207,229ion exchange 39, 122amphoterics: loss ofliberated ions 103analysis of columneffluents 101definition 77elution 88multicolumn systems 92preparation of column 90solvent composition 90ion-exchange membrane 78,79ion-exchange resins 78anion exchange resins,strongly basic 82apparatus 85conversion to another ionicform 91cross-linking 80exchange capacity 79mixed-bed resins 84, 87particle size 80selectivity 83selectivity coefficient 83strongly acidic 81strongly acidic cationexchanger 82, 87, 88strongly basic 81strongly basic anionexchanger 87, 88weakly acidic 81weakly acidic cationexchanger 82, 87, 88weakly basic 81weakly basic anionexchanger 82, 87, 88ion-exchange silicas 79ionic surfactants, massspectrometry 325ionisation techniques in massspectrometry 320chemical ionisation(CI) 321collisionally induceddecomposition (CID) 322electron impact (EI) 320electrospray (ES) 321fast atom bombardment(FAB) 321, 322gas chromatography(GC) 322hard ionisation 320liquid chromatography(LC) 322liquid secondary ionisationMS (LSIMS) 321,322particle beam (PB) 322soft ionisation 320, 321supercritical fluidchromatography(SFC) 322thermospray (TS) 321ISO standard see BSI andISO standards, listisolation of amphoterics 98isolation of anionics 96isolation of cationics 97isolation of nonionics 95isopropanol, infraredspectrum 270isopropanolamides 21, 164isoquinolinium 173Jacquinot advantage240k matrix method 289Kubelka--Munck function254lauryliminopropionic acid 182LC-MS 329quantitation 330LC-MS interfaceselectrospray 329particle beam interface 338plasma discharge 324, 329thermospray 329limitation of NMR 297linear alkylbenzenesulphonates 214,222,229,325,330,338liquid chromatography-massspectrometry (LC-MS) 320,323interfaces 323soft ionisation 323lock solvents 303low-resolution massspectrum 319LSIMS 330spectrum 331magnetic dipole 298magnetic field scanning 326magnetic flux 300mass analyser, magneticsector 326mass chomatograms 334mass measurement by massspectrometry 326mass spectra, libraries 321,329mass spectrometer, typesion trap mass analyser 327magnetic sector massanalyser 326quadrupole massanalyser 327sector massspectrometer 318triple quadrupoleinstruments 318mass spectrometry 215, 318quantitation 331sensitivity 319matrix effects 71, 72metastable ions 328method of standardadditions 153methylene blue 64Michelson interferometer 239microscope, infrared 255mixed anhydride reagent 145,159mixed-bed resins 87, 88mixed surfactants, two quatstogether 198amphoterics 200anionics withamphoterics 204anionics with quats 202anionics with weakbases 204any three speciestogether 196carboxylates withamphoterics 205
350mixed surfactants,two quats----contd.carboxylates withcationics 205carboxylates with quats 205carboxylates with weakbases 205co
Appendix 1 List of BSI and ISO Standards relating to surfactant analysis British Standards BS 3762 and 6829 deal respectively with the analysis of formulated detergent products and raw materials. Some parts are identical with ISO Standards. Conversely some of the ISO Standards
Modell 2004 Eeprom Alfa Romeo 145 Alt Prozessor Neu Prozessor www.obd2be.com . Citroen Xsara Eeprom Xsara Ab 2000 NEC-Hardware . Eeprom C2 Ab 2004 Tacho BSI Eeprom C3 Eeprom C4 Eeprom C5 Modell 2001 BSI Lötpunkte C5 Modell 2002 Tacho BSI Lötpunkte C5 BSI Valeo Eeprom C5 BSI Valeo V2 BSI neu Eeprom
BSI Standards Book Catalogue 2013. BSI’s essential guide to books, CD-ROMs and online products. BSI Brand styleguide. Guidelines Version 2.0 October 2012. Version 2.0 October 2012. BSI Brand styleguide. Guidelines Version 2.0 October 2012. Version 2.0 October 2012. To order please call BSI Customer Services on 44 (0)20 8996 9001. P&P 5.95 (inclusive of VAT); 9.95 Rest of the .
Audi Diagnostic VW AUDI OBD II Cluster Audi Diagnostic VW AUDI OBD II Cluster Audi Diagnostic VW AUDI OBD II Cluster . Triumph-BSI 95128 V2 C66 95040 407-BSI 607-BSI Triumph-BSI 95128 V1 95160 V1 95160 V2 MCU 95128 95160 C5-BSI Shenlong fukang 95040 V1 95040 V2 95160 New Passat Elysee BERLINGO-BSI 95128
Security (BSI) was established by the German Parliament in 1991. § 3 of the Act on the Establishment of the BSI, dated 17.12.1990 (Federal Law Bulletin I p. 2834) defines the tasks of BSI. The Federal Office for Information Security (BSI) was established by the German Parliament in 1991. 3 of the Act on the Establishment
Issue of orders 69 : Publication of misleading information 69 : Attending Committees, etc. 69 : Responsibility 69-71 : APPENDICES : Appendix I : 72-74 Appendix II : 75 Appendix III : 76 Appendix IV-A : 77-78 Appendix IV-B : 79 Appendix VI : 79-80 Appendix VII : 80 Appendix VIII-A : 80-81 Appendix VIII-B : 81-82 Appendix IX : 82-83 Appendix X .
(see Table 1. and Table 2): Secondary BSI: A BSI that is thought to be seeded from a site-specific infection at another body site (see Appendix B. Secondary BSI Guide and CDC/NHSN Surveillance Definitions for Specific Types of Infection [Ch-17], UTI [Ch-7], Pneumonia (Ch-6), and SSI (Ch-9) Secondary BSI Attribution Period (SBAP):
'ISO 9001 certified by BSI under certificate number FM123456' 'ISO 9001 Quality Management certified by BSI under certificate number FM123456' If you have multiple schemes, list these one after each other: 'ISO 9001 and ISO 14001 certified by BSI under certificate numbers FM123456, FM 987654' 'ISO 9001 Quality Management and ISO
Appendix G Children's Response Log 45 Appendix H Teacher's Journal 46 Appendix I Thought Tree 47 Appendix J Venn Diagram 48 Appendix K Mind Map 49. Appendix L WEB. 50. Appendix M Time Line. 51. Appendix N KWL. 52. Appendix 0 Life Cycle. 53. Appendix P Parent Social Studies Survey (Form B) 54
