Orion Star A329 Portable PH/ISE/Conductivity/RDO/DO Meter

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Thermo Scientific Orion Star A329 Portable pH/ISE/Conductivity/RDO/DO Meter Reference Guide

Ross and the COIL trade dress are trademarks of Thermo Fisher Scientific, Inc. and its subsidiaries. AQUAfast, AQUASensors, BOD AutoEZ, ionplus, KNIpHE, LogR, No Cal, ORION, perpHect, PerpHecT, pHISA, pHuture, Pure Water, Sage, ROSS, ROSS Ultra, Sure-Flow, Titrator PLUS, and TURBO2 are registered trademarks of Thermo Fisher Scientific, Inc. and its subsidiaries. A , All in One, Aplus, AUTO-BAR, AUTO-CAL, Auto-ID, AUTO-READ, AUTO-STIR, Auto-Test, AutoTration, CISA, digital LogR, DuraProbe, EZ Startup, ISEasy, Low Maintenance Triode, Minimum Stir Requirement, MSR, NISS, Optimum Results, Orion Dual Star, Orion Star, SAOB, SMART AVERAGING, SMART STABILITY, Star LogR, Star Navigator 21, Stat Face, Triode are trademarks of Thermo Fisher Scientific, Inc. and its subsidiaries. Guaranteed Success and The Technical Edge are service marks of Thermo Fisher Scientific, Inc. and its subsidiaries. 2011 Thermo Fisher Scientific Inc. All rights reserved. All trademarks are the property of Thermo Fisher Scientific, Inc. and its subsidiaries. The specifications, descriptions, drawings, ordering information and part numbers within this document are subject to change without notice. This publication supersedes all previous publications on this subject.

Thermo Scientific Orion Star A329 Portable pH/ISE/Conductivity/RDO/DO Meter Chapter 1 Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Chapter 2 Meter Overview. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 Meter Connections and Inputs. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 Power Source . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3 Electrodes and Other Connections . . . . . . . . . . . . . . . . . . . .4 Meter Display . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 Meter Keypad. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 Meter Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8 Chapter 3 Meter Setup . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9 Navigating the Setup Menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9 Setup Menu Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9 pH/ISE Channel Menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10 COND Channel Menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12 DO/RDO Channel Menu . . . . . . . . . . . . . . . . . . . . . . . . . . .14 Settings Menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16 View Log Menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .17 Diagnostics Menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .17 Chapter 4 pH, RmV and ORP Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19 pH Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19 Calibration Editing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .20 RmV Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20 ORP Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21 Chapter 5 ISE Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23 ISE Calibration. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23 Calibration Editing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .24 Chapter 6 Conductivity Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25 Automatic and Direct Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25 Calibration Editing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .26 Manual Conductivity Calibration. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26 Chapter 7 RDO/DO Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27 Air Dissolved Oxygen Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Water Dissolved Oxygen Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Manual Dissolved Oxygen Calibration. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Set Zero Dissolved Oxygen Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27 28 29 30 Chapter 8 Temperature Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31 Chapter 9 Measurement. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33

Chapter 10 Methods . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35 Saving the Current Meter Settings as a New Method. . . . . . . . . . . . . . . . . . . . . 35 Loading an Existing Method . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35 Editing, Copying or Deleting an Existing Method. . . . . . . . . . . . . . . . . . . . . . . . . 36 Chapter 11 Data Storage and Retrieval . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37 Data Storage Settings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37 Read Type Selection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .37 Computer and Printer Export Settings . . . . . . . . . . . . . . . . 38 Data Log Settings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38 Viewing the Calibration Log and Data Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39 Viewing the Calibration Log . . . . . . . . . . . . . . . . . . . . . . . . 39 Viewing the Data Log. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39 Exporting the Data Log to a Computer or Printer . . . . . . . . . . . . . . . . . . . . . . . . . 40 Clearing the Data Log. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41 Interfacing a Printer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42 Interfacing a Computer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42 Chapter 12 Customer Services . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43 Meter Errors and Recommended Actions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43 Meter Self Test and Checkout . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44 Meter Self Test . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44 Meter Checkout (pH) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44 Meter Checkout (Conductivity) . . . . . . . . . . . . . . . . . . . . . .45 Electrode Stability Test . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46 Meter Factory Reset . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47 Meter User Reset . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47 About Meter . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47 Assistance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47 Warranty and Registration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47 Ordering Information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 48 Chapter 13 Meter Compliance. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51 Notice of Compliance. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . WEEE Compliance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Declaration of Conformity. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Meter Specifications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . Appendix 1 51 51 51 53 Advanced Meter Features . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 57 Automatic pH Buffer Recognition Feature. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 57 Testing a pH Electrode for Automatic Buffer Recognition . .59 Electrode Condition Icon . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 58 Multipoint Calibration Curve Feature . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59 Automatic Blank (Non-linear) Correction Feature . . . . . . . . . . . . . . . . . . . . . . . 60 Conductivity Temperature Compensation and Reference Temperature . . . . . 62 Conductivity and Total Dissolved Solids (TDS). . . . . . . . . . . . . . . . . . . . . . . . . . . 62 Conductivity Automatic Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62 Dissolved Oxygen Barometric Pressure Compensation . . . . . . . . . . . . . . . . . . 64 Dissolved Oxygen Salinity Correction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 65

