Thermo Scientific Orion AQUAfast Powder And Tablet Reagent .
Thermo ScientificOrion AQUAfast Powder andTablet Reagent ChemistryUser Guidefor use with AquaMate 7000 Vis andAquaMate 8000 UV-Vis Spectrophotometers
2012 Thermo Fisher Scientific Inc. All rights reserved. All trademarks are the property of Thermo Fisher Scientific Inc.and its subsidiaries.
Table of ContentsChapter 1 Overview . 1Table 1: Orion AQUAfast Power and Tablet Reagent Chemistries . 2Chapter 2 Reagent Chemistry Instructions . 4Recommendations for Avoiding Measurement Errors . 4Loading and Running a Water Analysis Method on the Spectrophotometer. 5Loading a Test Method from the USB Stick to the AquaMate Instrument . 5Running a Test Method from the USB Stick. 8Running a Test Method from the AquaMate Instrument Library. 8Running a Test Method from the AquaMate SmartStart Menu . 8Using the One Point Adjustment Calibration Feature . 9Using the Reverse Color Feature . 10AC2002 Alkalinity-M (Alkalinity to pH 4.3), Acid/Indicator Method, Tablet Test Procedure . 11AC3002P Alkalinity-P (Alkalinity to pH 8.2), Acid/Indicator Method, Tablet Test Procedure . 12AC2027 Aluminum, Eriochrome Cyanine R Method, Tablet Test Procedure . 13AC4P27 Aluminum, Eriochrome Cyanine R Method, Powder & Liquid Test Procedure . 14AC2012 Ammonia as Nitrogen (N), Indophenole/Phenate Method, Tablet Test Procedure . 15AC4P12 Ammonia as Nitrogen (N), Salicylate Method, Powder Test Procedure . 16ACR011 Ammonia as Nitrogen (N), HR, Salicylate Method, Reaction Tube Test Procedure . 17ACR012 Ammonia as Nitrogen (N), LR, Salicylate Method, Reaction Tube Test Procedure. 18AC2035 Bromine, DPD Method, Tablet Test Procedure . 19AC2017 Chloride, Silver Nitrate/Turbidity Method, Tablet Test Procedure . 20AC2070 Chlorine, Free & Total, DPD Method, Tablet Test Procedure . 21AC2071 Chlorine, Free, DPD Method, Tablet Test Procedure . 23AC2072 Chlorine, Total, DPD Method, Tablet Test Procedure . 25AC3072 Chlorine, Total, High Range, KI / Acid Method, Tablet Test Procedure. 27AC4P71 Chlorine, Free, DPD Method, Powder Test Procedure . 28AC4P72 Chlorine, Total, DPD Method, Powder Test Procedure . 29AC2099 Chlorine Dioxide, DPD Method, Tablet Test Procedure . 30CODL00 COD, Low Range, Dichromate Reactor Digestion Method, Digestion Tube Test Procedure . 32CODH00 COD, Mid Range, Dichromate Reactor Digestion Method, Digestion Tube Test Procedure . 34CODHP0 COD, High Range, Dichromate Reactor Digestion Method, Digestion Tube Test Procedure . 35AC2029 Copper, Free & Total, Biquinoline Method, Tablet Test Procedure . 36AC2065 Copper, Zincon Method, Tablet Test Procedure . 37AC4P29 Copper, Free, Bicinchoninate Method, Powder Test Procedure. 38AC2098 Cyanuric Acid, Melamine Method, Tablet Test Procedure. 39
AC2009 Fluoride, SPADNS Kit Method, Liquid Test Procedure. 40AC3032T Hardness, Total, Low Range, Metallphthalein Method, Tablet Test Procedure . 42AC3032T Hardness, Total, High Range, Metallphthalein Method, Tablet Test Procedure. 43AC2030 Hydrazine, Dimethylamino-benzaldehyde Method, Powder Test Procedure. 44Iron Digestion Method . 45AC2078 Iron, Low Range, III, Soluble, TPTZ Method, Tablet Test Procedure . 46AC4P78 Iron, II & III, Soluble, 1,10-Phenanthroline Method, Powder Test Procedure . 47AC4P79 Iron, Total, TPTZ Method, Powder Test Procedure . 48AC2055 Manganese, Formaldoxime Method, Tablet Test Procedure. 49AC4P54 Manganese, Low Range, PAN Method, Powder & Liquid Test Procedure . 50AC4P55 Manganese, High Range, Periodate Oxidation Method, Powder Test Procedure . 51AC4P42 Molybdate / Molybdenum, Mercaptoacetic Acid Method, Powder Test Procedure . 52ACR007 Nitrate as Nitrogen (N), Chromotropic Acid Method, Reaction Tube Test Procedure . 53AC2046 Nitrite as Nitrogen (N), Diazotization (Azo) Method, Tablet Test Procedure . 