630 480 TOC-L PC - Shimadzu

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C391-E079FTotal Organic Carbon AnalyzerTOC-L

Global Standard forTOC AnalyzersCombustion Catalytic Oxidation/NDIR Detection Method TOC Analyzerswith a User-Friendly DesignTOC-V series, the world's top seller, has evolved. Easy-to-operate Output Akeyboard and easy-to-read TFT color LCD screen(standalone model)of measurement data to USB memory sticks or conventional PC printer(standalone model)wealth of options, including sea water sample measurement and compatibility with small samples volumes Space-savingand energy-saving designA Full Range of Models and OptionsProvide Total Solutions to Suit Your Application Selectfrom PC models, convenient for processing measurement data, and user-friendly standalone models Addoptions to measure everything from solid samples to gas samples TNmeasurement is also possible with the addition of the TN unitThe Utility of ShimadzuTOC AnalyzersSpace-Saving and Energy-Saving Design,Other Functions and FeaturesCompatibility of Optionsand Special AccessoriesFeaturesASI-L Autosampler and OCT-L 8-Port SamplerSpecificationsFlow Line DiagramsTNM-L Total Nitrogen Unit and SSM-5000ASolid Sample Combustion UnitExternal DimensionsDiagramsPC-Controlled ModelsStandalone Models

Process ControlEffluent treatment process controlProcesses(Plating, etching, washing, water-based cutting)Ultrapure water recycling andre-purification processesExample of TOC Measurement of Nickel Plating SolutionAnalysis instrument: TOC-LCPHMeasurement method: TOC measurement of Nickel Plating Solution,thousand fold dilution with pure water(TOC measurement (NPOC measurement) with sample acidification and sparging)Measurement results: TOC 12.80 mg/L (C.V. 0.22 %)(before dilution TOC 1.280 %)Quality ControlDrinking waterAluminum foilElectronic componentsWater supply equipmentRaw materials(Sulfuric acid, aqueous ammonia,hydrogen peroxide solution, etc.)Example of TN Measurement of Ammonium Sulfate Aqueous SolutionAnalysis instrument: TOC-LCPH TNM-LMeasurement method: TN measurement of Ammonium Sulfate Aqueous Solution,prepared nitrogen concentration 10 mg/LMeasurement results: TN 9.91 mg/L (C.V. 0.30 %)S h i m a d z uT O CUtilized in aInvestigations andExperimental ResearchGlobal environment and eutrophicationRiver water, lakes and marshes, underground water,sea water, soil, sludge, sediments, etc.Biodegradable plastics and cement secondary productsExample of TC (Total Carbon) Measurement of Poultry Manure CompostAnalysis instrument: TOC-LcsH SSM-5000A (980 C electric furnace)Measurement method: direct TC measurement of commercially availablepoultry manure compost, pulverized with a mortarMeasurement results: TC 27.26 %C (C.V. 0.57 %)4

WaterQuality ControlTap water (Drinking water, rawUltrapure waterwater)(Ultrapure water used in semiconductor manufacturing,Liquid Crystal manufacturing, pharmaceutical manufacturing,and nuclear power generation, as well as used ultrapure water)Effluent(Industrial effluent, water treatment effluent, etc.)Pool water, spa water, bath water, boiler water,water from industrial processesExample of TOC Measurement of Tap WaterAnalysis instrument: TOC-LCPHMeasurement method: TOC measurement (NPOC measurement)with sample acidification and spargingMeasurement results: TOC 932 µg/L(C.V. 0.72 %)A n a l y z e rVariety of FieldsPharmaceuticalManufacturingPharmaceutical water controlEvaluation of cleaning effectiveness(Cleaning validation)Example of TOC Measurement of Purified WaterAnalysis instrument: TOC-LCPHMeasurement method: TOC measurement (NPOC measurement)with sample acidification and spargingMeasurement results: TOC 63.3 µg/L (C.V. 2.05 %)5