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Chapter 1 Introduction Thank you for your purchase of the Orion Star A329 portable pH/ISE/Conductivity/RDO/DO meter. These meters are capable of measuring pH, mV, relative mV (RmV), ORP, ISE, conductivity, TDS, salinity, resistivity, dissolved oxygen and temperature in C or F. The Orion Star A329 portable pH/ISE/Conductivity/RDO/DO meter features t Q) SBOHF PG UP Q) VOJUT XJUI PS SFTPMVUJPO BOE VQ UP DBMJCSBUJPO QPJOUT t N7 SFMBUJWF N7 BOE 031 SBOHF PG UP N7 XJUI N7 SFTPMVUJPO t *4& SBOHF PG UP XJUI VQ UP UISFF TJHOJmDBOU mHVSF SFTPMVUJPO BOE VQ UP mWF DBMJCSBUJPO QPJOUT t POEVDUJWJUZ SBOHF PG UP N4 DN XJUI VQ UP GPVS TJHOJmDBOU mHVSF SFTPMVUJPO BOE VQ UP mWF DBMJCSBUJPO QPJOUT t 5%4 UPUBM EJTTPMWFE TPMJET SBOHF PG UP QQU XJUI VQ UP GPVS TJHOJmDBOU mHVSF SFTPMVUJPO t 4BMJOJUZ SBOHF PG UP QQU QSBDUJDBM TBMJOJUZ PS UP QQU /B M FRVJWBMFOU XJUI QQU SFTPMVUJPO t 3FTJTUJWJUZ SBOHF PG PINT UP NFHB PINT XJUI PIN SFTPMVUJPO t %JTTPMWFE PYZHFO SBOHF PG UP NH - PS UP TBUVSBUJPO VTJOH BO 3%0 PQUJDBM EJTTPMWFE PYZHFO QSPCF BOE UP NH - PS UP TBUVSBUJPO VTJOH B QPMBSPHSBQIJD EJTTPMWFE PYZHFO QSPCF XJUI B SFTPMVUJPO PG PS NH - BOE PS TBUVSBUJPO t "650 3&"% DPOUJOVPVT XJUI IPME PQUJPO BOE UJNFE NFBTVSFNFOU NPEFT t BMJCSBUJPO FEJUJOH t QPJOU EBUB MPH t .BOVBM SFBEZ "650 3&"% BOE UJNFE EBUB MPHHJOH GVODUJPOT t *1 SBUFE EVTU QSPPG BOE XBUFSQSPPG IPVTJOH 1MFBTF SFBE UIJT SFGFSFODF HVJEF UIPSPVHIMZ "OZ VTF PVUTJEF PG UIFTF JOTUSVDUJPOT NBZ JOWBMJEBUF ZPVS XBSSBOUZ BOE cause permanent damage to the meter. Thermo Scientific Orion Star A329 Portable pH/ISE/Conductivity/RDO/DO Meter Reference Guide 1

