Nanomechanical Testing In Materials Research And .
ProgramNanomechanical TestinginMaterials Research and Development IVOctober 6-11, 2013Olhão (Algarve), PortugalConference Chair:Dr. Johann MichlerMechanics of Materials and Nanostructures Laboratory,EMPA - Materials Science & Technology, Thun, SwitzerlandEngineering Conferences International32 Broadway, Suite 314 - New York, NY 10004, USAPhone: 1 - 212 - 514 - 6760, Fax: 1 - 212 - 514 - 6030www.engconfintl.org – info@engconfintl.org
Real Marina Hotel & SpaAv. 5 de Outubro8700-307 OlhãoTel.: [ 351] 289 091 300Fax: [ 351] 289 091 301
Engineering Conferences International (ECI) is a not-for-profit global engineering conferencesprogram, originally established in 1962, that provides opportunities for the exploration ofproblems and issues of concern to engineers and scientists from many disciplines.ECI BOARD MEMBERSBarry C. Buckland, PresidentPeter GrayMichael KingRaymond McCabeDavid RobinsonWilliam SachsEugene SchaeferP. SomasundaranDeborah WileyChair of ECI Conferences Committee: William SachsECI Technical Liaison for this conference: Ram DaroliaECI Executive Director: Barbara K. HickernellECI Associate Director: Kevin M. Korpics Engineering Conferences International
Organizing CommitteeGeorge M. Pharr (University of Tennessee, Knoxville, Tennessee, USA)Dr. Nigel M. Jennett (National Physical Laboratory, United Kingdom)Dr. Rejin Raghavan (EMPA – Materials Science & Technology, Switzerland)Steering CommitteeGeorge Pharr (University of Tennessee, USA)Mathias Göken (University of Erlangen-Nurnberg, Germany)Gerhard Dehm (MPIE, Düsseldorf, Germany)
Conference SponsorsAgilentAlemnisCSM InstrumentsHelmut Fischer AGHysitron, Inc.Kleindiek Nanotechnik GmbHMichalexMicro Materials Ltd.Nanomechanics, Inc.SURFACE systems technologySynton-MDP Inc.
Sunday, October 6, 201316:00 – 18:30Check-in (Lobby Praias)18:30 – 19:30Opening Reception19:30 – 19:45WelcomeConference Chair: Johann MichlerECI Technical Liaison: Ram Darolia19:45 – 20:15Plenary:In situ TEM and small-scale mechanical testing: The perfect combination?Marc LegrosCEMES-CNRS, France20:30DinnerNOTES Audiotaping, videotaping and photography of presentations are strictly prohibited. Please do not smoke at any conference functions. Turn your mobile phones to vibrate or off during technical sessions. The ECI office will be located in the Executive Lounge. Be sure to check your contact information on the Participant List in this program and make any corrections toyour name/contact information online. A corrected copy will be sent to all participants after the conference. Speakers – Please leave at least 5 minutes for questions and discussion. Be available for discussion duringmeals and social periods
Monday, October 7, 201307:30 – 09:00Breakfast buffet09:00 – 13:20In-situ TestingChair: Rejin Raghavan, EMPA, Switzerland and Max-Planck-Institute for Iron Research,Germany09:00 – 09:30Invited: In situ mechanical testing in electron microscopes to study small scaledeformation mechanismsDaniel Kiener, University of Leoben, Austria09:30 – 09:50X-ray µLaue: A novel view on fatigue damage at the micron scaleChristoph Kirchlechner, Max-Planck-Institute for Iron Research, Germany09:50 – 10:10Flaw-driven failure in nanocrystalline Pt nanostructuresWendy Gu, California Institute of Technology, USA10:10 – 10:30Critical-temperature/ Peierls-stress dependent size effects in body centered cubicnanopillarsSeung Min Han, Korea Advanced Institute of Science and Technology, South Korea10:30 – 11:00Coffee break11:00 – 11:20In-situ squared: Multi property thin film measurements during strainingMegan Cordill, Erich Schmid Institute, Austria11:20 – 11:50Invited: Probing deformation phenomena at small length scalesGerhard Dehm, Max-Planck-Institut für Eisenforschung, Germany11:50 – 12:10Synchrotron-based in situ mechanical testing of nanocrystalline metals and alloysPatric A. Gruber, Karlsruhe Institute of Technology, Germany12:10 – 12:30Ex-situ and in-situ study of the plastic deformation of InSb micropillars undercoherent x-raysLudovic Thilly, University of Poitiers, France13:00 – 14:00Lunch14:00 – 16:00Free time /ad hoc sessions16:00 – 16:30Afternoon coffee and snacks