Shimadzu 680 C Combustion Catalytic Oxidation/NDIR Detection MethodMeasurement System Combining Experience and ReliabilityFeaturesThe most important feature of a TOC analyzer is its ability to efficiently oxidize not only easilydecomposed, low molecular weight organic compounds, but also hard-to-decompose insolubleand macromolecular organic compounds. The 680 C combustion catalytic oxidation method,developed by Shimadzu and now used worldwide, can efficiently analyze all organiccompounds. Extremely wide measurement range from 4 µg/L to 30,000 mg/L, applicable to everythingfrom ultrapure water to highly contaminated water (TOC-LCSH/CPH)・ Capable of TC, IC, TOC ( TC-IC), and NPOC measurement; options enable POC (volatile organiccarbon), TOC via POC NPOC, and even TN (total nitrogen) measurements・ The blank check function evaluates system blanks by measuring ultrapure water processedautomatically within the instrumentTOC-LCSH/CSN Standalone Model・ The automatic dilution function enables measurements up to 30,000 mg/L Reliable sample injection system・ Automatic sample acidification and sparging・ The automatic dilution function reduces sample salinity, acidity, and alkalinity, significantly extendingthe period of use of catalysts and combustion tubes (The period of use depends on the sample andmeasurement conditions.)・ Stat or priority samples can be added at anytime to the analysis schedule without interruptingoperation even when an autosampler is used Select from 4 models to suit your application・ LCD and keyboard-equipped standalone models, and PC-controlled models・ High-sensitivity model with a detection limit of 4 µg/L, suitable for a variety of applications includingTOC-LCPH/CPN PC-Controlled Modelpure water measurements, as well as a standard model designed with cost/performance in mind Suitable for aqueous samples, as well as gas and solid samples(with manual injection kit and solid sample combustion unit) Compressed air can be used as the carrier gas(with carrier gas purification kit) Compatible with small sample volumes(with optional kit) Sea water samples can be continuously measured with minimal maintenance (withcombustion tubes for high salt samples) Measurement can be performed with good repeatability even with samples containinghighly sedimentary suspended organic matters (when high suspension kit is added)※The effect depends on sample and measurement conditionsMultifunction Sample Pretreatment Injection System6

Flow Line DiagramsTOC-LCPH High-Sensitivity ModelPrinterAcidDilution waterASI-L autosamplerDrainSparging gasSampleCarrier gasinletElectronicgas flowratecontrollerTC sampleinjection port,slide typeCarrier gasTC ction systemUltrapurewater trapfor blank checkDataprocessorUSBNon-dispersive infrareddetector (NDIR)IC sample injectionport, slide typePersonal computer(Not included inthe TOC analyzercomponents.)Dehumidifier/gaspretreatment unitIC reactionreagentIC reaction vesselTC furnaceTOC-LCSN Standard ction systemKeyboardSampleCarrier gasinletElectronicgas flowratecontrollerSparginggasCarrier gasTC sampleinjection port,slide typeUSB memory stickDisplayDilution waterASI-L autosamplerPrinterDataprocessorLAN (option)Dehumidifier/gaspretreatment unitTC combustiontubeNon-dispersiveinfrared detector (NDIR)TC furnace7

Software Features Intuitive Operabilityand a Wealth of FunctionsT O C - L CPH/CPN P C - C o n t r o l l e d M o d e lEnabling Simple, Intuitive OperationIcons and function namesshown on large buttonsUser-friendly display of the name,ID, and measurementresults for selected samples,all in specific columns・List of files used by type・Can be sorted by file name and date created・File details are displayed with tooltipOperationsare accessedby right-clickingon the tableInsert samples by dragging and dropping measurement conditions filesDrag the mouse over cells to batch-enter identical characterstrings, and sequential IDs and vial numbersClassification by type8User-friendly displayof instrument statususing text and em automatically enters sleep mode. It can be set to automatically Automatic changing of conditions and re-measurement ofout-of-range samplesrestart at a certain time.* PC software is included as standard with the standalone models. Adding a PCIf the sample peak exceeds the calibration curve range, measurement conditions,and communication cable allows the operator to use the software onsuch as dilution rate and injection volume, are automatically changed, and thestandalone models.measurement is repeated.11