54AC4P46 Nitrite as Nitrogen (N), Low Range, Diazotization (Azo) Method, Powder Test Procedure . 55ACD004 Nitrogen, Total, Low Range, Persulfate Digestion Method, Digestion Tube Test Procedure . 56ACD007 Nitrogen, Total, High Range, Persulfate Digestion Method, Digestion Tube Test Procedure . 58AC2048 Ozone, Indigo Blue, Tablet Test Procedure . 60AC2001 pH, Phenol Red Method, Tablet Test Procedure . 62AC3001 pH, Phenol Red Method, Liquid Test Procedure . 63AC2095 Phosphate, Ortho, Low Range, Phosphomolybdic Acid/Ascorbic acid Method, Tablet TestProcedure . 64AC2096 Phosphate, Ortho, High Range, Vanadomolybdate Method, Tablet Test Procedure . 65AC4P95 Phosphate, Ortho, Ascorbic Acid Method, Powder Test Procedure . 66ACD095 Phosphate as Phosphorous (P), Total, Persulfate Digestion/Ascorbic Acid Method, DigestionTube Test Procedure . 67ACD095AH Phosphate as Phosphorous (P), Acid Hydrolyzable, Acid Digestion/Ascorbic Acid Method,Digestion Tube Test Procedure . 69ACR095 Phosphate, Ortho, Ascorbic Acid Method, Reaction Tube Test Procedure . 71AC2060 Silica, Silicomolybdate Method, Tablet Test Procedure . 72AC2061 Silica, Silicomolybdate Method with Phosphate Removal, Tablet Test Procedure . 73AC4P60 Silica, High Range, Silicomolybdate Method, Powder Test Procedure . 74AC4P82 Sulfate, Barium Sulfate/Turbidity Method, Powder Test Procedure . 76AC2016 Sulfide, Methylene Blue Method, Tablet Test Procedure . 77AC2065 Zinc, Zincon Method, Tablet Test Procedure. 78
Chapter 1 OverviewThermo Scientific Orion AquaMate 8000 UV-Vis and AquaMate 7000 Vis spectrophotometers includea USB memory stick that contains over 260 preprogrammed methods for use with Orion AQUAfast,Merck and CHEMetrics reagent chemistries. Preprogrammed methods provide values for the testparameters required to run specific reagent chemistries on the instrument, including wavelength, cellpath length, concentration factors/curves and measurement unit. All preprogrammed methods arestored on the USB memory stick, so operators can select and load only the methods needed for theirapplications. Up to 90 methods can be stored on the AquaMate spectrophotometer and storedmethods can be added or removed as needed. AquaMate spectrophotometers allow a one pointadjustment on any preprogrammed method using a known standard to correct for variations in batchto batch reagent chemistries. Operators can also modify preprogrammed methods or create theirown custom methods, so additional parameters and test methods can be added at any time.The following instructions are for using Orion AQUAfast reagent chemistries with the AquaMatespectrophotometer. Preprogrammed methods use a specific vial size (path length) in the formula, andthe vial size specified in these instructions must be used for accurate analysis. The majority ofAQUAfast reagent methods use a 24mm round vial, Cat. No. AC2V24. Other vial sizes are noted in theindividual reagent chemistry instructions.Use the information in the following table to identify method names on the USB memory stick andthe test parameters associated with each method. This information is also included in the ThermoScientific AquaMate Master Methods List available on the user guide CD or on our website atwww.thermoscientific.com/water.Page 1