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Chapter 2 Meter Overview Meter Connections and Inputs Power Source 1PXFS BEBQUFS JODMVEFE XJUI CFODIUPQ NFUFST TPME TFQBSBUFMZ GPS QPSUBCMF NFUFST B 4FMFDU UIF BQQSPQSJBUF XBMM TPDLFU QMVH QMBUF b. Slide off the clear plastic cover from the plug plate. D 4MJEF UIF QMVH QMBUF JOUP UIF HSPPWF PO UIF CBDL PG UIF QPXFS BEBQUFS E POOFDU UIF QPXFS BEBQUFS UP UIF NFUFS BOE QPXFS PVUMFU #BUUFSJFT JODMVEFE XJUI QPSUBCMF NFUFST TPME TFQBSBUFMZ GPS CFODIUPQ NFUFST a. Select four AA alkaline batteries. C POmSN UIBU UIF NFUFS JT QPXFSFE PGG c. Remove the battery compartment cover. J 1PSUBCMF NFUFST o MPPTFO UIF TDSFXT IPMEJOH UIF CBUUFSZ DPWFS SFMFBTF UIF UPQ QPSUJPO PG UIF battery cover from the meter (use a coin or your finger) and release the bottom portion of the battery cover. E 0SJFOUBUF UIF CBUUFSJFT BT TIPXO JO UIF CBUUFSZ DPNQBSUNFOU IPVTJOH BOE JOTFSU CBUUFSJFT F 3FQMBDF UIF CBUUFSZ DPNQBSUNFOU DPWFS 'PS QPSUBCMF NFUFST o SFQMBDF UIF TDSFXT Orion Star A Series Portable 3FNPWF TDSFXT Thermo Scientific Orion Star A329 Portable pH/ISE/Conductivity/RDO/DO Meter Reference Guide 3

Electrodes and Other Connections 1SFQBSF UIF Q) FMFDUSPEF JPO TFMFDUJWF FMFDUSPEF *4& DPOEVDUJWJUZ DFMM 3%0 PQUJDBM EJTTPMWFE PYZHFO QSPCF polarographic dissolved oxygen probe and any other applicable electrodes according to the directions in the electrode user guide. POOFDU UIF BQQSPQSJBUF JUFNT BT MBCFMFE PO UIF NFUFS BOE BT TIPXO JO UIF mHVSF CFMPX DO/ RDO ATC/ COND REF USB BNC POWER RS232 Star A329 Meter Top Panel t #/ o *OQVU GPS Q) FMFDUSPEF JPO TFMFDUJWF FMFDUSPEF *4& PS 031 SFEPY FMFDUSPEF XJUI #/ PS XBUFSQSPPG #/ DPOOFDUPS t 3&' o *OQVU GPS SFGFSFODF FMFDUSPEF XJUI TUBOEBSE NN QJO UJQ DPOOFDUPS t "5 0/ o *OQVU GPS DPOEVDUJWJUZ DFMM PS "5 QSPCF XJUI QJO .JOJ%*/ DPOOFDUPS t %0 3%0 o *OQVU GPS 3%0 PQUJDBM EJTTPMWFE PYZHFO QSPCF PS QPMBSPHSBQIJD EJTTPMWFE PYZHFO QSPCF XJUI QJO .JOJ%*/ DPOOFDUPS t 1PXFS o *OQVU GPS UIF QPXFS BEBQUFS t 64# o *OQVU GPS UIF 64# DBCMF VTFE UP DPOOFDU UIF NFUFS UP B QSJOUFS PS DPNQVUFS t 34 o *OQVU GPS UIF 34 DBCMF VTFE UP DPOOFDU UIF NFUFS UP B QSJOUFS PS DPNQVUFS 4 Thermo Scientific Orion Star A329 Portable pH/ISE/Conductivity/RDO/DO Meter Reference Guide