Options for Configuring an AutomaticMeasurement SystemASI-L AutosamplerEven More Functionality and Convenience,Enabling Samples to Be Added During Continuous MeasurementFeatures Select from three vial types with different capacities to suit your application.Combination of vial capacity and number of vials・ 9 mL vials 93・ 24 mL vials 93・ 40 mL vials 68Two types of ASI-L units are available, one for 24 mL vials and the other for 9 mL and 40 mL vials. Optional magnetic stirrers agitate the sample in the vials to prevent the settling ofsuspended solids. Magnetic stirrers are installed at the measurement position andsubsequent measurement position to thoroughly agitate the samples prior tomeasurement.(Vials for 24mL and 40 mL are available. If 24 mL vials are used, vials No. 1 to No. 85 of the 93 totalvials can be stirred.)O C T- L 8 - P o r t S a m p l e rThe Bridge to Ultra-Simplified Automatic MeasurementFeatures Easy-to-use autosampler does not require special vials.Water sample can be measured directly in the collection bottles and thus do not need to be transferred tospecific size autosampler vials required with other systems. Up to 8 samples can be measured with a single OCT-L unit.Up to 16 samples can be measured by adding a second OCT-L. Commercially available stirrers can be used. (Stirrers are sold separately.) Samples can be added during continuous measurement.12

Wealth of Options Provides Greater FunctionalityT N M - L T N ( To t a l N i t r o g e n ) U n i tPerform Simultaneous TOC and TN MeasurementsFeatures 720 ºC catalytic thermal decomposition/chemiluminescence methods are adopted for TNmeasurement.There is no interference from metallic ions or bromine in sea water. Measurements over a wide range with a detection limit of 5 µg/L for TOC-LC*H to an upperlimit of 10,000 mg/L.(In the case of simultaneous TOC/TN measurement, TOC analysis using high-sensitivity catalysts isimpossible. TN measurement is not possible in combination with the SSM-5000A.)SSM-5000A Solid Sample Combustion UnitCapable of TOC Measurements in Solid SamplesFeatures Measurement of maximum 1 g samples with up to 30 mg carbon content reducesweighing errors, and errors due to uneven distribution of the sample carbon content.(The SSM-5000A cannot measure sea water samples and sea bottom sediment samples containingmuch salt.) Measurement of inorganic carbon (carbonate) in solid samples.(TN measurement is not available with the SSM-5000A.) Measurement of aqueous samples containing large quantities of suspendedsubstances.In addition to aqueous samples, carbon measurements canalso be performed on soil, sludge, sedimentation, and other Simply change the onscreen settings to switch between aqueous sample measurementwith the TOC-L, and solid sample measurement using the SSM-5000A.solid samples. By swabbing, the carbon in attached residuescan be measured for cleaning validation.【GMP Cleaning Validation Using the Swab Method】Swab samplingTransfer to sample boatTC measurementEasy wiperEasy wiperResidue evaluation using swab sampling with quartz microfiber filter paper and direct combustion carbon analysis(Please contact your local Shimadzu representative for further information.)13