Table 1: Orion AQUAfast Power and Tablet Reagent ChemistriesParameterReagentPart C2002Alkalinity-M, Acid/Indicator MethodTabletAlkalinityAC3002PAC3002PAlkalinity-P, Acid/Indicator MethodTabletAluminumAC2027AC2027Aluminum, Eriochrome Cyanine R MethodTabletAluminumAC4P27AC4P27Aluminum, Eriochrome Cyanine R MethodPowder,LiquidAmmoniaAC2012AC2012Ammonia as Nitrogen (N), Ammonia as Nitrogen (N), Salicylate MethodPowderAmmoniaACR011ACR011Ammonia as Nitrogen (N), High Range, onia as Nitrogen (N), Low Range, romine, DPD MethodTabletChlorideAC2017AC2017Chloride, Silver Nitrate/Turbidity MethodTabletChlorineAC2070AC207024Chlorine, Free & Total, DPD MethodTabletChlorineAC2071AC207124Chlorine, Free, DPD MethodTabletChlorineAC2072AC207224Chlorine, Total, DPD MethodTabletChlorineAC3072AC3072Chlorine, Total, High Range, KI / Acid MethodTabletChlorineAC4P71AC4P71Chlorine, Free, DPD MethodPowderChlorineAC4P72AC4P72Chlorine, Total, DPD MethodPowderChlorineDioxideAC2099AC209924Chlorine Dioxide, DPD MethodTabletCODCODL00CODL00COD, Low Range, Dichromate Reactor DigestionMethodDigestionTubeCODCODH00CODH00COD, Mid Range, Dichromate Reactor DigestionMethodDigestionTubeCODCODHP0CODHP0COD, High Range, Dichromate Reactor pper, Free & Total, Biquinoline MethodTabletCopperAC2065AC2065Copper, Zincon MethodTabletCopperAC4P29AC4P29Copper, Free, Bicinchoninate MethodPowderCyanuric Acid AC2098AC2098Cyanuric Acid, Melamine MethodTabletFluorideAC2009AC2009Fluoride, SPADNS Kit MethodLiquidHardnessAC3032TAC3032TLHardness, Total, Low Range, Hardness, Total, High Range, MetallphthaleinMethodTabletPage 2
HydrazineAC2030AC2030Hydrazine, Dimethylamino-benzaldehyde MethodPowderIronAC2078AC207824Iron, Low Range, III, Soluble, TPTZ MethodTabletIronAC4P78AC4P78Iron, II & III, Soluble, 1,10-Phenanthroline MethodPowderIronAC4P79AC4P79Iron, Total, TPTZ MethodPowderManganeseAC2055AC2055Manganese, Formaldoxime MethodTabletManganeseAC4P54AC4P54Manganese, Low Range, PAN MethodPowder,LiquidManganeseAC4P55AC4P55Manganese, High Range, Periodate OxidationMethodPowderMolybdate /AC4P42MolybdenumAC4P42Molybdate / Molybdenum, Mercaptoacetic AcidMethodPowderNitrateACR007ACR007Nitrate as Nitrogen (N), Chromotropic Acid MethodReactionTubeNitriteAC2046AC2046Nitrite as Nitrogen (N), Diazotization (Azo) Method TabletNitriteAC4P46AC4P46Nitrite as Nitrogen (N), Low Range, Diazotization(Azo) MethodPowderNitrogen,TotalACD004ACD004Nitrogen, Total, Low Range, Persulfate D007Nitrogen, Total, High Range, Persulfate ne, Indigo Blue MethodTabletpHAC2001AC2001pH, Phenol Red MethodTabletpHAC3001AC3001pH, Phenol Red MethodLiquidPhosphateAC2095AC2095Phosphate, Low Range, PhosphomolybdicAcid/Ascorbic Acid MethodTabletPhosphateAC2096AC2096Phosphate, High Range, Vanadomolybdate Method TabletPhosphateAC4P95AC4P95Phosphate, Ortho, Ascorbic Acid MethodPowderPhosphateACD095ACD095Phosphate as Phosphorous (P), Total, PersulfateDigestion/Ascorbic Acid MethodDigestionTubePhosphateACD095AH ACD095AHPhosphate as Phosphorous (P), Acid Hydrolyzable,Acid Digestion/Ascorbic Acid MethodDigestionTubePhosphateACR095ACR095Phosphate, Ortho, Ascorbic Acid MethodReactionTubeSilicaAC2060AC2060Silica, Silicomolybdate MethodTabletSilicaAC2061AC2061Silica, Silicomolybdate Method with PhosphateRemovalTabletSilicaAC4P60AC4P60Silica, High Range, Silicomolybdate MethodPowderSulfateAC4P82AC4P82Sulfate, Barium Sulfate/Turbidity MethodPowderSulfideAC2016AC2016Sulfide, Methylene Blue MethodTabletZincAC2065AC2065Zinc, Zincon MethodTabletPage 3
Chapter 2 Reagent Chemistry InstructionsThe measurement ranges specified in the following test procedures are provided by the chemistrymanufacturer and are based on standard solutions measured under ideal conditions. These rangesmay vary due to the type of sample being measured, since various interferences can have a majorinfluence on the accuracy of the method. Due to the fact that each sample is different, the only wayto check the tolerance (precision) is the Standard Additions Method. According to this method, firstthe original sample is tested. Then further samples (2 to 4) are taken and small amounts of a standardsolution are added, and further results are obtained. The amounts added range from approximatelyhalf, up to double the amount present in the sample itself. These supplementary results make itpossible to estimate the actual concentration of the original sample