Meter Display Display Icon Description 4IPXO XIFO UIF NFUFS JT SVOOJOH PO " QPXFS 4IPXO XIFO UIF NFUFS IBT CBUUFSJFT JOTUBMMFE Indicates data is being sent to a computer or printer. Indicates data is being sent to the data log. 4IPXO XIFO BO BMBSN JT TFU BOE UIF BMBSN WBMVF JT SFBDIFE *OEJDBUFT UIF NFUFS JT TFU UP CF JOUFSGBDFE XJUI B QSJOUFS PS DPNQVUFS WJB UIF 34 QPSU VUFS WJB UIF 34 QPSU *OEJDBUFT UIF NFUFS JT TFU UP CF JOUFSGBDFE XJUI B QSJOUFS PS DPNQVUFS WJB UIF 64# QPSU Displays the time and date entered in the setup menu. C 25.0 ATC HOLD %JTQMBZT UIF DVSSFOU UFNQFSBUVSF CBTFE PO UIF UFNQFSBUVSF QSPCF SFBEJOH PS FOUFSFE UFNQFSBUVSF WBMVF 4IPXT UIF PSJHJO PG UIF UFNQFSBUVSF BT ."/ FOUFSFE UFNQFSBUVSF PS "5 UFNQFSBUVSF QSPCF 4IPXO XIFO is pressed and the displayed measurement is frozen. *OEJDBUFT B DBMJCSBUJPO XBT TVDDFTTGVMMZ DPNQMFUFE *DPO XJMM CMJOL XIFO UIF DBMJCSBUJPO BMBSN JT TFU BOE UIF alarm value is reached. *OEJDBUFT UIF Q) FMFDUSPEF DPOEJUJPO BT HPPE UXP CBST GBJS POF CBS PS CBE TMBTI UISPVHI JU CBTFE PO UIF MBTU saved calibration and measurement stability. M 100 Indicates a method is in use and the number of the method being used. pH *OEJDBUFT UIF UZQF PG NFBTVSFNFOU BOE EFUFSNJOFT UIF UZQF PG DBMJCSBUJPO UIBU XJMM CF QFSGPSNFE ready Specifies the stability of the electrode as stabilizing or ready. 4IPXO XIFO UIF NFUFS JT JO "650 3&"% NPEF 5IF JDPO XJMM CMJOL XIJMF UIF SFBEJOH JT TUBCJMJ[JOH BOE TUPQ CMJOLJOH XIFO UIF SFBEJOH JT TUBCMF BOE UIF NFBTVSFNFOU JT MPDLFE PO UIF EJTQMBZ 7.000 pH %JTQMBZT UIF NFBTVSFNFOU WBMVF CBTFE PO UIF MBTU TBWFE DBMJCSBUJPO BOE DVSSFOU FMFDUSPEF SFBEJOH 6OJUT BSF TIPXO UP UIF SJHIU PG UIF WBMVF 0.0mV 4IPXT UIF SBX NJMMJWPMU SFBEJOH PG UIF FMFDUSPEF pH and ISE modes only. BUFFERS: 1.68, 4IPXT UIF CVGGFS WBMVFT VTFE GPS UIF MBTU TBWFE DBMJCSBUJPO pH mode only. STANDARDS: 0.10 1.0 10 4IPXT UIF TUBOEBSE WBMVFT VTFE GPS UIF MBTU TBWFE DBMJCSBUJPO ISE mode only. Std: 100 1413 12.9mS Cell Constant : 0.4750 Tc:-Ln Auto Baro Press : 757.3 Salt: 0.0 4IPXT UIF DPOEVDUJWJUZ TUBOEBSET VTFE GPS UIF MBTU TBWFE BVUPNBUJD PS EJSFDU DBMJCSBUJPO Conductivity mode only. 4IPXT UIF DFMM DPOTUBOU TFU JO UIF MBTU TBWFE NBOVBM DBMJCSBUJPO Conductivity mode only. 4IPXT UIF UZQF PG UFNQFSBUVSF DPNQFOTBUJPO JO VTF GPS DPOEVDUJWJUZ NFBTVSFNFOUT Conductivity mode only. 4IPXT UIF CBSPNFUSJD QSFTTVSF NFBTVSFE CZ UIF NFUFS (Auto) or entered by operator (Man.) and used to correct dissolved oxygen measurements. RDO/DO modes only. Displays the salinity correction factor used to correct dissolved oxygen measurements. RDO/DO modes only. 4IPXT UIF PQFSBUPS BTTJHOFE TBNQMF *% OVNCFS 4IPXT UIF PQFSBUPS BTTJHOFE VTFS *% OVNCFS cal %JTQMBZT UIF BDUJPO UIBU XJMM CF QFSGPSNFE XIFO f1 is pressed. sample ID %JTQMBZT UIF BDUJPO UIBU XJMM CF QFSGPSNFE XIFO f2 is pressed. channel %JTQMBZT UIF BDUJPO UIBU XJMM CF QFSGPSNFE XIFO f3 is pressed. Thermo Scientific Orion Star A329 Portable pH/ISE/Conductivity/RDO/DO Meter Reference Guide 5

