Thermo Scientific Orion AquaMate - Cloudinary

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User ManualThermo ScientificOrion AquaMateUV-Vis and Vis Spectrophotometers269-289800 Revision C July 2015

Table of ContentsChapter 1 . 8Spectrophotometer Introduction . 8Spectrophotometer Overview . 8Packing List . 9Orion AquaMate User Documentation CD . 10Intended Use . 10Safety and Special Notices . 11Chapter 2 . 12Spectrophotometer Basics . 12Spectrophotometer Components . 12Instrument Connections . 13Instrument Keypad . 13Vial Holder Carousels . 15Selecting and Positioning Vials and Cuvettes . 16Changing the Vial Holder Carousel . 17Sample Positioner Setting for the Vial Holder Carousel . 18Chapter 3 . 20Orion AquaMate Instrument Setup. 20Entering Parameter Values. 20Setting Utility Menu Options . 22Printer Setting . 22Date/Time Setup Setting . 24Standby Setting . 25Baseline Expiration Setting . 25Beeper Setting . 26Screen Contrast Setting . 26Calculator Function . 26Managing Stored Tests. 27Naming and Saving a Test . 27Loading Saved Test Files . 29Locking/Unlocking Tests using the Password . 30Deleting a Test . 30Using the SmartStart Test Feature. 30Chapter 4 . 32Water Analysis Test Menu . 32Preprogrammed Methods . 32Loading and Running a Water Analysis Method on the AquaMate Instrument . 33Loading Test Methods from USB Stick to AquaMate Instrument . 34Running a Test Method . 37Running a Water Analysis Test Method . 38Using the One Point Adjustment Feature . 40Using the Reverse Color Feature . 42Creating or Modifying a Test Method . 44How to Define the Test Method Parameters . 44How to Modify the Test Method Parameters . 45

Chapter 5 . 46Orion AQUAfast Reagent Chemistry Instructions for Orion AquaMate . 46Orion AQUAfast Colorimetric Reagents Compatible with Orion AquaMate Instruments . 46Orion AQUAfast Reagent Instructions . 48Recommendations for Avoiding Measurement Errors . 48AC2002 Alkalinity-M (Alkalinity to pH 4.3) Tablet Test . 49AC3002P Alkalinity-P (Alkalinity to pH 8.2) Tablet Test . 50AC2027 Aluminum Tablet Test . 51AC4P27 Aluminum Powder Pack & Liquid Test . 52AC2012 Ammonia Tablet Test . 53AC4P12 Ammonia Powder Pack Test. 54ACR012 Ammonia Low Range Reaction Tube Test . 55ACR011 Ammonia High Range Reaction Tube Test . 56AC2035 Bromine Tablet Test . 57AC2017 Chloride Tablet Test . 59AC2070 Chlorine (Free & Total) Tablet Test . 60AC2071 Chlorine (Free) Tablet Test . 62AC2072 Chlorine (Total) Tablet Test. 64AC4P71 Chlorine (Free) Powder Pack Test . 66AC4P72 Chlorine (Total) Powder Pack Test . 67AC3072 Chlorine (Total) High Range Tablet Test . 68AC2099 Chlorine Dioxide Tablet Test . 69CODL00 COD Low Range Digestion Tube Test . 71CODH00 COD Mid Range Digestion Tube Test . 73CODHP0 COD High Range Digestion Tube Test . 74AC2029 Copper (Free & Total) Tablet Test . 75AC4P29 Copper (Free) Powder Pack Test . 76AC2098 Cyanuric Acid Tablet Test . 77AC2009 Fluoride SPADNS Liquid Test . 78AC3032T Hardness (Total) Tablet Test . 80AC2030 Hydrazine Powder Test . 81AC2078 Iron (II & III) Tablet Test . 82AC4P78 Iron (Ferro) Powder Pack Test. 83AC4P79 Iron (Total) Powder Pack Test . 84AC2055 Manganese Tablet Test. 85AC4P54 Manganese Low Range Powder Pack & Liquid Test . 86AC4P55 Manganese High Range Powder Pack Test . 87AC4P42 Molybdate Powder Pack Test . 88ACR007 Nitrate Reaction Tube Test . 89AC2046 Nitrite Tablet Test . 90AC4P46 Nitrite Powder Pack Test . 91ACD004 Nitrogen (Total) Low Range Digestion Tube Test. 92ACD007 Nitrogen (Total) High Range Digestion Tube Test . 94AC3048 Ozone Tablet Test . 96AC2001 pH Tablet Test . 98AC3001 pH Liquid Test . 99AC2095-WA Phosphate (Ortho) Low Range Tablet Test . 100AC2096 Phosphate (Ortho) High Range Tablet Test . 101AC4P95 Phosphate (Ortho) Powder Pack Test . 102ACR095 Phosphate (Ortho) Reaction Tube Test . 103

