Appendix I - Trs Compound Testing Quality Assurance/Quality Control

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APPENDIX I – TRS COMPOUND TESTING QUALITYASSURANCE/QUALITY CONTROL

Table I-1Comparison of Original and Duplicate Data - Total Reduced Sulfur - Method RSK-175(a)New-Indy Catawba - Catawba, SCSample LocationOriginalResult(ppb)Hydrogen yl rence(ppb)(ppb)OriginalResult(ppb)Dimethyl SulfideDuplicatePercentResultDifference(ppb)Methyl MercaptanDateTime7/9/20218:45 10/20219:39 7/9/20219:25 0218:31 0219:53 inalDuplicateResult (ppb) Result (ppb)PercentDifference5A-ASB Zone 15B-ASB Zone 2NotesDuplicate for DMDS and DMS are notincluded in the average because half thedetection limit is greater than themeasured valueDuplicate for DMDS, DMS, and MMCare not included in the average becausehalf the detection limit is greater than themeasured value5C-ASB Zone 37/10/20218:14 -Aeration TankInlet7/10/202110:11 st-Aeration TankSurface7/10/202110:21 t-Aeration TankOutelt7/10/202110:23 218:00 /9/20215:40 100%7/9/20218:00 20215:45 :00 215:00 420.26-100%7/9/20218:05 7/9/20215:05 -88%1A ASB InfluentThe original results were above thecalibration range and are not included inthe average1B ASB Effluent2A Foul Condensate2B Stripped Condensate(a)Duplicate not averaged because so low incomparison with other samples.Duplicate is not averaged because halfthe detection limit is greater than themeasured valueResults in bold font were outside of the calibration range, and the laboratory report indicated that results should be considered estimated. Results initalic font were below the detection limit; half of the detection limit is reported. "N/A" is reported where results "peaked out."Results in grey shading were not averaged

APPENDIX J – TRS COMPOUND FBIO CALCULATIONS USINGH2SSIMS AND FORM XIII OF APPENDIX C TO 40 CFR PART 63

NCASI WASTEWATER HYDROGEN SULFIDE EMISSIONS SIMULATOR (H2SSIM)Version 1.3Data Type 1. Site IdentificationCompany NameNew‐IndyData Type 5. Zone Physical and Chemical ConditionsZone ConditionZone 1Zone 2Zone 3Facility NameCatawba SCDissolved Oxygen0.690.292Basin NameASBTemperature95.889.287.2pH8.758.578.74Data Type 2. Model Zone InformationZone 4UnitsFRun H2SSIMs.u.Number of Zones3Zone Location pe of BasinRedox ConditionData Type 3. Load .33MGDNumber of Aerators16156Total Sulfide0.025114.2mg/LTotal Horsepower12001125450Sulfate390390mg/LImpellor Size1.6251.6251.625Impellor RPM120012001200Diffused Air Flow000cmsWeir Height000feetData Type 4. Atmospheric el Controlsmg/LHPfeetRPMViewParametersClear InputSheet

H2SSIM ResultsBasin EmissionsTotal Emissions (H2S)Total Emissions (H2S)Total Emissions (H2S)Total Emissions (H2S)Emission Flux (H2S)Current taOx0.0061.05Unitsm1211.9gms/m yrZone EmissionsZone Emissions (H2S)Zone Emissions (H2S)Emission Flux (H2S)Liquid Conc. (Total Sulfide)Liquid Sulfide Load (lbs/yr)Zone 1Zone 2Zone S196.11Percent Inlet Sulfide Removed95.8%Zone 4214.711.99.9gms/m yrO2 Transfer Coeff.20.0100.0080.001mg/Lalpha 10.83119.30096.50011.100lbs/yralpha 20.6

