BarnsteadNanopure TOC-UV
Barnstead Nanopure TOC - UVultrapure water systemOperation ManualSeries 2115 and 2117Model No.D11951D12421LT2115X1 11/23/09Voltage100V - 240V100V - 240V
Table of ContentsSafety Information .3Alert Signals .3Warnings.3Introduction .5General Usage .5General Specifications .6Environmental Conditions.7Declaration of Conformity .7Unpacking.8Installation.9Choosing a Site .9UV Lamp Installation .10Other Accessories .10Bench Mounting .11Wall Mounting .11Installing the Control Panel in a Remote Location .12Water Connections .13Tubing Installation.14Electrical Connections .14Controls .15Main Power Switch .15Control Panel .15Switches .16Initial Operation .17Cartridge Pack Installation .17Initial Rinse .18System Cleaning Procedure.19Normal Operation .21Dispensing Water .22Automatic Dispensing.22User Settings .23Adjusting Display Brightness .23Setting the Displayed Language .23Setting the Date and Time .24Setting the Cell Constant .25Use of Standby Mode.26Selecting the Set Point .26Resetting the Cleaning Timer .27Resetting the UV Timer .28Resetting the TOC Lamp Timer .28Using the TOC Analyzer .29Setting Volumetric Dispensing .30Setting Timed Dispensing.30Performing a System Flush .31Changing Purity Units.31Temperature Compensation .31Auto Standby .32Unit Under Counter.32Accessories .34Feedwater Float or Pressure Switch .34Dispense Overflow Cutoff Float .35Performing an Electronic Calibration Using the Optional N.I.S.T. Calibration Module.36Manual Remote Dispenser and Accudispense Volumetric Remote Dispenser .37Computer/Printer Setup .38Connecting Nanopure to Computer and Communicating Through the RS-232 Port Using Hyperterminal or Procomm .38Connecting and Starting the Printer .40Printer Setup.41Maintenance and Servicing .42General Cleaning Instructions .42Cell Cleaning .42System Cleaning .43System Depressurization .44Cartridge Pack Replacement .450.2 Micron Filter Replacement .46UV Lamp Replacement .47TOC Lamp Replacement .48Fuse Replacement .48Shutdown .49Troubleshooting .50Replacement Parts .54Flow Chart .56Wiring Diagram.57Ordering Procedures .58Two Year Limited Warranty.60
Safety InformationAlert SignalsWarningWarnings alert you to a possibility ofpersonal injury.CautionCautions alert you to a possibility ofdamage to the equipment.NoteNotes alert you to pertinent facts andconditions.NoteThe UV lamp contains mercury. If broken or no longer needed, do not dispose of the UV lamp in the trash.Recycle or dispose of the UV lamp ashazardous waste.Your Thermo Scientific Barnstead Nanopure TOC - UVultrapure water system has been designed with function,reliability, and safety in mind. It is your responsibility toinstall it in conformance with local electrical codes. Thismanual contains important safety information. You mustcarefully read and understand the contents of this manualprior to the use of this equipment. For safe operation,please pay attention to the alert signals throughout themanual.Water purification technology employs one or more of thefollowing: chemicals, electrical devices, mercury vaporlamps, steam and heated vessels. Care should be takenwhen installing, operating or servicing Barnstead products. The specific safety notes pertinent to this Barnsteadproduct are listed below.WarningsTo avoid electrical shock, always:1. Use a properly grounded electrical outlet ofcorrect voltage and current handling capacity.2.Do not locate the Nanopure TOC - UV directlyover equipment that requires electrical service.Routine maintenance of this unit may involvewater spillage and subsequent electrical shockhazard if improperly located.3.Replace fuses with those of the same type andrating.4.Disconnect from the power supply prior to maintenance and servicing.To avoid personal injury:1. Do not use in the presence of flammable orcombustible materials; fire or explosion mayresult. This device contains components whichmay ignite such materials.2.This device is to be used with water feeds only.Cleaning agents must be used in compliancewith instructions in this manual. Failure to comply with the above could result in explosion andpersonal injury.3
SAFETY INFORMATION3.Avoid splashing cleaning solutions on clothing orskin.4.Ensure all piping connections are tight to avoidchemical leakage.5.Ensure adequate ventilation.6.Carefully follow manufacturer’s safety instructions on labels of chemical containers and material safety data sheets.7.Depressurize system prior to removing thecartridge pack.8.This unit is equipped with an ultraviolet lamp.Ultraviolet radiation is harmful to the eyes andskin. Do not attempt to observe the lampdirectly.9.Refer servicing to qualified personnel.10. A full cartridge pack may weigh about 20 lbs.4