Monday, October 7, 2013 (continued)16:30 – 19:00In-situ / Small Scale TestingChair: Daniel Kiener, University of Leoben, Austria16:30 – 17:00Invited: Dislocation-nucleation mediated deformation in single crystal goldnanowiresCynthia A. Volkert, University of Göttingen, Germany17:00 – 17:20TEM and AFM study of the elementary deformation mechanisms induced bynanoindentation in the MAX phase Ti 3 AlC 2Christophe Tromas, Institut Pprime – University of Poitiers, France17:20 – 17:50Invited: In-situ Laue diffraction during micro-compression: slip in bcc metalsHelena Van Swygenhoven, Paul Scherrer Institute / EPFL, Switzerland17:50 – 18:10Deformation localization and strain hardening during micro shear experiments ongold in the scanning electron microscopeSteffen Brinckmann, Max Planck Institute for Iron Research, Germany18:10 – 18:30Using small scale testing to extract the impact of structural defects on plasticitymechanismsDavid Bahr, Purdue University, USA19:00 – 19:30Poster Session I: PreviewChair: George Pharr19:30 – 20:45Dinner20:45 – 23:30Poster Session I
Tuesday, October 8, 201307:30 – 09:00Breakfast buffet09:00 – 13:20Variable temperature testing and IndentationChair: Bill Clegg, University of Cambridge, UK09:00 – 09:30Invited: In situ micro-thermomechanical testing: A general tool for investigatingplasticityJeffrey Wheeler, EMPA - Materials Science & Technology, Switzerland09:30 – 09:50Strain-rate sensitivity in bcc-metals temperature and microstructural influencesVerena Maier, University of Leoben, Austria / FAU Erlangen-Nürnberg, Germany09:50 – 10:20Invited: High temperature mechanical behavior of nanoscale multilayersJon Molina, IMDEA Materials Institute, Spain10:20 – 10:50Invited: Nano and micro-mechanical testing of reactive metals in vacuumDavid Armstrong, University of Oxford, UK10:50 – 11:20Coffee break11:20 – 11:50Invited: Extracting elastic properties of coatings on stiff and compliant substratesby nanoindentationSteve Bull, Newcastle University, UK11:50 – 12:10Plasticity size effects: when is a micro-pillar like a nanoindentation?Andy Bushby, Queen Mary University of London, UK12:10 – 12:40Invited: Temperature and strain-rate dependent dislocation nucleation in PdnanowhiskersDan Gianola, University of Pennsylvania, USA12:40 – 13:00Critical appraisal of a procedure for extracting primary and secondary creepparameters from nanoindentation dataBill Clyne, University of Cambridge, UK13:00 – 13:20Orientation informed indentation of magnesium on different length scalesClaudio Zambaldi, Max-Planck-Institute for Iron Research, Germany13:30 – 14:00Lunch14:00 – 16:00Free time /ad hoc sessions16:00 – 16:30Afternoon coffee with snacks
Tuesday, October 8, 2013 (continued)16:30 – 20:10New Instrumentations and DevelopmentsChair: Johann Michler, EMPA, Switzerland16:30 – 16:50New Directions at Nanomechanics Inc.Warren Oliver, Nanomechanics, Inc., USA16:50 – 17:10Measuring Adhesion, Compression, and Tensile Forces in the SEMStephan Kleindiek, Kleindiek Nanotechnik GmbH, Germany17:10 – 17:30The right nanoindenter tip designSimon Hostettler, Synton-MDP LTD, Switzerland17:30 – 17:50Evaluation of temperature changes in the periphery of nanoindenter measurements- Stabilization measures and strategiesDennis Bedorf, Surface & Surface systems technology GmbH & Co. KG, Germany17:50 – 18:10Instrumentation for displacement controlled, cyclic, elevated temperature,nanomechanical testingJean-Marc Breguet, Alemnis GmbH / EMPA, Switzerland18:10 – 18:30Nanoindentation “Made in Germany” The Helmut Fischer GroupDr. Tanja Haas, Helmut Fischer GmbH, Germany18:30 – 18:50Recent developments on 1000 C indentation machineMichel Fajfrowski, Michalex, France18:50 – 19:10Vacuum nanomechanics – progress towards 1000 degrees CBen Beake, MicroMaterials Ltd., UK19:10 – 19:30Evolution of instrumentation for nano mechanical testing: Indentation and scratchtesters, new bioindenterPhilippe Kempe, CSM Instruments SA, Switzerland19:30 – 19:50Express test: Evaluation and application of a novel technique for rapid acquisitionand mapping of accurate mechanical propertiesHolger Pfaff, Agilent Technologies GmbH, Germany19:50 – 20:10Innovations for nanoindentation in challenging environmentsDouglas Stauffer, Hysitron, USAFree evening / Dinner on your own