Meter Keypad measure (esc) Orion Star A200 and A300 Series Portable Keypad setup hold mode log/print Press the f1, f2 and f3 GVODUJPO LFZT UP QFSGPSN UIF BDUJPO TIPXO BCPWF FBDI LFZ PO UIF EJTQMBZ Press to turn the meter on. 8IFO UIF NFUFS JT PO QSFTT BOE RVJDLMZ SFMFBTF UP UVSO UIF EJTQMBZ CBDLMJHIU PO PS PGG PS IPME EPXO UP turn the meter off. In the measurement mode, press to take a measurement. In the setup, calibration and other menus, press to escape the current menu and return to the measurement mode. In the measurement mode, press to enter the setup menu. In the setup, calibration and other menus, press to scroll up through a list of options. In the continuous measurement mode, press to hold (freeze) the displayed measurement and press again to release (unfreeze) the measurement. In the setup, calibration and other menus, press to scroll left through a list of options. In the single channel measurement modes, press to change the displayed measurement mode. Options GPS DIBOOFM BSF Q) N7 3N7 SFMBUJWF N7 031 BOE *4& 0QUJPOT GPS DIBOOFM BSF POE DPOEVDUJWJUZ 5%4 4BMJOJUZ BOE 3FT SFTJTUJWJUZ 0QUJPOT GPS DIBOOFM BSF TBU EJTTPMWFE PYZHFO JO QFSDFOU TBUVSBUJPO NH - EJTTPMWFE PYZHFO JO NJMMJHSBNT QFS MJUFS PS ¡ QSPCF NFNCSBOF UFNQFSBUVSF In the setup, calibration and other menus, press to scroll right through a list of options. In the measurement mode, press to log or print a measurement. *O UIF TFUVQ DBMJCSBUJPO BOE PUIFS NFOVT QSFTT UP TDSPMM EPXO UISPVHI B MJTU PG PQUJPOT 6 Thermo Scientific Orion Star A329 Portable pH/ISE/Conductivity/RDO/DO Meter Reference Guide

1SFTT UP QPXFS UIF NFUFS PO 8IFO UIF NFUFS JT PO QSFTT BOE RVJDLMZ SFMFBTF on or off or press and hold 2. Press to turn the backlight GPS BCPVU UISFF TFDPOET UP QPXFS UIF NFUFS PGG to exit any meter function and return to the measurement mode. 3. The f1, f2, and f3 GVODUJPO LFZT QFSGPSN B WBSJFUZ PG NFUFS PQFSBUJPOT 5IF NFOV TQFDJmD PQFSBUJPO JT TIPXO above each key on the display. For example, press f1 in the measurement mode to start a calibration. 5IF , , or LFZT BSF VTFE BT OBWJHBUJPO LFZT VQ SJHIU EPXO MFGU XIFO TFMFDUJOH GSPN B mYFE list or grid of meter options. In the measurement mode, these keys are used to access the setup menu, change the measurement mode, manually log or print a measurement and hold (freeze) a displayed measurement in the continuous measurement mode. *O UIF DPOUJOVPVT NFBTVSFNFOU NPEF XIFO is pressed and the measurement is being held (frozen), only the LFZ XJMM CF GVODUJPOBM VOUJM UIF NFBTVSFNFOU JT SFMFBTFE VOGSP[FO Meter Maintenance 'PS SPVUJOF NFUFS NBJOUFOBODF EVTU BOE XJQF UIF NFUFS XJUI B EBNQ DMPUI *G OFDFTTBSZ XBSN XBUFS PS B NJME XBUFS CBTFE EFUFSHFOU DBO CF VTFE .FUFS NBJOUFOBODF DBO CF QFSGPSNFE PO B EBJMZ XFFLMZ PS NPOUIMZ CBTJT BT SFRVJSFE CZ UIF FOWJSPONFOU JO XIJDI UIF NFUFS JT PQFSBUFE *NNFEJBUFMZ SFNPWF BOZ TQJMMFE TVCTUBODF GSPN UIF meter using the proper cleaning procedure for the type of spill. Thermo Scientific Orion Star A329 Portable pH/ISE/Conductivity/RDO/DO Meter Reference Guide 7