by comparison.Test methods and ranges are subject to change without notice. For a list of the most up-to-date testmethods, visit www.thermoscientific.com/water.Recommendations for Avoiding Measurement Errors Thoroughly clean vials, caps and stir rods after each analysis in order to prevent carry-overerrors. Even minute reagent residues lead to incorrect measurements. Ensure that the outer walls of the vials are dry and clean before performing the analysis.Fingerprints or water droplets on the light entry surfaces of the vials lead to incorrectmeasurements. Blank and measurement procedures should be performed using the same vial wheneverpossible, since different vials can possess slightly different tolerances. Always take all readings with capped vials. Bubbles on the inside walls of the vial can lead to incorrect measurements. To prevent this, capthe vial and remove the bubbles by swirling the vial before performing the test. Always add the reagent to the sample straight from the foil. The reagent should never touchfingers or hands. Major temperature differentials between the instrument and environment can lead to incorrectmeasurements - i.e. due to the formation of condensate in the area of the lens or on the vial.Specified tolerances at T 20 C. For the best results, use a pipette to measure and add samples to vials or beakers.Page 4
Loading and Running a Water Analysis Method on the SpectrophotometerThe USB memory stick included with the AquaMate spectrophotometers contains over 260preprogrammed methods for use with Orion AQUAfast, Merck and CHEMetrics reagent chemistries.Methods can be accessed directly from the USB memory stick when connected to the AquaMatespectrophotometer or up to 90 methods can be stored on the instrument for quick and easy access.The USB memory stick contains four folders: Thermo, Orion, Merck and CHEMetrics. The Thermofolder is empty and all methods to be loaded on the AquaMate spectrophotometer need to be copiedto the Thermo folder. The Orion, Merck and CHEMetrics folders contain preprogrammed methodsspecific to that manufacturer. Information for methods in the Orion folder can be found in this user guide and the ThermoScientific Orion AquaMate Master Methods List document. Information for methods in the Merck and CHEMetrics folders can be found in the ThermoScientific Orion AquaMate Master Methods List document and on the manufacturer’swebsite.Recommendation: A copy of the methods on the USB memory stick should be saved to a computer orother data source in case the USB memory stick is accidentally deleted or otherwise corrupted.Loading a Test Method from the USB Stick to the AquaMate Instrument1. Access the USB memory stick using a computer.2. Copy the desired test method(s) from the Orion, Merck and/or CHEMetrics folders to theThermo folder.3. Remove the USB memory stick from the computer and insert it into the USB port on the frontof the AquaMate spectrophotometer.4. When the AquaMate spectrophotometer is first powered on, it will display the initialmeasurement screen. Press the Test key to access the test types.Page 5
5. Press the / keys to highlight Water Analysis and press the Enter key.6. Press the Stored Tests function key.7. Press the / keys to highlight Load test from USB drive and press the Enter key.8. Press the / keys to highlight the test method to be loaded and press the Load Testfunction key.9. Press the Save Test function key.Page 6
10. Press the / keys to highlight Save as an internal test and press the Enter key.11. Press the Accept Name function key.12. Press the / keys to highlight Include as a SmartStart test or Do not include as aSmartStart test and press the Enter key.13. Press the Run Test function key to begin using the test method. Refer to the specific reagentchemistry section for detailed instructions.Page 7