Wednesday, October 9, 201307:30 – 09:00Breakfast buffet09:00 – 13:00Mechanics of plasticity and fractureChair: Mathias Göken, University Erlangen-Nürnberg, Germany09:00 – 09:30Invited: Fracture and fatigue testing at the nano-scaleOliver Kraft, Karlsruhe Institute of Technology, Germany09:30 – 09:50Understanding low temperature plasticity in brittle intermetallics - Insights fromnanomechanical testingSandra Korte, RWTH Aachen University / FAU Erlangen-Nürnberg, Germany09:50 – 10:20Invited: Deformation of complex crystalsBill Clegg, University of Cambridge, UK10:20 – 10:50Coffee break10:50 – 11:20Invited: A more unified view on size effects in plasticityErica Lilleodden, Helmholtz-Zentrum Geesthacht, Germany11:20 – 11:40Plasticity of silica at the micron-scale: from nanomechanical testing to multiscalemodelingGuillaume Kermouche, CNRS, France11:40 – 12:10Invited: Strength of small materials under vibrationsAlfonso Ngan, University of Hong Kong, P. R. China12:10 – 12:30Small scale plasticity: Insights into displacement jump velocitiesRobert Maass, University of Göttingen, Germany12:30 – 12:50Mechanical properties of FCC metallic nanowires: A comparative simulation studyof single-crystalline and fivefold-twinned structuresErik Bitzek, FAU Erlangen-Nürnberg, Germany12:50 – 13:10Crystal plasticity modeling of nanoindentation near a grain boundary in alphatitaniumDavid Mercier, Max-Planck-Institute for Iron Research, Germany13:10 – 18:30Boxed lunch and excursion18:45 – 19:15Poster Session II: PreviewChair: George Pharr19:15 – 20:30Dinner21:00 – 23:30Poster Session II and Social Hour
Thursday, October 10, 201307:30 – 09:00Breakfast buffet09:00 – 12:50Mechanics of Thin FilmsChair: David Bahr, Purdue University, USA09:00 – 09:30Invited: Mechanical and thermal stability of nanotwinned AlloysAndrea Hodge, University of Southern California, USA09:30 – 09:50From telephone cord buckles to branches the relation between adhesion, residualstresses and morphology in thin film instabilitiesEtienne Barthel, CNRS / Saint-Gobain UMR125, France09:50 – 10:20Invited: Micro-cantilever tests as tools to support the development of hightemperature materials and coatingsMathias Göken, FAU Erlangen-Nürnberg, Germany10:20 – 10:40A new method to investigate fracture toughness in thin ceramic filmsMarco Sebastiani, University of Rome "Roma TRE", Italy10:40 – 11:10Coffee break11:10 – 11:40Invited: In-situ fracture testing of graded Pt-Ni-Al bond coats in a stable clampedbeam geometryVikram Jayaram, Indian Institute of Science, India11:40 – 12:00A micro double cantilever beam method to measure the fracture toughness of hardcoatingsShiyu Liu, University of Cambridge, UK12:00 – 12:20The deformation and fracture mechanisms of thin freestanding gold films studiedby bulge testsBenoit Merle, FAU Erlangen-Nürnberg, Germany12:20 – 12:50Invited: New methods to obtained better data from indentations measurementsJean-Luc Loubet, CNRS, France13:00 – 14:00Lunch14:00 – 16:00Free time /ad hoc sessions16:00 – 16:30Afternoon coffee and snacks
Thursday, October 10, 2013 (continued)16:30 – 18:40Deformation mechanismsChair: Cynthia Volkert, University of Göttingen, Germany16:30 – 17:00Invited: Size effect or no size effect - that is the question?Ralph Spolenak, ETH, Switzerland17:00 – 17:20Study by AFM and EBSD of plastic deformation mechanisms induced bynanoindentation in a hardmetal binder-like cobalt allotJoan Josep Roa, CIEFMA-Polytechnic University of Catalunya, Spain17:20 – 17:50Invited: Plasticity in small dimensions and the influence of defect structure,boundaries and environmentChristian Motz, Saarland University, Germany17:50 – 18:20Invited: New indentation testing approaches for studying deformation mechanismin SX and nanocrystalline materialsKarsten Durst, University of Erlangen-Nürnberg, Germany18:20 – 19:00Short Break19:00 – 20:00Reception20:00 – 23:30Conference Banquet