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Chapter 3 Meter Setup Navigating the Setup Menu *O UIF NFBTVSFNFOU NPEF QSFTT to enter the main setup menu. 2. Press , , or to scroll through the main setup menu options. Press f3 (select) to select a main setup menu option. 3. Press to scroll through setup submenu options. Press f3 (select) to select a setup submenu option. or 1FSGPSN UIF BQQSPQSJBUF BDUJPOT UP TFU UIF EFTJSFE QBSBNFUFS JO UIF TFUVQ TVCNFOVT a. To select a value from a list of options, press f3 (select) to set the value. b. To enter a numeric value, use the numeric entry screen. or to highlight the desired value and press i. Select the value to be entered by pressing f3 (select) or f3 (edit) 5IF OVNFSJD FOUSZ TDSFFO XJMM QPQVQ PO UIF EJTQMBZ ii. Press , , or to highlight a number, decimal place or negative sign; press f3 (enter) UP TFMFDU UIF IJHIMJHIUFE JUFN BOE SFQFBU VOUJM UIF EFTJSFE WBMVF JT TIPXO PO UIF UPQ PG UIF OVNFSJD entry screen. iii. Press f2 (done) to save the value and exit the numeric entry screen. 1SFTT f1 (back) and then to return to the measurement mode at any time. Setup Menu Overview pH/ISE Channel COND Channel DO/RDO Channel Settings Log View Diagnostics Method Method Method Mode & Settings t .FBTVSF .PEF t 3FBE 5ZQF t 3FTPMVUJPO t #VGGFS (SPVQ (pH only) t .FBTVSF 6OJU (ISE only) t #MBOL PSSFDU (ISE only) t -PX -FWFM 4UBCJMJUZ Mode & Settings t .FBTVSF .PEF t 3FBE 5ZQF t FMM 5ZQF t FMM , t 5%4 'BDUPSZ (TDS only) t 5ZQF (Salinity only) t 3FG 5FNQ t 5FNQ PNQ t 5FNQ PFGG t 4UBCJMJUZ t "WFSBHJOH t -JNJU "MBSN t BM %VF "MBSN Mode & Settings t .FBTVSF .PEF t .FBTVSF 6OJU t 3FTPMVUJPO t 3FBE 5ZQF t #BSP 1SFTT t 4BMJOJUZ PSSFDU t 4UBCJMJUZ t "WFSBHJOH t -JNJU "MBSN t BM %VF "MBSN t 3%0 BQ -JGF (RDO Only) t &YQPSU %BUB t %BUB -PH t %BUF 5JNF t -BOHVBHF t ,FZ 1SFTT #FFQ t "MBSN #FFQ t POUSBTU t "VUP 4IVU 0GG t 6TFS *% t 4BNQMF *% t %BUB -PH t BMJCSBUJPO -PH t 'BDUPSZ 3FTFU t 6TFS 3FTFU t 4FMG 5FTU t 4UBCJMJUZ 5FTU t "CPVU .FUFS (ISE only) t 4UBCJMJUZ t "WFSBHJOH t -JNJU "MBSN t BM %VF "MBSN Temperature t .BOVBM 5FNQ 7BMVF t 5FNQFSBUVSF 6OJU t 5FNQFSBUVSF Calibration t 5FNQFSBUVSF *OQVU Temperature t .BOVBM 5FNQ 7BMVF t 5FNQFSBUVSF 6OJU t Temperature Calibration t 5FNQFSBUVSF Input Temperature t .BOVBM 5FNQ 7BMVF t 5FNQFSBUVSF 6OJU t 5FNQFSBUVSF Calibration t 5FNQFSBUVSF Input Thermo Scientific Orion Star A329 Portable pH/ISE/Conductivity/RDO/DO Meter Reference Guide 9