ACD095 Phosphate (Total) Digestion Tube Test . 104ACD095AH Phosphate (Acid Hydrolysable) Digestion Tube Test . 106AC2060 Silica Tablet Test . 108AC2061 Silica with Phosphate Removal Tablet Test . 109AC4P60 Silica Powder Pack Test . 110AC4P82 Sulfate Powder Pack Test. 111AC2016 Sulfide Tablet Test . 112AC2065 Zinc Tablet Test. 113Color Measurement from Application Log #131 . 114UVA and UV254 Measurements from Application Log #137. 118Chapter 6 . 122Standard Curve Test Menu . 122Concentration Measurements using the Standard Curve Application (Custom Method) . 122Setting the Parameters for a Standard Curve . 123Measuring Standards for a Standard Curve . 124Measuring Samples using a Standard Curve . 126Editing a Standard Curve . 129Selecting a Different Curve Fit for a Standard Curve . 130Recalling an Existing Standard Curve Method . 131Chapter 7 . 132Wavelength Scanning Test Menu . 132Setting the Parameters for a Scan . 133Collecting a Baseline Scan and Scanning a Sample. 134Viewing and Manipulating Scanned Data. 136Recalling an Existing Scanning Method . 141Chapter 8 . 142Absorbance, % Transmittance and Concentration Measurements . 142Absorbance & % Transmittance Measurements . 142Using the Basic A-%T-C Test Method. 142Using the Advanced A-%T-C Test Method . 144Concentration Measurements . 147Using the Basic A-%T-C Test Method. 147Using the Advanced A-%T-C Test Method . 150Multiwavelength . 154Absorbance Ratio . 157Absorbance Difference . 1593-Point Net . 161Kinetics . 163Chapter 9 . 168Performance Verification . 168Performance Verification Tests . 168Accessing the Performance Verification Tests . 169Troubleshooting Checklist . 169Wavelength Accuracy – Internal . 170Wavelength Accuracy – Standards . 171Photometric Accuracy . 173Noise Measurement. 175Stray Light. 176

Chapter 10 . 178Maintenance . 178Routine Care. 179Cleaning and Maintaining Vials and Cuvettes . 179Cleaning the Windows of the Sample Compartment . 181Changing the Fuse . 182Replacing the Tungsten Lamp . 184Chapter 11 . 186Customer Services . 186Technical Support . 186External Device Interfacing and Data Transfer . 187AquaMate Spectrophotometer Setup for Computer Interfacing . 187USB Computer Cable Interfacing and USB Driver Installation . 188Example Data Collection Program . 191AquaMate Spectrophotometer Setup for Printer Interfacing. 195USB Printer Cable Interfacing and Printing Data. 196Instrument Specifications. 197Ordering Information . 199Appendix A. 202General Instrument Information . 202Parameters . 202Concentration Units . 207Calculations for Software . 209

1CHAPTER 1Spectrophotometer IntroductionSpectrophotometer OverviewThermo Scientific Orion Aqu

Thermo Scientific . Orion AquaMate. UV-Vis and Vis Spectrophotometers . . Thermo Fisher Scientific provides this document to its customers with a product purchase to use in the product operation. The contents of this document are subject to change without notice. All technical information in this document is for reference purposes only.

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