NCASI WASTEWATER HYDROGEN SULFIDE EMISSIONS SIMULATOR (H2SSIM)Version 1.3Data Type 1. Site IdentificationCompany NameNew‐IndyData Type 5. Zone Physical and Chemical ConditionsZone ConditionZone 1Zone 2Zone 3Facility NameCatawba SCDissolved Oxygen0.060.051.5Basin NameASBTemperature97.1689.687.8pH8.088.398.38Data Type 2. Model Zone InformationZone 4UnitsFRun H2SSIMs.u.Number of Zones3Zone Location pe of BasinRedox ConditionData Type 3. Load .36MGDNumber of Aerators16156Total Sulfide0.01296.9mg/LTotal Horsepower12001125450Sulfate390390mg/LImpellor Size1.6251.6251.625Impellor RPM120012001200Diffused Air Flow000cmsWeir Height000feetData Type 4. Atmospheric el Controlsmg/LHPfeetRPMViewParametersClear InputSheet

H2SSIM ResultsBasin EmissionsTotal Emissions (H2S)Total Emissions (H2S)Total Emissions (H2S)Total Emissions (H2S)Emission Flux (H2S)Current etaOx0.0061.05Unitsm1224.1gms/m yrZone EmissionsZone Emissions (H2S)Zone Emissions (H2S)Emission Flux (H2S)Liquid Conc. (Total Sulfide)Liquid Sulfide Load (lbs/yr)Zone 1Zone 2Zone S232.67Percent Inlet Sulfide Removed90.6%Zone 4249.220.610.2gms/m yrO2 Transfer Coeff.20.0470.0410.002mg/Lalpha 10.83553.500476.40018.500lbs/yralpha 20.6

NCASI WASTEWATER HYDROGEN SULFIDE EMISSIONS SIMULATOR (H2SSIM)Version 1.3Data Type 1. Site IdentificationCompany NameNew‐IndyData Type 5. Zone Physical and Chemical ConditionsZone ConditionZone 1Zone 2Zone 3Facility NameCatawba SCDissolved Oxygen0.110.111Basin NameASBTemperature93.329289.54pH8.028.017.99Data Type 2. Model Zone InformationZone 4UnitsFRun H2SSIMs.u.Number of Zones3Zone Location pe of BasinRedox ConditionData Type 3. Load .33MGDNumber of Aerators21156Total Sulfide0.01446.9mg/LTotal Horsepower15751125450Sulfate390390mg/LImpellor Size1.6251.6251.625Impellor RPM120012001200Diffused Air Flow000cmsWeir Height000feetData Type 4. Atmospheric el Controlsmg/LHPfeetRPMViewParametersClear InputSheet

H2SSIM ResultsBasin EmissionsTotal Emissions (H2S)Total Emissions (H2S)Total Emissions (H2S)Total Emissions (H2S)Emission Flux (H2S)Current etaOx0.0061.05Unitsm1224.2gms/m yrZone EmissionsZone Emissions (H2S)Zone Emissions (H2S)Emission Flux (H2S)Liquid Conc. (Total Sulfide)Liquid Sulfide Load (lbs/yr)Zone 1Zone 2Zone S272.2Percent Inlet Sulfide Removed79.1%Zone 4242.224.911.1gms/m yrO2 Transfer Coeff.20.0280.0240.002mg/Lalpha 10.83319.800265.30027.600lbs/yralpha 20.6

NCASI WASTEWATER HYDROGEN SULFIDE EMISSIONS SIMULATOR (H2SSIM)Version 1.3Data Type 1. Site IdentificationCompany NameFacility NameBasin NameNew‐IndyData Type 5. Zone Physical and Chemical ConditionsZone ConditionZone 1Zone 2Catawba SCDissolved Oxygen0Primary ClarifierTemperature135.8pH9.01Data Type 2. Model Zone InformationZone 3Zone 4UnitsFRun H2SSIMs.u.Number of Zones1Zone Location metersMixingModerateType of BasinRedox ConditionData Type 3. Load nfluentUnitsAnoxicFlow24.060MGDNumber of Aerators0Total Sulfide114.20mg/LTotal Horsepower0Sulfate3900mg/LImpellor Size1.625Impellor RPM1200Diffused Air Flow0Weir Height0.38Data Type 4. Atmospheric el feetRPMcmsmetersViewParametersClear InputSheet