pH/ISE Channel Menu 5IF Q) *4& IBOOFM TFUVQ NFOV JT VTFE UP SFWJFX BOE DIBOHF QBSBNFUFST SFMBUJOH UP Q) N7 SFMBUJWF N7 031 BOE *4& measurements and calibrations. Main Setup Menu pH/ISE Channel 2nd Level Method 3rd Level Menu Options .FOV BMMPXT UIF DVSSFOU NFUFS TFUUJOHT UP CF TBWFE BT B OFX NFUIPE an existing method to be run on the meter, or an existing method to be WJFXFE FEJUFE DPQJFE EFMFUFE PS QSJOUFE List of Methods Mode and Settings Measure Mode Menu Description t Q) t N7 t 3N7 t 031 t *4& .FOV VTFE UP TFMFDU UIF EJTQMBZFE NFBTVSFNFOU NPEF XIJDI EFUFSNJOFT UIF UZQF PG DBMJCSBUJPO UIF NFUFS XJMM QFSGPSN .FOV VTFE UP TFMFDU IPX UIF NFUFS XJMM UBLF NFBTVSFNFOUT Auto ( )– Press to take a measurement. When the measurement is stable, it is locked on the display until is pressed again. t "VUP Read Type t POUJOVPVT t 5JNFE Continuous – The measurement is constantly updated on the display and stabilizing or ready JT TIPXO UP JOEJDBUF UIF measurement stability. Timed – Measurements are taken at a set time interval. To enter the time interval, highlight t Timed press to highlight the hours (HH), minutes (MM) or seconds (SS), press f3 (edit) and use the numeric entry screen to change the values. t %FDJNBM 1MBDF t %FDJNBM 1MBDFT Resolution (pH mode) Menu used to select the resolution for the displayed measurement values. t %FDJNBM 1MBDFT t TJHOJGJDBOU EJHJU Resolution (ISE mode) t TJHOJGJDBOU EJHJUT Menu used to select the resolution for the displayed measurement values. t TJHOJGJDBOU EJHJUT t 64" t %*/ Menu used to select the buffer group used for automatic buffer recognition during pH calibrations. 64" o Q) CVGGFST %*/ o Q) CVGGFST .FBTVSF 6OJU *4& NPEF t QQN t . t NH t 1FSDFOUBHF t QQC t /POF .FOV VTFE UP TFMFDU UIF VOJUT EJTQMBZFE XJUI *4& NFBTVSFNFOUT Blank Correct (ISE mode) t :FT t /P .FOV VTFE UP UVSO BVUPNBUJD CMBOL OPO MJOFBS DPSSFDUJPO PO PS PGG for ISE measurements. The automatic blank correction feature uses BO BMHPSJUIN UP DPNQFOTBUF GPS UIF OPO MJOFBSJUZ PG BO JPO TFMFDUJWF FMFDUSPEF JO MPX MFWFM TUBOEBSET BOE TBNQMFT Buffer Group (pH mode) -PX -FWFM 4UBCJMJUZ t 0GG (ISE mode) t 0O 10 .FOV VTFE UP UVSO MPX MFWFM TUBCJMJUZ PO PS PGG GPS *4& NFBTVSFNFOUT 5IF MPX MFWFM TUBCJMJUZ GFBUVSF JNQSPWFT UIF BDDVSBDZ PG MPX DPODFOUSBUJPO *4& NFBTVSFNFOUT CZ BMMPXJOH UIF FMFDUSPEF UP IBWF B longer amount of time to stabilize in calibration standards (about three to five minutes). Thermo Scientific Orion Star A329 Portable pH/ISE/Conductivity/RDO/DO Meter Reference Guide