IntroductionCongratulations on your purchase of a BarnsteadNanopure TOC - UV ultrapure water system. This waterpurification system is designed to provide low TOC, highresistivity, reagent grade water that exceeds ASTM TypeI, ISO 3696 and CLSI-CLRW Type I standards. It uses afour-stage deionization process combined with a UV lampand a 0.2 micron filter to polish suitable feed water (distilled, deionized, or reverse osmosis) to produce low TOC( 5 ppb) water with a resistivity of up to 18.2 megohmcm. Water resistivity is continuously monitored by a resistivity cell and displayed on a digital display. Actual systemTOC values, obtained by an integrated TOC analyzer, canbe concurrently displayed with the resistivity.The electronics can be verified and calibrated utilizing aN.I.S.T. Traceable Calibration module. See accessoryordering information.Please read the instructions carefully to ensure that youreceive maximum benefit from the Nanopure UV. Also,please fill out and return the enclosed warranty registration card as it will help us assure you of proper warrantycoverage.General UsageDo not use this product for anything other than its intended usage.5
General SpecificationsDimensions and Clearance RequirementsDimensions13.5” W x 19.5” H x 17.0” D (34.3 x 49.5 x 43.2 cm)ClearancesSides - 9” (22.9 cm) minimum for servicing.Above - 3” (7.6 cm) minimum for removal of the top cover.Front - 4.75” (12.1 cm) minimum for opening the front door.Feed Water RequirementsTypesTOCTurbidityPressure RangeTemperature RangeTDS (CaCO3)SilicaSiltRO, DI, distilled.Less than 1.0 ppm.1.0 N.T.U. maximum.Gravity feed to 100 psig (7kg/cm2) maximum.4 C - 40 C (40-104 F) 70 ppm 1 ppm 5% SDIProduct WaterWater QualityResistivityTOCBacteria 18.2 mΩ-cmLess than 5 ppb 0.01 CFU/mLFlow RateUp to 2 lpm maximum at minimum inlet feed water pressure 10 PSIG with a new final filter.Volumetric DispenseAccuracy: 5%Repeatability: 3%TOC AnalyzerRangeAccuracyCycle TimeWater ConsumptionMin. Water Resistivity61 to 250 ppb 1 ppb or 15% (whichever is greater) 3.5 minutes 15 ml per cycle 10 MΩ for specified accuracy
GENERAL SPECIFICATIONSElectrical RequirementsThe Nanopure TOC - UV is equipped with 2 power cords to be plugged into an electrical outlet of the appropriate voltage.U.K. customers use cord, CRX100 and fuses for 240V installation.Model D11951, D12421 100-240 VAC, 100 watts, 47-63 Hz, 1 phaseEnvironmental ConditionsOperating:Storage:4 C - 40 C; 20% to 80% relative humidity, non-condensing. InstallationCategory II (over-voltage) in accordance with IEC 664. Pollution Degree 2 inaccordance with IEC 664.Altitude limit: 3,500 meters.-25 C to 65 C; 10% to 85% relative humidity.Declaration of ConformityWe hereby declare under our sole responsibility that this product conforms with the technical requirements ofthe following standards:EMC:EN 61000-3-2 Limits for Harmonic Current EmissionsEN 61000-3-3 Limits for Voltage Fluctuations and FlickerEN 61326-1 Electrical Equipment for Measurement, Control, and Laboratory Use; Part I:General RequirementsSafety:EN 61010-1Safety Requirements for Electrical Equipment for Measurement, Control andLaboratory Use; Part I: General Requirementsper the provisions of the Electromagnetic Compatibility Directive 89/336/EEC, as amended by 92/31/EEC and93/68/EEC, and per the provisions of the Low Voltage Directive 73/23/EEC, as amended by 93/68/EEC.The authorized representative located within the European Community is:Thermo Fisher Scientific419 Sutton RoadSouthend On SeaEssex SS2 5PHUnited KingdomCopies of the Declaration of Conformity are available upon request.7
Unpacking1.Remove the unit from its shipping container.Remove all contents carefully. Ensure that theUV lamp, feed and drain tubing, cleaning cartridge, wall bracket, accessory parts bag andpower cords (see list below) are removedfrom the packaging materials before discarding. Put the Nanopure TOC - UV on a bench.UV LampCleaning CartridgeWall Bracket (Unit)Wall Bracket (Remote Display)LMX13CMX25BC1190X12BC1190X10Accessory Parts Bag Includes:Feed Water Tube, 3/8” O.D.Drain Tube, 14” O.D.Display CableBlank DisplayPlug AdapterPower CordsTU1119X7TU1190X12WHX20DL1190X18CEX42Also required for installation:* Customer Supplied Fasteners to mount unit and remotedisplay.8