H2SSIM ResultsBasin EmissionsTotal Emissions (H2S)Total Emissions (H2S)Total Emissions (H2S)Total Emissions (H2S)Emission Flux (H2S)Current m yrkanoxThetaOx0.0061.05Zone 1Zone 2Unitsm10.00gms/sn0.2167.6lbs/yrMLVSS2500gms/m yrO2 Transfer Coeff.2Zone EmissionsZone Emissions (H2S)Zone Emissions (H2S)Emission Flux (H2S)Liquid Conc. (Total Sulfide)Liquid Sulfide Load (lbs/yr)5.076mg/Lalpha 10.8358634.300lbs/yralpha 20.6Percent Inlet Sulfide Removed99.3%10.8Zone 3Zone 42

NCASI WASTEWATER HYDROGEN SULFIDE EMISSIONS SIMULATOR (H2SSIM)Version 1.3Data Type 1. Site IdentificationCompany NameNew‐IndyData Type 5. Zone Physical and Chemical ConditionsZone ConditionZone 1Zone 2Facility NameCatawba SCDissolved Oxygen0Basin NamePrimary ClarifierTemperature133.4pH9.1Data Type 2. Model Zone InformationZone 3Zone 4UnitsFRun H2SSIMs.u.Number of Zones1Zone Location metersMixingModerateType of BasinRedox ConditionData Type 3. Load ardpipeUnitsAnoxicFlow23.980MGDNumber of Aerators0Total Sulfide96.90mg/LTotal Horsepower0Sulfate3900mg/LImpellor Size1.625Impellor RPM1200Diffused Air Flow0Weir Height0.38Data Type 4. Atmospheric el feetRPMcmsmetersViewParametersClear InputSheet

H2SSIM ResultsBasin EmissionsTotal Emissions (H2S)Total Emissions (H2S)Total Emissions (H2S)Total Emissions (H2S)Emission Flux (H2S)Current 0028.0gms/m yrZone 1Zone 2Zone EmissionsZone Emissions (H2S)Zone Emissions (H2S)Emission Flux (H2S)Liquid Conc. (Total Sulfide)Liquid Sulfide Load (lbs/yr)Percent Inlet Sulfide Removed99.2%Zone 3Zone 428.0gms/m yrO2 Transfer Coeff.24.610mg/Lalpha 10.8353070.200lbs/yralpha 20.6

NCASI WASTEWATER HYDROGEN SULFIDE EMISSIONS SIMULATOR (H2SSIM)Version 1.3Data Type 1. Site IdentificationCompany NameNew‐IndyData Type 5. Zone Physical and Chemical ConditionsZone ConditionZone 1Zone 2Facility NameCatawba SCDissolved Oxygen0Basin NamePrimary ClarifierTemperature130.6pH9.04Data Type 2. Model Zone InformationZone 3Zone 4UnitsFRun H2SSIMs.u.Number of Zones1Zone Location metersMixingModerateType of BasinRedox ConditionData Type 3. Load ardpipeUnitsAnoxicFlow23.140MGDNumber of Aerators0Total Sulfide46.90mg/LTotal Horsepower0Sulfate3900mg/LImpellor Size1.625Impellor RPM1200Diffused Air Flow0Weir Height0.38Data Type 4. Atmospheric el feetRPMcmsmetersViewParametersClear InputSheet

H2SSIM ResultsBasin EmissionsTotal Emissions (H2S)Total Emissions (H2S)Total Emissions (H2S)Total Emissions (H2S)Emission Flux (H2S)Current 24.7gms/m yrZone 1Zone 2Zone EmissionsZone Emissions (H2S)Zone Emissions (H2S)Emission Flux (H2S)Liquid Conc. (Total Sulfide)Liquid Sulfide Load (lbs/yr)Percent Inlet Sulfide Removed99.2%Zone 3Zone 424.7gms/m yrO2 Transfer Coeff.22.470mg/Lalpha 10.8327436.200lbs/yralpha 20.6

NCASI WASTEWATER HYDROGEN SULFIDE EMISSIONS SIMULATOR (H2SSIM)Version 1.3Data Type 1. Site IdentificationCompany NameNew‐IndyData Type 5. Zone Physical and Chemical ConditionsZone ConditionZone 1Zone 2Facility NameCatawba SCDissolved Oxygen0.25Basin NamePost ASB TankTemperature85.2pH7.67Data Type 2. Model Zone InformationZone 3Zone 4UnitsFRun H2SSIMs.u.Number of Zones1Zone Location tMixingModerateType of BasinRedox ConditionData Type 3. Load erateFlow24.390MGDNumber of Aerators2Total Sulfide0.00250mg/LTotal Horsepower150Sulfate3900mg/LImpellor Size1.625Impellor RPM1200Diffused Air Flow0cmsWeir Height0metersData Type 4. Atmospheric el Controlsmg/LHPfeetRPMViewParametersClear InputSheet

