NITON XL3t 700 Series Analyzer User’s Guide
NITON XL3t 700 Series AnalyzerUser’s GuideVersion 6.4
ContentsContentsAbout This User’s Guide .iUnpacking and Assembling Your NITON XRF Analyzer .iThe NITON XRF Analyzer Overview .iiThe Control Panel .iiInstrument Startup .viThe NAV Menu .viiiThe Battery Life Indicator .ixThe Menu Path .xChapter 1Thermo ScientificApplications . 1-1The NAV Menu . 1-1The Tools Menu . 1-2Print. 1-2Backlight. 1-2Avg Forward . 1-2Avg Back. 1-3Stop Avg Fwd/Back. 1-4Example Averaging. 1-5Live Spectrum Feed. 1-6Activating and Deactivating the Live Spectrum. 1-6RoHS Compliance . 1-7RoHS Operating Procedure . 1-7Interpreting the symbols on-screen. 1-7Plastics Analysis Mode . 1-9Thickness Correction . 1-10How to apply Thickness Correction. 1-10When to use Thickness Correction . 1-11Examples. 1-12Analyzing Bulk Samples . 1-15Testing Prepared Samples . 1-18The Data Entry Screen. 1-19Data Entry Screens for Plastics Mode. 1-19Navigating the Data Entry Screen . 1-21The Virtual Keyboard . 1-22All Alloys Analysis . 1-25Cu/Zn/Pb Analysis. 1-28Ta/Hf/Re Test Menu . 1-29Match Signature Analysis . 1-31The Store Signature Screen . 1-33SuperChem Analysis . 1-35The SuperChem Teach Menu. 1-38NITON Analyzer User’s Guide1-1
ContentsAnalysis and Sorting of Aluminum Alloys . 1-43Introduction. 1-43Performance. 1-43Sorting requirements. 1-43Specific needs. 1-44Disabling Aluminum Analysis . 1-45Analyzing Metal Alloy Samples . 1-47The Data Entry Screen. 1-50Selecting Data Entry from View Data Mode . 1-52Navigating the Data Entry Screen . 1-53The Virtual Keyboard . 1-54The Results Screen . 1-56Match Number . 1-57Camera and Small Spot Video . 1-59How to Use the Camera. 1-59How to Use the Small Spot Technology . 1-60Using the Small Spot. 1-62Mining. 1-62He Purged. 1-62Consumer Goods Analysis . 1-63TestAll Analysis. 1-64Metal . 1-66Painted Metal. 1-66Thin Metal. 1-66Plastic. 1-66PVC Plastic. 1-66Thin Plastic. 1-66Aluminum Alloys . 1-66Layered Materials . 1-66Non-Metals. 1-66Other . 1-66Metals & Minerals Analysis. 1-67Consumer Plastics Analysis . 1-68Painted Products Analysis . 1-69The View Data Screen . 1-71Scrolling Down Through the CompleteListing of Elements . 1-72Sorting Elements. 1-72Element Sorts. 1-73Composition Sorts . 1-73Error Sorts . 1-73Spectrum Graph. 1-73The Erase All Data Screen. 1-75The Erase Readings Screen. 1-76The Erase Signatures Screen. 1-77The Erase SuperChem Screen . 1-78Thermo ScientificNITON Analyzer User’s Guide1-2
ContentsThe Erase SuperPrec Screen . 1-79The View Libraries Menu . 1-80The View Signatures Menu. 1-81The View SuperChem Screen. 1-82The View SuperPrec Screen . 1-83The Calibrate Detector Screen . 1-85The Calibrate Touch Screen Screen . 1-87Calibrating the Touch Screen WithoutUsing the Touch Screen . 1-89The Specs Screen. 1-91The Date and Time Screen . 1-92The Rotate Screen 180 Toggle . 1-93The Adjust Backlight Screen . 1-94The Hardware Setup Screen. 1-95The Filter Config Screen . 1-100The Language Settings Screen . 1-106The Printer Setup Screen . 1-108Print LOD . 1-109Print Complete . 1-109Print Data Field . 1-109Print Date & Time . 1-109The Beep Setup Menu . 1-110Mode . 1-111First Beep. 1-111Second Beep. 1-111Third Beep. 1-111Beep on Grade Match . 1-111The Sort Element Display Menu. 1-112The Set Element Threshold Menu . 1-117The Adjust Alloy Thresholds Menu . 1-121The Set Display Units Menu. 1-123The Display Units Screen. 1-124Changing Sigma. 1-125Sigma . 1-125Confidence Intervals . 1-125Adjusting the Sigma Values. 1-126Toy Mode. 1-127Thermo ScientificNITON Analyzer User’s Guide1-3
ContentsThermo ScientificChapter 2Routine Maintenance Guidelines . 2-1Battery Pack and Battery Charger. 2-1Replacing The Battery Pack . 2-1Recharging The Battery Pack . 2-2Maintenance, Cleaning and Repairs . 2-6Replacing the Kapton Window . 2-7Storing and Transporting Your XL3 Analyzer . 2-9Networking and Connectivity. 2-11Setting up Wireless Networking. 2-11Available Devices Screen . 2-12Bluetooth Search Screen. 2-15The Connected Screen . 2-18Bluetooth Status Screen . 2-21Reset Bluetooth Device . 2-23GPS Data Tracking. 2-24Example of GPS Data . 2-24GPS Options. 2-26Tested Units include: . 2-26Entering Data with a Barcode reader. 2-27Supported Barcode Readers. 