Friday, October 11, 201307:30 – 09:00Breakfast buffet09:00 – 11:20Combinatorial synthesis, Analysis and Architectural design of materialsChair: Ralph Spolenak, ETH, Switzerland09:00 – 09:30Invited: Mechanics and physics of nano-solids: from strength and fracture tohierarchical design of architected materials through in-situ experimentsJulia Greer, California Institute of Technology, USA09:30 – 09:50Approaches to strengthen bulk metallic glassesOliver Franke, University of Southern California, USA09:50 – 10:20Invited: SEM-in situ testing of nanolaminatesWilliam Mook, Los Alamos National Laboratory, USA10:20 – 10:50Coffee break10:50 – 11:10Integrated in-situ experiments full field crystal plasticity simulations to analyzestress strain partitioning in multi-phase alloysCemal Cem Tasan, Max-Planck Institute for Iron Research, Germany11:10 – 11:30Time-dependent mechanical-electrical coupled behavior of single crystal ZnOnanorodsYong-Jae Kim, Hanyang University, Korea11:30 – 11:50Super-plastic flow of confined nanocrystalline CuRejin Raghavan, EMPA11:50 – 13:00General Discussion (Optional)13:00 – 14:30Lunch and Departure
Poster List1.Express test- evaluation and application of a novel technique for rapid acquisition andmapping of accurate mechanical propertiesHolger Pfaff, Agilent Technologies2.Mechanical properties of silicon oxide coatings deposited by plasma enhanced CVD andassessed by instrumented nanoindentationJon Arrikaberri, Asociación de la Industria de Navarra3.Fabrication and deformation of three-dimensional biomimetic eeramic nano-architectedmaterialsLucas R. Meza, California Institute of Technology4.Limitations of a common method for extraction of the creep stress exponent fromindentation dataJames Dean, Cambridge University5.Hardness of finely dispersed carbides in iron-based hard alloysAlexandra Yulinova, Chemnitz University of Technology6.New method for mechanical characterization of viscoelastic materials using a modifiedspherical nanoindenterPhilippe Kempe, CSM Instruments7.Hydrogen effect on dislocation nucleation in a ferritic alloy Fe-15Cr as observed pernanoindentationGuillaume Kermouche, Ecole Des Mines de Saint-Etienne8.Measuring the stress-strain curves of materials using repeated micro-impact testingG. Kermouche, Ecole Des Mines de Saint-Etienne9.A new method to measure the mechanical properties of very thin top layers bynanoindentationGaylord Guillonneau, Ecole Nationale d'Ingénieurs de Saint-Etienne10.Cast aluminium microwiresJérôme Krebs, Ecole Polytechnique Fédérale de Lausanne11.Combinatorial experimentation for nanomechanical characterization: Elevatedtemperature nanoindentation testing of composition gradientsGaurav Mohanty, EMPA12.In situ compression testing of miniaturized Cu samples with grain boundariesPeter J. Imrich, Erich Schmid Institute of Materials Science13.Alloy development of TI-based thin films for microstructural stability mechanicalproperties and microstructural analysisDiana Courty, ETH Zurich14.Size-dependent plasticity in ionic crystal systems: The influence of temperature,orientation and doping levelYu Zou, ETH Zurich
15.Pillar compression testing of low stacking fault energy FCC alloysMatthias Schamel, ETH Zurich16.Nanoindentation and deformation of γ-Mg17Al12 at high temperaturesHarshal Mathur, FAU Erlangen-Nürnberg17.Investigation of the temperature dependence of polymeric materials withnanoindentationTanja Haas, Helmut Fischer GmbH Institut für Elektronik und Messtechnik18.Long-term creep behaviour with the instrumented indentation testGottfried Bosch, Helmut Fischer GmbH Institut für Elektronik und Messtechnik19.Thermal expansion and steady state creep study in a TSV-structureJaroslav Lukes, Hysitron, Inc.20.In situ electromechanical study of nanowiresDouglas Stauffer, Hysitron, Inc.21.High-temporal-resolution analysis of nanoindentation-induced pop-ins in metalsDouglas Stauffer, Hysitron, Inc.22.Time and temperature dependent mechanical properties of materials at nanometerlength scaleDouglas Stauffer, Hysitron, Inc.23.Indenter dependent behavior of the Zr-based bulk