Milli-Q Synthesis And Milli-Q Synthesis A10 User Manual

Milli-Q Synthesis and Milli-Q Synthesis A10User Manual

NoticeThe information in this document is subject to change without notice and should not be construed as a commitmentby Millipore Corporation. Millipore Corporation assumes no responsibility for any errors that might appear in thisdocument. This manual is believed to be complete and accurate at the time of publication. In no event shallMillipore Corporation be liable for incidental or consequential damages in connection with or arising from the use ofthis manual.CopyrightPRINTED IN FRANCE.ALL RIGHTS RESERVED.ã 2002 MILLIPORE CORPORATION.THIS BOOK OR PARTS THEREOF MAY NOT BE REPRODUCED IN ANY FORM WITHOUT THE WRITTENPERMISSION OF THE PUBLISHERS.Rev. 0 - 06/02TrademarksMillipore is a registered trademark of Millipore Corporation.Elix, Q-Gard, MilliPak and Milli-Q are registered trademarks of Millipore Corporation.Quantum, RiOs and A10 are trademarks of Millipore Corporation.Pyrogard is a registered trademark of Millipore Corporation.Teflon is a registered trademark of E.I. du Pont de Nemours & Co.Tygon is a registered trademark of the Norton Company.ASTM is a registered trademark of the American Society for Testing and Materials.Allen is a registered trademark of the Holo-Krome Technology Corporation.Santoprene is a registered trademark of Advanced Elastomer Systems.SLO-BLO is a registered trademark of Littlefuse, Inc.Windows and EXCEL are registered trademarks of Microsoft Corporation.All other trademarks are trademarks of their respective manufacturers.Milli-Q Synthesis/Milli-Q Synthesis A10

Milli-Q Synthesis and Milli-Q Synthesis A10230V version: European versionDECLARATION OF CONFORMITYEUROPEAN UNION EC DIRECTIVESDirective 89/336/CEEDirective 73/23/CEE These Lab Water Systems are designed and manufactured in application of the following European Councildirectives :- 89/336/CEE relating to Electromagnetic compatibility.- 73/23/CEE relating to electrical equipment designed for use within certain voltage limits. Standards to which conformity is declared as applicable are the following :-EN 55022 Classe B: 1998: Limits and method of radio-disturbance characteristics ofinformation technology equipment.-EN 50082-1: 1997: Electromagnetic compatibility: generic immunity standard.-EN 61000-3-2 : 1995 / A1 and A2 : 1998 / A14 : 2000 : Electromagnetic compatibility(EMC) Part 3-2: limits : Limits for harmonic current emissions (equipment input current up to andincluding 16A per phase )-EN 61000-3-3 : 1995 : Electromagnetic compatibility (EMC) Part 3: limits. Section 3 :limitation of voltage fluctuation and flicker in low voltage supply systems for equipment withrated current inferior or equal 6A.-EN 61010-1: 1993 /A2: 1995: Safety requirements for electrical equipment formeasurement, control, and laboratory use.IT IS IMPORTANT TO READ THESE INSTRUCTIONS BEFORE USING THIS EQUIPMENT.Protection insured by this device could be compromised in case of wrong use. Please follow the providedinformation. It is highly recommended not to perform any work or maintenance to the internal parts or equipment ofthe system. All internal maintenance or part replacements are to be solely performed by Millipore servicetechnicians.Here is some additional information for technical reference.Electrical specifications:Milli-Q Synthesis: 230V, 50 Hz, 0.26 AmpsMilli-Q Synthesis A10: 230V, 50 Hz, 0.26 AmpsThe rating and the specifications of all fuses used are listed in Chapter 9, Appendix 1 of this manual.The system must be electrically connected to an earth grounded power supply.In the event of any problems with this equipment, please do not hesitate to contact your local Millipore ServiceRepresentative.Milli-Q Synthesis/Milli-Q Synthesis A10

TABLE OF CONTENTSCHAPTER 11-1INTRODUCTION . 1USING THIS MANUAL .1Matching this manual with your Milli-Qâ .1How to use the keypad and the LCD .1Commonly used abbreviations in this manual .21-2SAFETY INFORMATION .31-3CONTACTING MILLIPORE .4Telephone.4Internet or Email .4CHAPTER 22-1PRODUCT INFORMATION . 5MILLI-Q PRODUCT WATER SPECIFICATIONS .5Water produced by the Milli-Q Synthesis or Synthesis A10 .5Flowrate.5Resistivity.5Particles .5Pyrogens .5TOC .5Micro-Organisms .5Comparison of Milli-Q Water and ASTM Standard Specifications .52-2SCHEMATIC OF MAIN COMPONENTS .62-3DESCRIPTION OF MAIN COMPONENTS .7Inlet Solenoid Valve .7Pressure Relief Valve.7Pump .7Q-Gard .7What are the different types of Q-Gards ?.7When do I change the Q-Gard Purification Pack ?.8UV Lamp.8When do I change the UV Lamp ? .8Quantum .8What are the different types of Quantum Cartridges ?.8When do I change the Quantum Ultrapure Cartridge ? .8Pyrogard 5000 UF Cartridge .9Resistivity Sensor.9Resistivity and temperature measurements .9Temperature Compensation / Conductivity Measurements .9Resistivity/temperature measurements in agreement with USP 24 requirements.9Milli-Q Synthesis/Synthesis A10i

