01991 D2 Phaser MON14.qxp:210x279

Bruker AXSD2 PHASERDiffraction Solutionsthink forwardXRD

Compact all-in-onedesktop designInnovative high-endgoniometer designIntegrated PC / monitorDIFFRAC.SUITE softwareLeading detector technologyThe whole worldof X-ray diffractionon a desktop –D2 PHASERStatus display LEDsTransport handles1-dimensional LYNXEYE detectorInternal chillerUSB and Ethernet connectorsIntegrated drawer forkeyboard and mouseD2 PHASER with openedfront coverX-ray on status LEDsWhat do you obtain when patentedtechnologies, award-winning software,a fully functional PC with monitor andstate-of-the-art detectors meet up withleadership in innovative X-ray diffraction?Perfect solutions for powder diffraction.And if it all fits onto a desktop,it is called D2 PHASER!What enables this evolutionary leap to take place andhow can the amazing performance of this space savingsensation actually be explained?First of all, you develop an ultra compact goniometer,file a patent, complete the system with all the othercomponents for autonomous operation and package thewhole configuration together with a fully functional PC,monitor, keyboard and mouse, into a compact housing.Second, you use the unique DIFFRAC.SUITE softwarefor controlling the instrument and analyzing the data.Since its introduction the DIFFRAC software has developed into a high performance tool for the characterizationof crystalline phases in research and industry.Third, you use only the best components, forexample the LYNXEYE detector. This state-of-the-art andextremely efficient 1-dimensional detector simultaneously captures a large angular range and radically reducesthe measurement time: hours turn into minutes.Combining all of these incredible innovations creates adesktop X-ray diffractometer which has the analyticalperformance and functions of a large instrument, butwhich is easy to transport and opens up the whole worldof powder diffraction without a lot of infrastructure.D2 PHASER – all-in-one desktop design2D2 PHASER – never before was desktopX-ray diffraction better, smaller and morepowerful!3

Holderswith variouscavitiesHolder forautomatedsamplepreparationHolder forclaysLow backgroundholders forsmall sampleamountsAirtightholder forenvironmentsensitivesamplesHolder forfilter samplesD2 PHASER – thedesktop giant!Wishes come true – comprehensive,unique and non-destructive characterizationof crystalline samples by means of X-raydiffraction (XRD) with the D2 PHASER.Our D2 PHASER opens the door to modern XRD for you.This means qualitative and quantitative phase analysis,polymorphism investigation, the determination ofcrystallinity, all the way through to structure investigation– all of it fast, simple, efficient and with high quality.It is not just its analytical performance that makes theD2 PHASER so revolutionary, but also its flexibility inhandling very diverse samples. Different materialproperties require different sample preparations.Therefore, besides a series of standard sample holdersmade from PMMA or steel, the D2 PHASER also offersholders for small sample amounts, low-absorbing andweakly diffracting samples, for filters, for environmentsensitive samples and for examining materials that tendto show a preferred orientation.Cement &Raw MaterialsMinerals& MiningGeology &ExplorationCeramicsChemistry& CatalystsResearch& EducationPharmaceuticalsEnvironmentLYNXEYE fast-lane editionWhat makes the D2 PHASER absolutely unique is theintegration of the world's leading 1-dimensional detectorfor X-ray powder diffraction: Our LYNXEYE.With a performance enhancement in terms of intensityby a factor of more than 150, the D2 PHASER is actuallyplaying in the top class. Additionally the LYNXEYE allowssuppression of sample fluorescence providing an excellent peak-to-background ratio even for strongly fluorescent samples, eliminating any need for secondarymonochromators.D2 PHASER – slide-up front cover for sample loading, monitor remains activeD2 PHASER – X-ray diffraction in anew dimension!Phase identification and quantificationDegree of crystallinity determinationPhase properties (cell parameters,crystallite size, and lattice strain)Crystal structure analysisWide variety of different sample holders ofindustrial standard dimension (Ø 51.5 mm)45