H2SSIM ResultsBasin EmissionsTotal Emissions (H2S)Total Emissions (H2S)Total Emissions (H2S)Total Emissions (H2S)Emission Flux (H2S)Current 002304.3gms/m yrZone EmissionsZone Emissions (H2S)Zone Emissions (H2S)Emission Flux (H2S)Liquid Conc. (Total Sulfide)Liquid Sulfide Load (lbs/yr)Zone 1Zone 2Percent Inlet Sulfide Removed‐26.6%Zone 3Zone 42304.3gms/m yrO2 Transfer Coeff.20.007mg/Lalpha 10.8385.400lbs/yralpha 20.6

NCASI WASTEWATER HYDROGEN SULFIDE EMISSIONS SIMULATOR (H2SSIM)Version 1.3Data Type 1. Site IdentificationCompany NameNew‐IndyData Type 5. Zone Physical and Chemical ConditionsZone ConditionZone 1Zone 2Facility NameCatawba SCDissolved Oxygen0.53Basin NamePost ASB TankTemperature84.5pH7.69Data Type 2. Model Zone InformationZone 3Zone 4UnitsFRun H2SSIMs.u.Number of Zones1Zone Location tMixingModerateType of BasinRedox ConditionData Type 3. Load erateFlow24.340MGDNumber of Aerators2Total Sulfide0.000830mg/LTotal Horsepower150Sulfate3900mg/LImpellor Size1.625Impellor RPM1200Diffused Air Flow0cmsWeir Height0metersData Type 4. Atmospheric el Controlsmg/LHPfeetRPMViewParametersClear InputSheet

H2SSIM ResultsBasin EmissionsTotal Emissions (H2S)Total Emissions (H2S)Total Emissions (H2S)Total Emissions (H2S)Emission Flux (H2S)Current 2135.7gms/m yrZone EmissionsZone Emissions (H2S)Zone Emissions (H2S)Emission Flux (H2S)Liquid Conc. (Total Sulfide)Liquid Sulfide Load (lbs/yr)Zone 1Zone 2Percent Inlet Sulfide Removed‐70.8%Zone 3Zone 42135.7gms/m yrO2 Transfer Coeff.20.003mg/Lalpha 10.8338.300lbs/yralpha 20.6

NCASI WASTEWATER HYDROGEN SULFIDE EMISSIONS SIMULATOR (H2SSIM)Version 1.3Data Type 1. Site IdentificationCompany NameNew‐IndyData Type 5. Zone Physical and Chemical ConditionsZone ConditionZone 1Zone 2Facility NameCatawba SCDissolved Oxygen3.68Basin NamePost ASB TankTemperature84.5pH7.6Data Type 2. Model Zone InformationZone 3Zone 4UnitsFRun H2SSIMs.u.Number of Zones1Zone Location tMixingModerateType of BasinRedox ConditionData Type 3. Load erateFlow23.470MGDNumber of Aerators2Total Sulfide0.00180mg/LTotal Horsepower150Sulfate3900mg/LImpellor Size1.625Impellor RPM1200Diffused Air Flow0cmsWeir Height0metersData Type 4. Atmospheric el Controlsmg/LHPfeetRPMViewParametersClear InputSheet

H2SSIM ResultsBasin EmissionsTotal Emissions (H2S)Total Emissions (H2S)Total Emissions (H2S)Total Emissions (H2S)Emission Flux (H2S)Current 245.9gms/m yrZone EmissionsZone Emissions (H2S)Zone Emissions (H2S)Emission Flux (H2S)Liquid Conc. (Total Sulfide)Liquid Sulfide Load (lbs/yr)Zone 1Zone 2Percent Inlet Sulfide Removed75.4%Zone 3Zone 4245.9gms/m yrO2 Transfer Coeff.20.001mg/Lalpha 10.839.100lbs/yralpha 20.6