InstallationCautionWall composition, condition andconstruction as well as fastener typemust be considered when mountingthis unit. The mounting surface andfasteners selected must be capable ofsupporting a minimum of 150 lbs.(68kg). Inadequate support and/or fasteners may result in damage to mountingsurface and/or equipment. If you areunsure of mounting surfacecomposition, condition and construction or correct fasteners, consult yourbuilding maintenance group orcontractor.Choosing a SiteThe Nanopure TOC - UV features a removable controlpanel display which allows the system to be mountedalmost anywhere within the laboratory. Use the wallbracket for wall mounted systems as a template to drillmounting holes. (The Nanopure TOC - UV does notinclude screws and fasteners for mounting.) Please referto the “General Specifications” section for clearancerequirements.WarningDo not locate the Nanopure TOC - UVdirectly over equipment that requireselectrical service. Routine maintenance of this unit may involve waterspillage and subsequent electricalshock hazard if improperly located.Do not use in the presence offlammable materials; fire or explosionmay result. This device containscomponents which may ignite suchmaterials.NOTEThe outlet of a gravity feed storagereservoir must be above or at thesame level as the inlet of theNanopure TOC - UV.********************************************9
INSTALLATIONNoteThe UV lamp contains mercury. Ifbroken or no longer needed, do notdispose of the UV lamp in the trash.Recycle or dispose of the UV lamp ashazardous waste.CautionDO NOT TOUCH THE GLASS PORTION OF THE LAMP! It is recommended that lint-free gloves be wornwhen handling the lamp. The glassportion must be free of fingerprints,perspiration, etc. Even a light coatingof perspiration will reduce the effectiveness of the lamp. If the glass portion of the lamp is touched, clean itwith a damp, lint-free cloth: useisopropyl alcohol as required.UV Lamp InstallationLocate the UV chamber inside the left door of theNanopure TOC - UV. Install the UV Lamp as follows:1. Disconnect the power cord from the unit.2.Access the left side of the unit by unlatching thescrew securing the door with a flathead screwdriver. Open the door. The UV lamp will beinstalled vertically.3.Remove the UV lamp from its packaging. DONOT TOUCH THE GLASS PORTION OF THELAMP! It is recommended that lint-free glovesbe worn when handling the lamp. The glass portion must be free of fingerprints, perspiration,etc. Even a light coating of perspiration willreduce the effectiveness of the lamp. If the glassportion of the lamp is touched, clean it with adamp, lint-free cloth: use isopropyl alcohol asrequired.4.Remove black cap by sliding off UV housing.5.Insert the lamp halfway into the UV lamp chamber and plug it in, then fully insert the lamp intothe chamber.6.Make sure the UV lamp cable is tucked behindthe chamber before closing and relatching thedoor.Other AccessoriesOptional accessories for this unit include a float switch,low pressure switch, N.I.S.T. Traceable CalibrationModule, standard remote dispenser, Accudispense volumetric remote dispenser, dispense overflow cutoff floatand printer. If you purchased a float switch or low pressure switch, refer to page 31 of this manual. If you purchased a standard or Accudispense volumetric remotedispenser, refer to their respective operator’s manuals forinstallation instructions.Figure 1: UV Lamp Installation - Left side view10
INSTALLATIONCautionWall composition, condition and construction, as well as fastener type,must be considered when mountingthis unit. The mounting surface andfasteners selected must be capable ofsupporting a minimum of 150 lbs.(68kg). Inadequate support and/or fasteners may result in damage to mountingsurface and/or equipment. If you areunsure of mounting surface composition, condition and construction or correct fasteners, consult your buildingmaintenance group or contractor.NotePlease refer to the “GeneralSpecifications” section for clearancerequirements.WarningDo not locate the Nanopure TOC - UVdirectly over equipment that requireselectrical service. Routine maintenance of this unit may involve waterspillage and subsequent electricalshock hazard if improperly located.NOTEThe outlet of a gravity feed storagereservoir must be above or at thesame level as the inlet of theNanopure TOC - UV.