2-28Setting Up and Using the USB port. 2-29The Installation Wizard . 2-30Chapter 3Radiation and General Safety . 3-1Radiation and General Safety . 3-1Radiation Protection Basics. 3-1Time . 3-1Distance. 3-2Shielding. 3-2Exposure to Radiation. 3-2Monitoring your radiation exposure. 3-4Pregnancy and Radiation Exposure . 3-5How to Use the NITON XL3t Analyzer Safely. 3-6Know where the beam is . 3-6The Shutter-Open Indicator Lights. 3-7Handle and Use with Respect . 3-8Follow a Radiation Protection Program . 3-8Take Proper Care of your NITON XL3t Analyzer 3-8Avoid Over-Exposures. 3-8Safe Handling of Samples. 3-9Small Samples . 3-9Irregularly Shaped Samples . 3-9Low Density Materials (such as plastics). 3-9NITON Analyzer User’s Guide1-4
ContentsRadiation Profile . 3-10Primary Radiation. 3-13Secondary Radiation . 3-14Deep and Shallow Dose . 3-14Storage & Transportation . 3-15Storage . 3-15Transportation . 3-15EMERGENCY PROCEDURES . 3-16Lost or Stolen Instrument . 3-16Damaged Instrument . 3-16Minor Damage. 3-16Major damage . 3-17Emergency Response Information. 3-17Europe . 3-17Asia . 3-18Registration and Licensing . 3-19FAQ. 3-19Regarding Safety Devices for the OpenBeam Configuration:. 3-20Contact Information . 3-21Radiation Safety Group. 3-21Service Departments . 3-21United States Regulatory AuthorityContact Information . 3-21Appendices . A-1Appendix A: .A-1Appendix B: .A-4Appendix C:.A-7How to Use SpectraView .A-7Viewing the Information in SpectraView Mode .A-7Multiple Spectra.A-8SpectraView Navigation .A-8Appendix D: .A-10Appendix E: .A-12Appendix F: .A-14Limited Warranty Provision for Use withPurchase and License Agreement for ThermoScientific XRF Detection instruments: .A-14Specific warranties of some common accessories:.A-14Thermo ScientificNITON Analyzer User’s Guide1-5
Contents1-6NITON Analyzer User’s GuideThermo Scientific
About This User’s GuideWARNING! Do not attempt to use this analyzer without first reading andunderstanding the entire User’s Guide!CAUTION NITON Analyzers are not intrinsically safe analyzers in regard tosparking. All pertinent Hot Work procedures should be followed in areas ofconcern.Unpacking andAssembling YourNITON XRF AnalyzerThermo Scientific Inspect the shipping carton for signs of damage such as crushed or waterdamaged packaging. Immediately notify the shipping company andThermo Fisher Scientific, in the United States, toll free, at (800)875-1578, or outside the United States, at 1-978-670-7460, if there isany visible damage to the shipping container or any of its contents. Open the packing carton. If your analyzer is not packed in its carryingcase, please call Thermo Fisher Scientific immediately, in the UnitedStates, toll free, at (800) 875-1578, or outside the United States, at 1-978-670-7460. Verify the contents of the shipping container against the enclosedpacking list. If there are any discrepancies between the actual contents ofthe shipping container and the enclosed packing list, please notifyThermo Fisher Scientific immediately, in the United States, toll free, at(800) 875-1578, or outside the United States, at 1-978-670-7460. Open the carrying case and visually inspect the analyzer for damagebefore removing it from the case. Call the shipper and Thermo FisherScientific if you find any damage to the case or its contents. Save the shipping carton and all packing materials. Store them in a safe,dry area for reuse the next time that you ship the analyzer.NITON XL3 Analyzer User’s Guidei
The NITON XRFAnalyzer OverviewThe NITON XL3 Analyzer is a single unit, hand held, high performanceportable x-ray fluorescence (XRF) elemental analyzer.Control panelRearInterlockTop ViewKaptonMeasurementWindowLCD touch screenFront ViewRear ViewTriggerLED lightsBattery Pack/HandleProximity SensorSide ViewFigure 0-1. Analyzer OverviewThe Control PaneliiNITON XL3 Analyzer User’s GuideThe control panel is located on the analyzer’s top housing, directly below theLCD touch screen (see Figure 0-1). The control panel consists of a 4 waytouch pad, a center button, and two control buttons, one on each side.Using either the control panel or the touch screen you may navigate throughall of the analyzer’s screens and menus. You can control the movement of thescreen cursor by pressing the four way control pad in one of four directionsto highlight each of the menu options. The Select button in the center ofthe four way touch pad is used to select highlighted menu options. Theon/off/escape button both controls the power to the analyzer and serves asan "escape" button. When the on/off/escape button is pushed andimmediately released, it functions as an "escape", and brings you back to theMain Menu from the current screen in the menu system.Thermo Scientific