Page 1Appendix C FormsAPPENDIX C FORMS - CALCULATING FRACTION BIODEGRADEDData Date:Instructions:7/9/21Enter data in green shaded sections of this page of this spreadsheet only.I. BIOTREATMENT UNIT DESCRIPTIONNumber of 75 HP AeratorsNumber of 100 HP AeratorsTotal HorsepowerTemperatureLengthWidthAverage DepthAerator RotationAgitation Area per 75 HP aeratorAgitation Area per 100 HP aeratorImpellor DiameterUnitsZone 1Zone 2Zone 619.56045030.671248624312001452220619.5II. OVERALL PARAMS - total flowsFlowm3/secInfluent ConcentrationEffluent ConcentrationWind SpeedIV. RESULTSfbio - MMCFraction biodegradedFraction air emissionsFraction remaining in unit effluentII. OVERALL PARAMS - individual flowsFlowMGD24.39MMCmg/L0.090.00mphFlowMGDInlet Stream **24.06Condensate Stream0.327Outlet24.392** except condensate flowMMCmg/L0.000236.73130.00072NA - individual flow/conc data not availableIII. ZONE DATAMMCUnitsConc.mg/LTemp.FInlet0.09Average Zone ConcentrationZone 1Zone 2Zone 5982.86082.00.8Input 07098/25/2021 2:01 PM

Page 2APPENDIX C FORMS - CALCULATING FRACTION BIODEGRADEDPARAMETERS FOR CALCULATING MASS TRANSFER COEFIICIENTSData Date:Methyl MercaptanGeneralviscosity of airviscosity of waterdensity of airdensity of waterMW of airMW of waterDiff of O2 in H2Ograv const.RAerator Motor EffO2 Trans CorrectWind SpeedDiff of EtherO2 Trans7/9Diff in g/molcm2/slb-ft/s2/lbatm-m3/mol Kfractionm/sm/slb O2/HP-hDiff in 32.178.21E-050.850.831.698.50E-063Henry's fBetaUDetherJEquil. Ratio (Hc)or (Keq)m3 liq to m3 gas1.29E-01MWg/mol48.1ScG0.671Antoine Eqtnbc942.8239.07TURBULENTKL ParamsZone 1Zone 2Zone 3w126.3126.3126.3Re2.07E 06 2.07E 06 2.07E 06PI350633506335063Power Number, p7.92E-04 7.92E-04 7.92E-04Fr8.06E 02 8.06E 02 8.06E 02Total TurbArea (ft2)23232217808712Total TurbArea (m2)2158.32023.4809.3Frac. Agitated0.0440.0300.011(by surface aerators)QUIESCENT0.980.92Depth1.37SurfArea (ft2)532900715208778752SurfArea (m2)49573.02 66532.22 72443.40F/D Ratio183298332NANANAThese Parameters are used ScL - MMCwhen F/D 14 AND U 3.25m/sDIFFUSEDAir flow, cfmAir flow, m3/sParams 070900.00000.00000.0008/25/20212:01 PM

Stripping Coefficients (KL)Page 3APPENDIX C FORMS - CALCULATING FRACTION BIODEGRADEDCalculating Mass Transfer Coefficient KL for Various ZonesData Date:7/9Surface AerationTurbulent AreaZone1MMCZone 2MMCZone 3MMCQuiescient AreakL, m/sU10 3.25F/D 14 14 F/D 51.2 F/D 51.2Temp AdjHkGm/skLm/sKL turbm/skGm/sU10 034.02E-06NAKL 0709kLm/sKL quiscm/sKL 02E-064.00E-061.33E-048/25/20212:01 PM