********************Bench Mounting1.Place the Nanopure TOC - UV on a bench topthat is accessible to pretreated water, electricityand an atmospherically vented drain.Wall MountingInstall the Nanopure TOC - UV on a wall in a convenientlocation that is accessible to water, an atmosphericallyvented drain and electricity.1. Locate the wall bracket packed separately fromthe unit.2.Using the wall bracket as a template, locate anddrill the mounting holes in the wall. A minimum offour (customer-supplied) fasteners will berequired — two on the top and two on the bottom.3.Attach the wall bracket to the wall using the customer-supplied fasteners.4.Remove the locking screws on each side of thewall bracket.5.Pull the two locking slides on each side of thewall bracket out as far as they will go.6.Hang the unit on the wall bracket by sliding themounting pins into the wall bracket slots.7.Push the locking slides on each side of the wallbracket in as far as they will go.8.Replace the locking screws.************************11
INSTALLATIONNoteThe removable control panel was notdesigned to be repeatedly removedfrom the unit, therefore, you mayexperience difficulty when attemptingto remove it. It is thereforerecommended that the control panelbe permanently mounted in a remotelocation or remain intact with the unit.CautionRepeated removal and replacement ofthe control panel from the top covermay eventually cause it to becomedamaged.NoteA bracket is available that will allowyou to mount the control panel on thebench. If bench mounting is desired,please order bracket AY1367X2.NoteThe blank protective cover on the rearside panel display connector shouldremain in place when the display isnot remotely located.Installing the Control Panel in aRemote LocationFor your convenience, the control panel can be removedfrom the unit and mounted at a convenient location within10 ft. (3.1 m.) of the unit. To remove the control panelfrom the unit:1. Turn the unit OFF and disconnect it from thepower supply.2.Slide the control panel upward about 1/4” (.64cm) to 3/8” (.95 cm) - (just enough to clear connector on top cover), pull forward, and remove.(The control panel fits tightly in the unit so it maybe difficult to remove.)3.Replace the control panel with the blank panelprovided with the unit to protect the electricalconnector.4.Using the wall bracket as a template, locate anddrill the mounting holes in the wall. A minimumof two (customer-supplied) fasteners will berequired. Attach the wall bracket to the wallusing the customer-supplied fasteners.5.Locate the 25-pin connector on the back topright of the unit. Remove the protective blackcover and store it for future use if the controlpanel is returned to the top cover.6.Locate the 10 ft. (3.1 m.) 25 pin M-F cableincluded with the unit; attach the female end tothe 25 pin connector on the back top right of theunit, and the other end to the connector on thebottom of the control panel.7.Tighten the cable screws on each end to securethe cable to the unit and control panel.8.The control panel may now be mounted on thewall.Blank panelWall MountBracketFigure 2: Mounting the Control Panel12
INSTALLATIONCautionDo not
BarnsteadNanopure TOC-UV ultrapurewatersystem OperationManual Series2115and2117 ModelNo. Vol
TOC Analysis as a Non-Specific Analytical Technique TOC analysis is a “Non-Specific” analytical method. TOC is not only used in the cleaning validation process, but also for the monitoring of the pharmaceutical water used within the cleaning process and for the preparation of drugs. T
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RTCA, Inc. 1150 18th Street, NW, Suite 910 Washington, DC 20036 Phone: (202) 833-9339 Fax: (202) 833-9434 www.rtca.org RTCA Paper No. 287 -13/TOC-07 November 7, 2013 Meeting Summary, November 7, 2013 Tactical Operations Committee (TOC) The third meeting of the Tactical Operations Committee (TOC) held November 7, 2013 at RTCA
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Eli Schragenheim - Supporting TOC implementations worldwide Between the need-date and the safe-date Very often there is a considerable difference between the date we need the output and the date we can reliably commit to TOC assumes we look primarily to the safe-date Especially as CCPM is able to promise safe-dates that are better than the current actual completion dates
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