Plug’nAnalyze On-SiteReadyHand CarryWeightNoWaterSupplyNoHighPowerNoPC &PeripheralsAll-in one is everything you need –D2 PHASERCan XRD – the best method for phasecharacterization – really produce highquality data without the need for acorresponding infrastructure?Yes! With our D2 PHASER a new era begins.All that is required is a simple domestic wall socket andyou can start producing outstanding analytical results:Plug ‘n Analyze. Since it is a desktop system it requiresonly a minimum amount of space and is in no wayinferior to a large system in terms of its analyticalperformance. Resolution, angular accuracy and datastatistics set new standards in this class of analyticalinstruments; data quality which you can rely on and withwhich even complex questions can be answered.Our D2 PHASER is a transportable all-in-one instrumentthat requires no additional cooling water or PC peripherals.This means that there is nothing to prevent it from beingused outdoors: simply switch-on a power generator, plugin the connector and start measuring!DIFFRAC.EVAQualitative phase identification- ICDD PDF2 and PDF4- User-defined databasesSemi-quantitative phase analysis- RIR method- Combined XRD-XRF analysisPublication-ready reportingDIFFRAC.TOPASQuantitative AnalysisDIFFRAC.TOPASStructure AnalysisQuantitative phase analysis- Crystalline phases- Amorphous phasesIndexing (LSI and LP-Search methods)Degree of crystallinitydeterminationSpiking methodPONKCS methodPawley and LeBail fittingRietveld structure refinementAb-initio structure determination- Simulated annealing- Charge Flipping- 3D Fourier analysisMicrostructure analysisD2 PHASER – X-ray diffraction tool foreveryone – everywhere!Minimal electrical powerconsumption (650 W)No cooling water supplyNo significant tube ageing –practically endless tube lifetimeMinimal space required67

XRD on polycrystalline material – more intensity with LYNXEYE detectorCommon point detector setupX-RaySourceScintillationCounterIn an XRD experimentperformed on polycrystalline material the incidentX-ray beam is diffracted byinnumerous crystallites inspecific 2Theta directions.SampleIncidentBeamD2 PHASER – dataquality, functionalityand safety withoutany compromisesDiffractedBeams2ThetaTo record the exact2Theta positions a narrowslit in front of a pointdetector is required.Advanced 1D detector setupThe LYNXEYE literallyprovides more than 150integrated slits, allowingmore than 150 2Thetapositions to be recordedsimultaneously.LYNXEYEMicro StripSensorWe give you our word: Good Diffraction Practice andBest Data Guarantee!Safety assurance:Each instrument always complies with the world’shighest statutory requirements regarding X-ray safety,machine and electrical safety. This certainty isobtained after stringent scrutiny by independentinstitutions.0.030The best in its class: the D2 PHASER.Shake on it!A simple domestic wallsocket is all you needIntensity increases by afactor of more than 150Minimum spacerequirementsNo installation100% working strips atdelivery – guaranteedHandles for convenienttransportationNo instrumentconfigurationEnergy discriminationfor sample fluorescencesuppressionMaximum X-ray safetywith radiation levelsignificantly below 1µSv/hNo infrastructureScanning and snapshotmodeClearly visible warningand operating elementsNo pre-installationrequirementsAngular coverage 5.5 2ThetaAlignment accuracybetter than 0.02 2Theta– guaranteedAll-in-one analytics:X-ray source:Island-mode:Simple sample loadingCommon sealedX-ray tube designInternal cooling systemNo alignmentWhy is this important?Accurate and verifiableinstrument alignment isa basic requirement foraccurate and reliable phaseidentification or structureanalysis.0.0100.000-0.010-0.020- 0.020 20.0040.0060.0080.00100.00120.00140.002Theta [ ]Unrivaled resolution5000SRM 660a4000FWHM 0.0421 2Θ30002000Very small peak width ofless than 0.05 2Thetaobtained by high-resolutionXRD measurement ofLaB6 (NIST SRM 660a)with LYNXEYE detector;0.1 divergence and 1.5 Soller slit.Why is this important?Good instrument resolutionis a prerequisite to resolveoverlapping diffractionpeaks in complex powderpatterns.1000029.908Desktop design:-0.040CountsWe guarantee that our 1-dimensional LYNXEYE is absolutely faultless! This is due to Bruker AXS’ uniquedetector design. By integrating the LYNXEYE detectorin the D2 PHASER it becomes the fastest and mostefficient desktop diffractometer in the world.Instrument alignment 0.02 2Theta over thewhole angular range –guaranteed!LYNXEYE detector:-0.030The D2 PHASER is pre-aligned at delivery. Everysingle instrument must pass our strict test procedure,which is based on the internationally accepted reference material corundum. The corundum reference issupplied with the instrument, so you can check yourinstrument at any time.Detector guarantee: 0.020 0.020Two independent, fail-safe safety circuits and “X-rayOn” monitors guarantee that the most recent radiation and personal safety regulations are observed.Alignment guarantee:LYNXEYE DetectorScintillation Counter0.040Deviation 2Theta [ ]Our D2 PHASER delivers uncompromisingly good and reliable analyses. Thestrict quality standards of our entireproduct range are applied to the assembling, testing and certified safety of theD2 PHASER!Instrument alignment – a sound base for accuracy!Plug’n Analyze:30.1030.3030.502Theta [ ]30.70Industrial standardsample holdersTheta/Theta geometry,horizontal samplesFully-fledgedintegrated PCLow power load –no tube ageingHigh speed ethernetconnection2 USB portsVirtually infinitetube lifetimeCr, Co, Cu radiationOn-site and remoteoperation30.909