Page 4FORM XIII. DATA FORM FOR THE ESTIMATION OF MULTIPLE ZONEBIODEGRADATION FROM UNIT CONCENTRATIONSData Date:7/9NAME OF THE FACILITYCOMPOUND for site specific biorate determinationNumber of zones in the biological treatment unitVOLUME of full-scale system (cubic meters)Average DEPTH of the full-scale system (meters)FLOW RATE of wastewater to the unit (m3/s)FLOW RATE of condensate to the unit (m3/s)Total wastewater flowrate - (including condensates) (m3/s)ESTIMATE OF KL (m/s)Concentration in the wastewater treated in the unit (mg/L)Concentration in the condensates (mg/L)Concentration in wastewater (total - inc. cond) in (mg/L)Concentration in the effluent (mg/L)123455-A6788-A9TOTAL INLET FLOW (m3/s) line 4 plus the number on line 5 (or 5-A)TOTAL RESIDENCE TIME (s) line 2 divided by line 10.TOTAL AREA OF IMPOUNDMENT (m2) line 2 divided by line 3Lines 13 through 15 Not UsedZoneNumberConcentration for zone,Ci (mg/L)10.17977858320.032830.002987167456TOTALS - sum for each zone.15Area of thezone, A (m2)49506.4166442.823272346.0608101112Estimate of KLin the emoval by air stripping (g/s). Line 16.Loading in effluent (g/s). Line 9 times line 10.Total loading (g/s). {(line 5*line 8) (line 4*line 7)} or {line 5-A*line 8-A}.Removal by biodegradation (g/s) Line 19 minus (line 17 line 18).Fraction biodegraded: Divide line 20 by line 19.Fraction air emissions: Divide line 17 by line 19.Fraction remaining in unit effluent. Divide line 18 by 19.FormXIII 0709MMC198890.561.08783331.0540.0141.069see 301828322.15 daysAIR STRIPPINGKL A Ci (g/s)5.0623 2.82E 010.7940 24.206750.029 59.82860.8200.0088/25/20212:01 PM

Page 1Appendix C FormsAPPENDIX C FORMS - CALCULATING FRACTION BIODEGRADEDData Date:Instructions:7/10/21Enter data in green shaded sections of this page of this spreadsheet only.I. BIOTREATMENT UNIT DESCRIPTIONNumber of 75 HP AeratorsNumber of 100 HP AeratorsTotal HorsepowerTemperatureLengthWidthAverage DepthAerator RotationAgitation Area per 75 HP aeratorAgitation Area per 100 HP aeratorImpellor DiameterUnitsZone 1Zone 2Zone 619.56045031.001248624312001452220619.5II. OVERALL PARAMS - total flowsFlowm3/secInfluent Concentration1.314Effluent ConcentrationWind SpeedIV. RESULTSfbio - MMCFraction biodegradedFraction air emissionsFraction remaining in unit effluentII. OVERALL PARAMS - individual flowsFlowMGD24.34MMCmg/L0.070.00095mphFlowMGDInlet Stream **23.98Condensate Stream0.355Outlet24.338** except condensate flowMMCmg/L0.00044.8270.0009NA - individual flow/conc data not availableIII. ZONE DATAMMCUnitsConc.mg/LTemp.FInlet0.1Average Zone ConcentrationZone 1Zone 2Zone 7094.37192.91.3Input 07108/25/2021 2:01 PM

Page 2APPENDIX C FORMS - CALCULATING FRACTION BIODEGRADEDPARAMETERS FOR CALCULATING MASS TRANSFER COEFIICIENTSData Date:Methyl MercaptanGeneralviscosity of airviscosity of waterdensity of airdensity of waterMW of airMW of waterDiff of O2 in H2Ograv const.RAerator Motor EffO2 Trans CorrectWind SpeedDiff of EtherO2 Trans7/10Diff in lg/molcm2/slb-ft/s2/lbatm-m3/mol Kfractionm/sm/slb O2/HP-hDiff in 532.178.21E-050.850.831.698.50E-063Henry's fBetaUDetherJEquil. Ratio (Hc)or (Keq)m3 liq to m3 gas1.29E-01MWg/mol48.1ScG0.671Antoine Eqtnbc942.828239.07TURBULENTKL ParamsThese Parameters are usedwhen F/D 14 AND U 3.25m/sZone 1Zone 2Zone 3w126.3126.3126.3Re2.07E 06 2.07E 06 2.07E 06PI350633506335063Power Number, p7.92E-04 7.92E-04 7.92E-04Fr8.06E 02 8.06E 02 8.06E 02Total TurbArea (ft2)23232217808712Total TurbArea (m2)2158.32023.4809.3Frac. Agitated0.0440.0300.011(by surface aerators)QUIESCENT0.980.92Depth1.37SurfArea (ft2)532900715208778752SurfArea (m2)49573.02 66532.22 72443.40F/D Ratio183298332DIFFUSEDAir flow, cfmAir flow, m3/sParams 071000.00000.00000.0008/25/20212:01 PM