TABLE OF CONTENTSPoint Of Use Valve.9MilliPak .10What types of MilliPak Filters are there ?. 10When do I change the MilliPak ? . 10A10 TOC Monitor.12What does the A10 do ?. 12What maintenance is involved with the A10 ? . 12Does the A10 need to be calibrated ? . 12TOC SUITABILITY TEST . 122-4TECHNICAL SPECIFICATIONS .13Dimensions (System and Clearance) .13Weight .13Electrical.13Measurement Ranges for TOC, Resistivity, Conductivity and Temperature.13Materials of Construction .14Noise Level .14CHAPTER 3PRE INSTALLATION .153-1PRE INSTALLATION CHECKLIST .153-2PRE INSTALLATION CHECKLIST – “ARMLESS” MILLI-QS .163-3OPTIONAL EQUIPMENT YOU MAY NEED .17Wall Mounting Bracket.17Pressure Regulator.17Ball Valve for shutting off the feedwater supply .17Remote Point Of Use Dispenser .17Remote Point Of Use Dispenser used on a “Production” type Milli-Q .18Footswitch.18Printer or Computer Cable.18Remote Display with Keypad .18“Explore Data” Software .183-4INSTALLATION REQUIREMENTS .20Consumables needed for installation .20Space and Weight Requirements.20Electrical Requirements.20Feedwater Requirements .21Environmental Requirements .21Other Requirements.213-5UNPACKING THE MILLI-Q BOX – WHAT’S INSIDE ? .22Milli-Q Synthesis/Synthesis A10ii

TABLE OF CONTENTSCHAPTER 44-1INSTALLATION . 24CONNECTING TO A SUPPLY OF FEEDWATER .24Feedwater is from a reservoir .24Feedwater is from a pressurised source such as a pipe (a loop) .244-2CONNECTION OF TUBING AND THE POWERCORD .26Feedwater Tubing.26Feedwater Pressure Relief Tubing .26UF Reject tubing .26Connecting the Power Cord .274-3INSTALLATION OF THE Q-GARD.274-4TURNING ON THE SYSTEM POWER .304-5INSTALLATION OF THE QUANTUM CARTRIDGE .304-6INSTALLATION OF THE TYGON TUBING .304-7PURGING THE AIR FROM THE SYSTEM .324-8HYDRATING THE SYSTEM .334-9INSTALLATION AND RINSING OF THE MILLIPAK .354-10 HOW TO CALIBRATE THE FLOWRATE FROM THE MILLI-Q .354-11 HOW TO CHANGE THE DISPLAYED LANGUAGE .384-12 HOW TO SHOW EITHER MW.CM OR mS/CM (RESISTIVITY OR CONDUCTIVITY UNITS) .394-13 HOW TO SHOW NON TEMPERATURE COMPENSATED RESISTIVITY OR CONDUCTIVITY VALUES .41What is temperature Compensation ? .41Why use non temperature compensated values ? .414-14 HOW TO SET THE DATE AND THE TIME OF DAY.44CHAPTER 5USING THE MILLI-Q. 465-1HOW TO GET WATER FROM THE MILLI-Q .465-2STANDBY, PRE OPERATE AND PRODUCT MODE .48What is STANDBY mode ? .48What is PRE OPERATE mode ? .48What is PRODUCT mode ? .485-3HOW TO VIEW THE RESISTIVITY, TEMPERATURE AND TOC .49Viewing Resistivity.49Viewing Temperature .49Viewing TOC .495-4HOW TO USE THE FOOTSWITCH (OPTIONAL ACCESSORY).505-5HOW TO DISPENSE AN EXACT AMOUNT OF PRODUCT WATER .505-6HOW TO VIEW THE AGE OF THE CONSUMABLES .525-7HOW TO UNDERSTAND MILLI-Q MESSAGES.54Milli-Q Synthesis/Synthesis A10iii