metallic glassHu Huang, Jilin University24.In situ characterization of stress-coupled grain boundary migration in nanocrystallinemetalsPaul Rottmann, Johns Hopkins University25.Nanoindentation and compression testing of silver nanowires on substrateJae Hyun Kim, KAIST26.Methodology of stress measurement in copper and silicon around through-silicon via byusing nanoindentation and micro raman spectroscopy for advanced semiconductorinterconnectsJae Hyun Kim, KAIST27.Size and orientation dependent deformation behavior of a dual phase steelMoritz Wenk, Karlsruhe Institute of Technology28.Deformation behavior of copper thin films during nanoimprintingAnke Schachtsiek, Karlsruhe Institute of Technology29.Mechanical and electrical integrity of printed and evaporated silver films on compliantsubstratesThomas Haas, Karlsruhe Institute of Technology30.Mechanical testing of the interface between different metallization layers on annealedborophosphosilicate glassBernhard Völker, Kompetenzzentrum Automobil- und Industrie-Elektronik GmbH
31.Influence of microstructure on thermo-mechanical fatigue of Cu films on substratesWalther Heinz, Kompetenzzentrum Automobil- und Industrie-Elektronik GmbH32.Elastic modulus mapping of multilayered bouligand chitin structureIgor Zlotnikov, Max Planck Institute of Colloids and Interfaces33.Nanomechanical characterization of the prismatic layer in the mollusc shell pinnanobilisBernd Bayerlein, Max Planck Institute of Colloids and Interfaces34.Dislocation emission from short penny-shaped cracks: A study using a multiscalemodel of atomistic and dislocation dynamicsSteffen Brinckmann, Max-Planck-Institut für Eisenforschung GmbH35.The mechanical and adhesion behavior of a Cr interlayer between Cu and polyimideVera M. Marx, Max-Planck-Institut für Eisenforschung GmbH36.Combining micromechanics with microstructural evolution in lead-free solderBastian Philippi, Max-Planck-Institut für Eisenforschung GmbH & Materials Center LeobenGmbH37.The influence of humidity and temperature on the time-dependent response ofviscoelastic materials during nanoindentationBen D. Beake, Micro Materials Ltd38.Durability under severe mechanical contact: Predicting performance with nano-impacttestingBen D. Beake, Micro Materials Ltd39.In situ AFM and SEM investigation of Cu single crystals during microbending testsJosef Kreith, Montanuniversität Leoben40.Improving the accuracy and precision of nanoindentation resultsWarren Oliver, Nanomechanics Inc.41.Nanoindentation assisted acoustic measurementsAntanas Daugela, Nanometronix LLC42.Dynamic mechanical properties and long-term deformation behaviour of viscousmaterials (MeProVisc)Xiaodong Hou, National Physical Laboratory43.Probing the interaction of plasticity size effects with dislocation mobility and stackingfault energyNigel Jennett, National Physical Laboratory44.Thermal design and time-dependent dimensional drift behaviour of sensors, materialsand structures (T3D)Xiaodong Hou, National Physical Laboratory45.Extracting mechanical properties of porous coatings using nanoindentation techniquesNoushin Moharrami, Newcastle University46.Steels revisited by nanomechanical testingBjørn Rune Sørås Rogne, Norwegian University of Science and Technology
47.A study of the micro-cantilever size effect for single slip in alpha zirconiumJicheng Gong, Oxford University48.Plasticity in W6%Re revealed by in situ Laue diffractionAinara Irastorza-Landa, Paul Scherrer Institute (PSI) - Éc
11:50 – 12:10 Synchrotron-based in situ mechanical testing of nanocrystalline metals and alloys Patric A. Gruber, Karlsruhe Institute of Technology, Germany 12:10 – 12:30 Ex-situ and in-situ study of the plastic deformation of InSb micropillars under
with the atomic force microscope: Methods, theory and applications Ricardo Garcia, Instiuto Ciencia de Materiales de Madrid, CSIC R. Garcia, Chem. Soc. Rev. 49, 5850-5884 (2020) Introduction Classification Nanomechanical methods Theory of nanomechanical AFM Force-distance curve methods FV family Torsional harmonics Parametric methods Bimodal AFM
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