LCD touchscreenOn/off/escapebuttonLCD touchscreen catchClear/enterbuttonSelect buttonInterlock button4-way touch padFigure 0-2. The Control PanelPush and hold the on/off/escape button for at least 3 seconds to turn theanalyzer on.Push the on/off/escape button and hold it down for about 10seconds to shut off power to the analyzer from any screen in the menusystem.You also have the option of operating the analyzer, including navigating themenu system, by using the built in touch screen. To select a menu option,tap on the icon once. The touch screen icons have the same functionality asthe four way touch pad, the on/off/escape button, and the select or enterbutton. This User's Guide will refer to the process of choosing a course ofaction by selecting an icon from a menu, either using the touch screen orusing the control panel buttons, as “selecting.”Selecting the Return icon works everywhere throughout the User Interfaceto bring you back to the previous menu from the current menu in the menusystem. Use the on/off/escape button to return to the Main Menu.Thermo ScientificNITON XL3 Analyzer User’s Guideiii
The LCD Touch ScreenThe LCD TouchScreenThe LCD Touch Screen on your XL3 Analyzer is designed to swing up anddown to different angles for ease in viewing and interacting with youranalyzer. The LCD Touch Screen is connected to your analyzer along thebase of the screen, right above the Control panel. The screen is not designedto separate from the analyzer, but can be adjusted to any arbitrary anglebetween zero degrees - that is, flush with the analyzer - and 85 degrees,which is almost perpendicular. The LCD Touch Screen will stay at anygiven angle between these extremes until moved to a different angle. Whenin closed position, the screen is secured by a catch at the top center of thescreen housing.Figure 0-3. XL3 Analyzer Showing LCD Screen Tilted. To raise the LCD Touch Screen, disengage the catch at the top-center ofthe LCD Touch Screen housing and gently pull the screen towards youuntil it is at the best angle for your use. To close the LCD Touch Screen, gently push away from you along thetop edge of the screen housing. The screen will swing down until thecatch solidly engages with an audible click.Note The LCD Touch Screen cannot be removed from your XL3 analyzer.Removing or attempting to remove the LCD Touch Screen will damageyour analyzer and void your warranty.Note Always close your LCD Touch Screen before storing or transportingyour XL3 analyzer.ivNITON XL3 Analyzer User’s GuideThermo Scientific
The Data PortsThe Data PortsPower PortUSB PortRemote Trigger PortSerial PortFigure 0-4. Data Ports on the XL3Thermo ScientificUSB PortThe USB Port is a communications and control port, for uploading anddownloading data, configuration files, and software to the analyzer.Remote Trigger PortThe Remote Trigger Port controls the analyzer’s trigger function, for usewith the Extend-a-pole, In Situ Tripod, and test stands.Serial PortThe Serial Port is a communications and control port, for uploading anddownloading data, configuration files, and software to the analyzer.Power PortThe power port is used to run the XL3 under external power.NITON XL3 Analyzer User’s Guidev
The Data PortsInstrument StartupTo turn on the analyzer, depress the on/off/escape button on the controlpanel for approximately 10 seconds.Figure 0-5. System Start ScreenOn startup, the screen will be replaced by a Start Screen (see Figure 0-5)which will automatically count down from 9 to 0 in increments of onesecond.Figure 0-6. Logon ScreenWhen the Start is complete, the Start Screen will be replaced by the Logonscreen (see Figure 0-6.) Tap anywhere on this screen to continue.The Logon Screen will be replaced by a Warning Screen, see Figure 0-7,advising you that this analyzer produces radiation when the lights areflashing. You must acknowledge this warning by selecting the “Yes” buttonbefore logging on. Selecting the “No” button will return you to the LogonScreen.viNITON XL3 Analyzer User’s GuideThermo Scientific