Stripping Coefficients (KL)Page 3APPENDIX C FORMS - CALCULATING FRACTION BIODEGRADEDCalculating Mass Transfer Coefficient KL for Various ZonesData Date:7/10Surface AerationTurbulent AreaZone1MMCZone 2MMCZone 3MMCQuiescient AreakL, m/sU10 3.25F/D 14 14 F/D 51.2 F/D 51.2Temp AdjHkGm/skLm/sKL turbm/skGm/sU10 034.02E-06NAKL 0710kLm/sKL quiscm/sKL 02E-064.00E-061.34E-048/25/20212:01 PM

Page 4FORM XIII. DATA FORM FOR THE ESTIMATION OF MULTIPLE ZONEBIODEGRADATION FROM UNIT CONCENTRATIONSData Date:7/10NAME OF THE FACILITYCOMPOUND for site specific biorate determinationNumber of zones in the biological treatment unitVOLUME of full-scale system (cubic meters)Average DEPTH of the full-scale system (meters)FLOW RATE of wastewater to the unit (m3/s)FLOW RATE of condensate to the unit (m3/s)Total wastewater flowrate - (including condensates) (m3/s)ESTIMATE OF KL (m/s)Concentration in the wastewater treated in the unit (mg/L)Concentration in the condensates (mg/L)Concentration in wastewater (total - inc. cond) in (mg/L)Concentration in the effluent (mg/L)123455-A6788-A9TOTAL INLET FLOW (m3/s) line 4 plus the number on line 5 (or 5-A)TOTAL RESIDENCE TIME (s) line 2 divided by line 10.TOTAL AREA OF IMPOUNDMENT (m2) line 2 divided by line 3Lines 13 through 15 Not UsedZoneNumberConcentration for zone,Ci (mg/L)10.1548520.04041666730.00016975456TOTALS - sum for each zone.15Area of thezone, A (m2)49506.4166442.823272346.0608101112Estimate of KLin the 94Removal by air stripping (g/s). Line 16.Loading in effluent (g/s). Line 9 times line 10.Total loading (g/s). {(line 5*line 8) (line 4*line 7)} or {line 5-A*line 8-A}.Removal by biodegradation (g/s) Line 19 minus (line 17 line 18).Fraction biodegraded: Divide line 20 by line 19.Fraction air emissions: Divide line 17 by line 19.Fraction remaining in unit effluent. Divide line 18 by 19.FormXIII 0710MMC198890.561.08783331.0510.0161.066see 828322.16 daysAIR STRIPPINGKL A Ci (g/s)4.4409 28.678940.9841 24.349790.002 71.9290.0138/25/20212:01 PM

Page 1Appendix C FormsAPPENDIX C FORMS - CALCULATING FRACTION BIODEGRADEDData Date:Instructions:7/11/21Enter data in green shaded sections of this page of this spreadsheet only.I. BIOTREATMENT UNIT DESCRIPTIONNumber of 75 HP AeratorsNumber of 100 HP AeratorsTotal HorsepowerTemperatureLengthWidthAverage DepthAerator RotationAgitation Area per 75 HP aeratorAgitation Area per 100 HP aeratorImpellor DiameterUnitsZone 1Zone 2Zone 619.56045031.971248624312001452220619.5II. OVERALL PARAMS - total flowsFlowm3/secInfluent Concentration1.314Effluent ConcentrationWind SpeedIV. RESULTSfbio - MMCFraction biodegradedFraction air emissionsFraction remaining in unit effluentII. OVERALL PARAMS - individual flowsFlowMGD23.47MMCmg/L0.020.0013mphFlowMGDInlet Stream **23.14Condensate Stream0.334Outlet23.472** except condensate flowMMCmg/L0.00051.05200.0013NA - individual flow/conc data not availableIII. ZONE DATAMMCUnitsConc.mg/LTemp.FInlet0.0Average Zone ConcentrationZone 1Zone 2Zone 015565.68.3Input 07118/25/2021 2:01 PM