Running a Test Method from the USB Stick1. Make sure the test method to be run is in the Thermo folder on the USB stick and the USBstick is connected to the USB port on the front of the AquaMate spectrophotometer.2. From the initial measurement screen, press the Test key to access the test types.3. Press the / keys to highlight Water Analysis and press the Enter key.4. Press the Stored Tests function key.5. Press the / keys to highlight Load test from USB drive and press the Enter key.6. Press the / keys to highlight the appropriate test method and press the Load Testfunction key.7. Press the Run Test function key.Running a Test Method from the AquaMate Instrument Library1. From the initial measurement screen, press the Test key to access the test types.2. Press the / keys to highlight Water Analysis and press the Enter key.3. Press the Stored Tests function key.4. Press the / keys to highlight Load internal test and press the Enter key.5. Press the / keys to highlight the appropriate test method and press the Load Testfun
Thermo Scientific Orion AquaMate 8000 UV-Vis and AquaMate 7000 Vis spectrophotometers include a USB memory stick that contains over 260 preprogrammed methods for use with Orion AQUAfast, Merck and CHEMetrics reagent chemistries. Preprogrammed methods provide values for the test . Thermo Fisher Scientific .
tion (Thermo Orion 12.9 mS Conductivity Standard, Orion 011006), 0.01 molar KCl (Thermo Orion 1413 S Conductivity Standard, Orion 011007) or entry of the temperature-compensated conductivity of another known calibration solution. To protect the batteries, the meter switches off automati-cally when not operated for a longer time than specified.
Preface Safety and Special Notices ii Thermo Scientific BindIt Software for KingFisher Instruments User Manual Thermo Scientific Thermo Scientific KingFisher Presto User Manual (Cat. no. N17413) Thermo Scientific KingFisher 96 User Manual (Cat. no. 15018890) The Thermo Scientific BindIt Software user manual can be found in PDF format in the
PULSE ARC / MICRO TIG WELDERS Orion 200i Welder Orion 200 i Welding Power Supply, (welder, swing arm, microscope and all acc. come in one box) Orion 250s Arm Orion 250s Micro Pulse Arc Welder with Free-Floating Microscope Package (Orion Arm) (2 boxes) Orion 250s ADL Orion 250s Micro Pulse A
Thermo ScientificThermo Scientific Orion ROSS Ultra, ROSS Ultra Triode and ROSS pH Electrodes 9 and water saturated with KCl. The ratio of methanol to water should be similar to the sample composition. For tips on measuring pH in non-aqueous samples, see Thermo Scientific Water Analysis Instruments Application Note 007.
Thermo ScientificTM Orion AQ3010 便携式浊度仪 Thermo ScientificTM Orion AQ3140 便携式 COD 测量仪 �䰳謋餑檯櫁 崬鎬胔 Orion COD㝵緒䰳獤㵸騩衊0-15000mg/L 僇圀婓栞蟭䰳斦紛讈穢 4饛7徠胾燪詭胾䰳楅傰崬㮅銁妭紛 17嚖枙悷5000瀐獤㵸 IP67䇝憠譀鈖
Thermo Scientific Orion Star and Star Plus Meter User Guide EN-1 Chapter I Introduction Congratulations! You have selected an industry-leading Thermo Scientific Orion Star or Star Plus series meter that is designed for electrochemistry measurements in the field or in the laboratory .
5 Our Thermo Scientific Orion Versa Star Pro and Thermo Scientific Orion Star A series benchtop meters are designed to address a variety of measurement requirements for dependable performance. Identify the best match based on your required features, performance specifications and budget.
Alison Sutherland 579 Alison Sutherland 1030 Alison Will 1084 Alison Haskins 1376 Alison Butt 1695 Alison Haskins 1750 Alison Haskins 1909 Alison Marr 2216 Alison Leiper 2422 Alistair McLeod 1425 Allan Diack 1011 Allan Holliday 1602 Allan Maclachlan 2010 Allan Maclachlan 2064 Allan PRYOR 2161 Alys Crompton 1770 Amanda Warren 120 Amanda Jones 387 Amanda Slack 729 Amanda Slack 1552 Amanda .