Compatibility of Options and Special Accessories : Compatible, -: Not compatibleTypeOptionsSpecialAccessoriesNameTOC-L CSH/CPHTOC-L CSN/CPNAccessories for 9mL vial638-92327-41ASI-L*19 mL vial (100 pcs.)autosampler638-53096638-93199-58Accessories for 24mL via(for 24 mL vial)638-92325-41638-93200-5824 mL vial (100 pcs.)(for 9 mL /638-4146240 mL vial)24 mL vial septum (100 pcs.)038-00165-6124 mL vial cap (100 pcs.)638-20074-01Accessories for 40mL vial638-92326-4140 mL vial(with septum, 72 pcs.)038-00158-11OCT-L*1 8-port sampler638-93201-58 (one unit)638-93202-58 (two units)TNM-L TN unit638-91108-58SSM-5000A solid sample combustion unit638-93210 See page 12.Up to two OCT-L units can be connected. Only one can be connectedwhen the POC kit is used. See page 13. See page 13.Carrier gas purification kit638-41447-04ー Nitrogen carrier gas kit638-42054-02 Manual injection kit638-93149-03 ー Suspended sample kit638-41586 Suspended sample kit, with ASI parts638-93151-04External sparging kit638-77183-40External sparging kit, with ASI parts638-77183-41 ASI-L flow line parts are added to the suspended sample kit. Sparging can be performed with any sample container. Sparging can be performed inside ASI-L vials. ーThis kit enables the measurement of smaller volumes of samples.Example of sample consumption: Standard specifications: 8 mL/3measurements Using this kit: 5 mL/3 measurements.However,there are some performance limits such as maximum sensitivity rangeis about 0-1 mg/L, maximum measuring range decreases, ASI-L andexternal sparging kit need to measure NPOC automatically. ー ーB-type halogen scrubber638-52572-03 High-salt sample combustion tube kitFor TOC-L CPN/CSN: 638-93176-01For TOC-L CPH/CSH: 638-93176-02 Data can be output via the LAN board. Includes a 20 m carrier gas pipe.POC measurement kitFor TOC-L CPN/CSN: 638-42101-01For TOC-L CPH/CSH: 638-42101-02Cell switching valve set638-56239-41Magnetic stirrerFor 24 mL vial: 638-67099-41For 40 mL vial: 638-67100-41Kit for small sample volumes638-59328High Suspension KitsHigh Conc. TC638-42167-41High Conc. IC638-42167-42Low Conc. TC638-42167-43Low Conc. IC638-42167-44LAN board638-79070-41Air supply pipe set638-41204*1: Select either ASI-L or OCT-L. They cannot be used simultaneously.14ExplanationSee page 12.Vial sets do not include vials.Please purchase separately.Carbon dioxide, hydrocarbons and other carbon-containingcompounds are removed from compressed air and otherpressurized gases, so that they can be used as carrier gas.High-purity nitrogen gas (min. 1 ppm of each CO, CO 2 andHC) can be used as the carrier gas. When this option is used,the measurement range for both TC and IC expands from theconventional range (0 to 500 µg/L) to 0 to 100 mg/L. Whenusing TNM-L, this kit cannot be used.Samples can be injected manually using a micro syringe. Gassamples and aqueous samples can be injected.TC and CO 2 measurements in gas samples can be performed.This kit enables measurement of the volatile organic carbon (POC)driven from the sample during the sparging process at roomtemperature.This option for the SSM -50 0 0A enables high-sensitivit ymeasurement of solid samples.This option for the ASI-L enables agitation of 24 ml and 40 mlvial samples. (If 24 mL vials are used, vials No. 1 to No. 85 of the93 total vials can be stirred.)This kit changes the sample flow line diameter from 0.5 mm to0.8 mm, enabling the injection of larger suspended substancesinto the combustion tubes. (Parts for ASI-L are not included.)T he s e kit s enable m easurem ent of s ample s cont ainingsedimentary organic matter with good repeatability. Thereare kit for high concentration sample (injection volume 80 µL)and for low concentration sample (injection volume 150 µL). Itdoesn’t support IC measurements with TOC-L standard model.This kit effectively removes corrosive gases produced whenmeasuring samples containing salts, thereby easing NDIR celldegradation.When measuring samples containing salts, this kit extends thelifetime of combustion tubes and catalysts, reducing maintenancefrequency. It enables seawater measurement approx. 2,500 timesby injecting 40 µL. (It’s not a guaranteed value.)