Page 2APPENDIX C FORMS - CALCULATING FRACTION BIODEGRADEDPARAMETERS FOR CALCULATING MASS TRANSFER COEFIICIENTSData Date:Methyl MercaptanGeneralviscosity of airviscosity of waterdensity of airdensity of waterMW of airMW of waterDiff of O2 in H2Ograv const.RAerator Motor EffO2 Trans CorrectWind SpeedDiff of EtherO2 Trans7/11Diff in lg/molcm2/slb-ft/s2/lbatm-m3/mol Kfractionm/sm/slb O2/HP-hDiff in 532.178.21E-050.850.831.698.50E-063Henry's fBetaUDetherJEquil. Ratio (Hc)or (Keq)m3 liq to m3 gas1.29E-01MWg/mol48.1ScG0.671Antoine Eqtnbc942.828239.07TURBULENTKL ParamsThese Parameters are usedwhen F/D 14 AND U 3.25m/sZone 1Zone 2Zone 3w126.3126.3126.3Re2.07E 06 2.07E 06 2.07E 06PI350633506335063Power Number, p7.92E-04 7.92E-04 7.92E-04Fr8.06E 02 8.06E 02 8.06E 02Total TurbArea (ft2)30492217808712Total TurbArea (m2)2832.72023.4809.3Frac. Agitated0.0570.0300.011(by surface aerators)QUIESCENT0.980.92Depth1.37SurfArea (ft2)532900715208778752SurfArea (m2)49573.02 66532.22 72443.40F/D Ratio183298332DIFFUSEDAir flow, cfmAir flow, m3/sParams 071100.00000.00000.0008/25/20212:01 PM

Stripping Coefficients (KL)Page 3APPENDIX C FORMS - CALCULATING FRACTION BIODEGRADEDCalculating Mass Transfer Coefficient KL for Various ZonesData Date:7/11Surface AerationTurbulent AreaZone1MMCZone 2MMCZone 3MMCQuiescient AreakL, m/sU10 3.25F/D 14 14 F/D 51.2 F/D 51.2Temp AdjHkGm/skLm/sKL turbm/skGm/sU10 034.02E-06NAKL 0711kLm/sKL quiscm/sKL 02E-064.00E-061.37E-048/25/20212:01 PM

Page 4FORM XIII. DATA FORM FOR THE ESTIMATION OF MULTIPLE ZONEBIODEGRADATION FROM UNIT CONCENTRATIONSData Date:7/11NAME OF THE FACILITYCOMPOUND for site specific biorate determinationNumber of zones in the biological treatment unitVOLUME of full-scale system (cubic meters)Average DEPTH of the full-scale system (meters)FLOW RATE of wastewater to the unit (m3/s)FLOW RATE of condensate to the unit (m3/s)Total wastewater flowrate - (including condensates) (m3/s)ESTIMATE OF KL (m/s)Concentration in the wastewater treated in the unit (mg/L)Concentration in the condensates (mg/L)Concentration in wastewater (total - inc. cond) in (mg/L)Concentration in the effluent (mg/L)MMC12 198890.563 1.087833341.01450.0155-A1.0286 see table7 0.00054181.0528-A 0.015509490.001295TOTAL INLET FLOW (m3/s) line 4 plus the number on line 5 (or 5-A)TOTAL RESIDENCE TIME (s) line 2 divided by line 10.TOTAL AREA OF IMPOUNDMENT (m2) line 2 divided by line 3Lines 13 through 1

H2SSIM Results Basin Emissions Units Total Emissions (H2S) 0.071 gms/s kgen 0.25 Total Emissions (H2S) 4922.0 lbs/yr ThetaGen 1.06 Total Emissions (H2S) 2.5 tons/yr KDO 0.05 Total Emissions (H2S) 2.2 tonnes/yr KSO4 10 Emission Flux (H2S) 11.9 gms/m 2 yr kanox 0.006 ThetaOx 1.05 Zone Emissions Zone 1 Zone 2 Zone 3 Zone 4 Units m1 Zone Emissions (H2S) 0.02 0.03 0.02 gms/s n 0.2

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