TABLE OF CONTENTSCHAPTER 6MAINTENANCE .576-1MAINTENANCE SCHEDULE .576-2HOW TO REPLACE THE Q-GARD.586-3HOW TO REPLACE THE QUANTUM CARTRIDGE .596-4HOW TO REPLACE THE MILLIPAK .646-5HOW TO SANITISE AND CLEAN THE UF CARTRIDGE .66How often would I normally Sanitise and Clean the UF Cartridge ? .66Things to know BEFORE you sanitise the UF Cartridge.66Sanitising and Cleaning the UF Cartridge.666-6HOW TO CLEAN THE SCREEN FILTER .706-7HOW TO TIGHTEN THE POU DISPENSER ARM .716-8HOW TO REPLACE THE A10 UV LAMP .726-9HOW TO CLEAN THE A10 TOC MONITORING DEVICE .72How long does the A10 Cleaning take ?. 72Why would I need to do an A10 Cleaning ? . 72Would an A10 Cleaning ever happen automatically ?. 72How do I do an A10 Cleaning ? . 73How do I cancel the A10 CLEANING once it is started ?. 746-10 HOW TO CALIBRATE THE A10 TOC MONITORING DEVICE .746-11 HOW TO PERFORM AN AIR PURGE .756-12 HOW TO REPLACE THE UV LAMP .76CHAPTER 7TROUBLESHOOTING .77The problem is Low or No Flowrate from the POU Dispenser .77The problem is Low Resistivity of the Product Water .78The problem is there is no power to the Milli-Q system.79The problem is there is an “ERROR Number” Alarm displayed .79Continuation of “ERROR Number” Alarm displayed .80The problem is a message is displayed with a Flashing Service or Alarm LED .81Other Troubleshooting items.82CHAPTER 8ORDERING INFORMATION .838-1CATALOGUE NUMBERS FOR CONSUMABLES .838-2CATALOGUE NUMBERS FOR ACCESSORIES .848-3CATALOGUE NUMBERS FOR ALL MILLI-QS .84CHAPTER 9APPENDIXES .85APPENDIX 1HOW TO REPLACE THE MAIN POWER FUSE .85APPENDIX 2HOW TO TRANSFER INFORMATION TO A PRINTER .86Milli-Q Synthesis/Synthesis A10iv

TABLE OF CONTENTSRequirements needed .87What to do .87What does the Printout look like ?.88APPENDIX 3HOW TO TRANSFER INFORMATION TO A COMPUTER .89Requirements needed .89How to do it.89APPENDIX 4HOW TO USE A REMOTE DISPLAY .92APPENDIX 5HOW TO USE A REMOTE POU DISPENSER .92APPENDIX 6COMP MODE 1 AND COMP MODE 2.93Milli-Q Synthesis/Synthesis A10v

INTRODUCTIONChapter 11-1INTRODUCTIONUSING THIS MANUALMATCHING THIS MANUAL WITH YOUR MILLI-QâThis manual is intended for use with a Millipore Milli-Q Synthesis or Milli-Q Synthesis A10 WaterPurification System.This Owner’s Manual is a guide for use during the installation, normal operation and maintenance of a Milli-QSynthesis or Milli-Q Synthesis A10 Water Purification System. It is highly recommended to completely read thismanual and to fully comprehend its contents before attempting installation, normal operation or maintenance of theWater Purification System.You can easily identify your type of Water Purification System if you do not see the Catalogue Number. The Milli-QSynthesis and Synthesis A10 Water Purification Systems have an Orange Door on the front cabinet.If this manual is not the correct one for your Water Purification System, then please contact Millipore.HOW TO USE THE KEYPAD AND THE LCDThe Keypad and LCD (liquid crystal display) are located on the front of the Water System Cabinet.The Keypad buttons sometimes have a slight delay when pressed. As an example, suppose you want to change theMilli-Q from STANDBY mode to PRE OPERATE mode. This is done by pressing the OPERATE/STANDBY Keypadbutton for about two seconds.There are four Keypad buttons. These are labelled as OPERATE/STANDBY, MEASURE, CLEANING and MENU.POWERS T AND B YOPERATE / STANDBYPOWERP REMEASURECLEANINGOP E RA T ESERVICESERVICEALARMALARMMENUOPERATE / STANDBYMEASURECLEANINGMENUSee the drawing above for their placement.The LCD is a backlit, dual line 16-character display.The LEDs are located to the right of the LCD (see above). The POWER LED is green. This is lit when the WaterSystem microprocessor has electrical power. The SERVICE LED is yellow. This will flash when a service type of LCDmessage is displayed (i.e. EXCH. CARTRIDGES. is shown, meaning to change the cartridges in the system). TheALARM LED is red. This will flash when an alarm condition is indicated on the LCD (i.e. PAK NOT IN PLACE,meaning a purification pack is not fully in place or is absent).Milli-Q Synthesis/Synthesis A101