Specifications TOC-L Series Total Organic Carbon AnalyzerHigh-Sensitivity ModelItemsTOC-L CPHModelStandard ModelTOC-L CSHTOC-L CPNTOC-L CSN680 C combustion catalytic oxidation – non-dispersive infrared detection (NDIR) methodMeasurement MethodPC-controlledOperation MethodStandalone *PC control availablePC-controlledStandalone *PC control availableTC, IC, TOC ( TC-IC), NPOC (TOC measurement via acidification and sparging) *Option: POC, TOC ( NPOC POC), TNMeasured ItemsApplicable SamplesAqueous (optional solid/gas samples)TC: 0 to 30,000 mg/LIC:0 to 35,000 mg/L(Option)TN: 0 to 10,000 mg/LPOC: 0 to 500 mg/LMeasurementRangeTC: 0 to 30,000 mg/LIC:0 to 3,000 mg/L(Option)TN: 0 to 10,000 mg/LPOC: 0 to 500 mg/LDetection LimitTC, IC: 4 µg/L, TN: 5 µg/LTC: 50 µg/L, IC: 4 µg/L, TN: 20 µg/LReproducibilityTC, IC, NPOC: CV 1.5 % max. or 4 µg/L max(Optional TN: CV 3.0 % max. or 5 µg/L max)TC, NPOC: CV 1.5 % max. or 50 µg/L max, IC: CV 1.5 % max. or 4 µg/L max(Optional TN: CV 3.0 % max. or 20 µg/L max)Measuring TimeTC: approx. 3 min, IC: approx. 3 min (Optional TN: approx. 4 min)TC: approx. 3 min, IC: approx. 4 min (Optional TN: approx. 4 min)Sample InjectionAutomatic sample injection using a syringe pump and slide type injection mechanismSample InjectionVolume10 to 2,000 µL variableTC: 10 to 150 µL variable, IC: 10 to 4,500 µL variableIC RemovalAutomatic addition of acid and spargingSample DilutionDilution rate of 2 to 50 (automatic sample dilution by syringe pump), dilution accuracy: 2 % max. (2 to 20 ), 5 % max. (21 to 50 )Display andOperationsOperated by PCOperation by color LCD screenand keyboard*Operation by PC is also possibleOperated by PCOperation by color LCD screenand keyboard*Operation by PC is also possibleExternal Memory(Standalone Type)—USB flash memory used—USB flash memory usedPrinter—Portable thermal printer andPC USB printer can be used—Portable thermal printer andPC USB printer can be used(Standalone Type)High-purity air (CO, CO 2, HC content: Each 1 ppm max., dew point: -50 C max.)Supply pressure: 200 10 kPa (Additional use of optional carrier gas regulator: 300 to 600 kPa)Optional use of nitrogen gas (not possible in the TN measurement). With the standard model, optional use of pressurized gas.Carrier Gas150 mL/min (230 to 250 mL/min during sparging)(Variable flow rate)Gas Consumption230 mL/min (A separate 100 mL/min is required forsparging with ASI-L. (variable flow rate))Power Supply100 to 240 V AC, 600 VA (Permitted range: 90 to 264 V AC)Applicable RegulationsCEAmbientTemperature Range5 to 35 CDimensionsW340 D660 H480 mm (Excluding protrusions. For details, see the External Dimensions Diagram.)WeightApprox. 35 kg ASI-L Autosampler TNM-L TN (Total Nitrogen) UnitSelect from three types:9 mL, 24 mL, 40 mLMeasurementMethodChemiluminescenceNumber of Vials9 mL: 93, 24 mL: 93, 40 mL: 68Measured ItemsTN (total nitrogen)Vial SeptumWith dedicated septum(excluding 9 mL vials)MeasurementRange0 to 10,000 mg/LVial TypesPossibleSample Sparging(The optional external spargingkit is required.)DimensionsW370 D540 H490 mm(excluding protrusions)WeightApprox. 14 kgDetection Limit5 µg/L (CPH, CSH)20 µg/L (CPN, CSN)ReproducibilityCV 3 % max.Measuring TimeApprox. 4 minAirOzone Source Gas(compressed air or housing air) SSM-5000A Solid Sample Combustion UnitCombustion catalytic oxidationTC OxidationMethod(TC furnace temperature: 900 C)IC ReactionMethodAcidification(IC furnace temperature: 200 C)Measured ItemsTC, IC, TOCMeasurementRangeTC: 0.1 to 30 mg carbonTC: (1 to 20 µg carbon inhigh-sensitivity measurement)IC: 0.1 to 20 mg carbonMaximumSample Amount1g(aqueous content: 0.5 g)Measuring TimeNormally 5 to 6 minutes500 mL/min OCT-L 8-Port SamplerNumber of OCT-LUnits ConnectedUp to 2 OCT-L unitsfor a single TOC-LVial TypesAny sample container can be usedNumber of Vials8 for a single OCT-L16 for dual OCT-LSample SpargingNo sparging with OCT-L; spargingis done in the TOC-L syringeDimensionsW245 D245 H440 mm(excluding protrusions)WeightApprox. 3.5 kgDimensionsW270 D240 H160 mm(excluding protrusions)WeightApprox. 6 kgCarrier GasPower Requirements99.9 % O 2 at 500 mL/minHigh-purity O2 gas is required forhigh-sensitivity measurement.100 to 127 or 220 to 240 V ACas ordered, 700 VADimensionsW450 D656 H290 mmWeightApprox. 30 kg15