pH/ISE Channel Menu (cont.) Main Setup Menu 2nd Level Mode and Settings (cont.) 3rd Level Menu Options t 4NBSU 4UBCJMJUZ t 'BTU Stability t .FEJVN t 4MPX Averaging t 0GG t "VUPNBUJD 4NBSU t -JNJU "MBSN On Off t "MBSN 4FUUJOHT -JNJU "MBSN -PX High )JHI -PX t )JHI -JNJU t -PX -JNJU Menu Description .FOV VTFE UP TFMFDU IPX UIF TUBCJMJUZ PG UIF EJTQMBZFE NFBTVSFNFOU values is indicated. Smart Stability automatically compensates for measurement conditions and optimizes the meter response time. Menu used to turn the averaging function on or off. Automatic Smart automatically compensates for measurement conditions and optimizes the meter response time. Menu used to turn the limit alarm on or off and to set the limit alarm parameters. The limit alarm is triggered if the measurement goes above B IJHI WBMVF BOE PS CFMPX B MPX WBMVF TFU CZ UIF PQFSBUPS 1SFTT or to change the setting on each line, press or to select another line and use the numeric entry screen to enter limit values. Menu used to turn the calibration due alarm on or off and to set the t BM %VF "MBSN On Cal Due Alarm Off t BM %VF -JNJU pH/ISE Channel (cont.) calibration due alarm time. The calibration due alarm is triggered if a TFU BNPVOU PG UJNF IBT QBTTFE XJUIPVU B DBMJCSBUJPO CFJOH QFSGPSNFE Press or to change the setting on the top line, press or to select another line and use the numeric entry screen to enter the calibration due value in hours. Temperature Manual Temp Value 5FNQFSBUVSF 6OJU Temperature Calibration Default value or last entered value .FOV VTFE UP TFU UIF UFNQFSBUVSF WBMVF UIBU XJMM CF VTFE GPS BMM NFBTVSFNFOUT BOE DBMJCSBUJPOT 6TF UIF OVNFSJD FOUSZ TDSFFO UP FOUFS the temperature. t FMTJVT t 'BISFOIFJU Menu used to select the temperature units. t "5 t 4PMVUJPO Temperature t .FNCSBOF Temperature t 4PM .FN Temperature t "5 4PM Mem Temp .FOV BMMPXT UIF UFNQFSBUVSF NFBTVSFE CZ BO "5 QSPCF TFQBSBUF PS built in to an electrode), solution temperature measured by a DO probe, membrane temperature measured by a DO probe or a combination of these to be adjusted by the operator. t "5 Temperature Input t %0 1SPCF t .BOVBM .FOV VTFE UP TFMFDU UIF TPVSDF PG UIF UFNQFSBUVSF NFBTVSFNFOU XIFO NVMUJQMF FMFDUSPEFT XJUI UFNQFSBUVSF GVODUJPO BSF DPOOFDUFE UP UIF NFUFS Thermo Scientific Orion Star A329 Portable pH/ISE/Conductivity/RDO/DO Meter Reference Guide 11

COND Channel Menu 5IF 0/% IBOOFM TFUVQ NFOV JT VTFE UP SFWJFX BOE DIBOHF QBSBNFUFST SFMBUJOH UP DPOEVDUJWJUZ 5%4 TBMJOJUZ BOE resistivity measurements and calibrations. Main Setup Menu COND Channel 2nd Level Method 3rd Level Menu Options .FOV BMMPXT UIF DVSSFOU NFUFS TFUUJOHT UP CF TBWFE BT B OFX NFUIPE an existing method to be run on the meter, or an existing method to be WJFXFE FEJUFE DPQJFE EFMFUFE PS QSJOUFE List of Methods Mode and Settings Measure Mode Menu Description t POEVDUJWJUZ t 4BMJOJUZ t 5%4 t 3FTJTUJWJUZ Menu used to select the displayed measurement mode. .FOV VTFE UP TFMFDU IPX UIF NFUFS XJMM UBLF NFBTVSFNFOUT Auto ( )– Press to take a measurement. When the measurement is stable, it is locked on the display until is pressed again. t "VUP Read Type t POUJOVPVT t 5JNFE Continuous – The measurement is constantly updated on the display and stabilizing or ready JT TIPXO UP JOEJDBUF UIF measurement stability. Timed – Measurements are taken at a set time interval. To enter the time interval, highlight t 5JNFE press to highlight the hours (HH), minutes (MM) or seconds (SS), press f3 (edit) and use the numeric entry screen to change the values. Cell Type t 4UBOEBSE t 641 Menu used to set the type of conductivity cell used as standard or 641 4FMFDU TUBOEBSE GPS NPTU DPOEVDUJWJUZ DFMMT PS TFMFDU 641 GPS FMFDUSPEF MPX MFWFM DPOEVDUJWJUZ DFMMT .% value or FMM , Default last entered value .FOV VTFE UP FOUFS UIF OPNJOBM DFMM DPOTUBOU , WBMVF PG UIF DPOEVDUJWJUZ cell. The nominal cell constant is used during automatic conductivity DBMJCSBUJPOT 5IF WBMVF XJUI BVUPNBUJDBMMZ VQEBUF XIFO B DPOEVDUJWJUZ calibrat

Thermo Scientific Orion Star A329 Portable pH/ISE/Conductivity/RDO/DO Meter Reference Guide

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very common in real analysis, since manipulations with set identities is often not suitable when the sets are complicated. Students are often not familiar with the notions of functions that are injective ( one-one) or surjective ( onto). Sample Assignment: Exercises 1, 3, 9, 14, 15, 20. Partial Solutions: 1.