TOC-LExternal Dimensions Diagrams TOC-L TNM-L OCT-L PC TOC-LTNM-L340480TOC-LPC441630480OCT-L660245Unit: mm34050 TOC-L SSM-5000A100Unit: mm TOC-L ASI-L nit: mmUnit: mmRelated Products ON-LINE TOC-V C S H Combustion Catalytic Oxidation/NDIR TOC-VW Wet Oxidation/NDIR Method・ Wet oxidation/NDIR TOC analyzer, offering truly impressive ultrapurewater measurements.・ TOC analyzer, featuring 680 ºC combustion catalytic oxidation/NDIR・ Designed with a focus on high sensitivity, oxidation performance, andlow blanks.Method Online Modelmethods and continuous online measurements.・ Enables automated, high-sensitivity monitoring of pure water and tapwater, with minimal maintenance. A pharmaceutical water controlprogram is also available.For Research Use Only. Not for use in diagnostic procedures.This publication may contain references to products that are not available in your country. Please contact us to check the availability of theseproducts in your country.Company names, products/service names and logos used in this publication are trademarks and trade names of Shimadzu Corporation, itssubsidiaries or its affiliates, whether or not they are used with trademark symbol “TM” or “ ”.Third-party trademarks and trade names may be used in this publication to refer to either the entities or their products/services, whether or notthey are used with trademark symbol “TM” or “ ”.Shimadzu disclaims any proprietary interest in trademarks and trade names other than its own.www.shimadzu.com/an/The contents of this publication are provided to you “as is” without warranty of any kind, and are subject to change without notice. Shimadzudoes not assume any responsibility or liability for any damage, whether direct or indirect, relating to the use of this publication. Shimadzu Corporation, 2018First Edition: January 2011, Printed in Japan 3655-06805-20AIK

Measurement method: TN measurement of Ammonium Sulfate Aqueous Solution, prepared nitrogen concentration 10 mg/L Measurement results: TN 9.91 mg/L (C.V. 0.30 %) Example of TOC Measurement of Nickel Plating Solution Analysis instrument: TOC-LCPH Measurement method: TOC measurement of

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