The Data PortsFigure 0-7. Warning ScreenAfter selecting the “Yes” button, the Virtual Numeric Keypad becomesavailable for you to log onto the analyzer.Figure 0-8. Virtual Numeric Keypad for LogonThermo ScientificNITON XL3 Analyzer User’s Guidevii
The Data PortsSelect your 4 digit security code, followed by the enter (E) key. Thetemporary password assigned by default is 1-2-3-4, followed by the “E” key.If you enter an incorrect number, you can use the “ “ key to backspace overit, ot use the “C” key to clear everything. After you have completed the logon procedure, the word "USER" will appear on the bottom of the screen,then the Main Menu will appear. Note that security codes are editable.Please see the NDT manual for instructions on creating user-definablepasswords.Check the date/time. The time should be set correctly for accurate andverifiable record keeping (See Chapter 1 page 92).Your analyzer can be stored and operated safely in temperatures from -10º C(14º F) to 50º C (122º F). You will not be able to take a measurement if theanalyzer overheats. If it is hot to the touch, you should allow it to coolbefore testing.The NAV MenuFigure 0-9. The NAV MenuThe Navigation Menu, or NAV Menu, is available in all screens, thoughonly through the touch screen interface. Within a menu, the particularoptions available from the NAV Menu may change with the context. Forexample, within the View Menu, the NAV Menu changes optionsdepending on the mode you are currently using.viiiNITON XL3 Analyzer User’s GuideThermo Scientific
The Data PortsAccess the NAV Menu by selecting the word NAV in the screen. Adrop-down menu of choices will appear. Selecting an option from the NAVMenu will take you directly to a particular menu, no matter where you arein the menu hierarchy. Selecting the “View” option from the NAV Menu,for example, will bring you directly to the Data Menu.The NAV Menu cannot be selected through the Control Panel.The Battery Life IndicatorThe Battery Life Indicator is visible on all screens in the menu system. Theindicator is visible in the top right portion of the screen, and graphicallyshows you how much battery life is left, enabling you to change batteries asneeded to avoid unexpected shutdowns.Battery Life IndicatorBattery Life KeyExternal Power SourceFull Battery90% Battery Life75% Battery Life50% Battery Life25% Battery Life05% Battery LifeFigure 0-10. Battery Life IndicatorThe more green visible in the indicator, the higher the charge. The more redvisible in the indicator, the lower the charge. It’s best to charge one batterywhile using the other, to avoid work slowdowns or stoppages due to batterycharge conditions.WARNING! In the highly unlikely event that the x-ray tube remains onwhen the trigger is not depressed, disconnect the battery pack immediatelyto turn off the x-ray tube, and call Thermo Fisher Scientific’s ServiceDepartment in the United States, toll free, at (800) 875-1578, or outsidethe United States at 1-978-670-7460, or your local Authorized NITONAnalyzers Service Center.Thermo ScientificNITON XL3 Analyzer User’s Guideix
The Data PortsThe Menu PathThe Menu Path shows you graphically how to get to the function beingdescribed in several discrete steps from the universal start position, the MainMenu.Figure 0-11. Example Menu PathIn the Menu Path, the order is top to bottom, then if needed left to right,starting with the Main Menu and ending with the function wanted. Thearrows show the succession of menus, while the icon to be selected ishighlighted by a heavy rectangular border.This Menu path should be read as:To get to this screen, starting at the Main Menu, select the Mode icon,select the Alloy icon, select the Chemistry icon, then select the All Alloysicon.xNITON XL3 Analyzer User’s GuideThermo Scientific
ApplicationsThe NAV MenuChapter 1The NAV MenuApplicationsThe NAV Menu enables you to move between various menus and screensdirectly, without going through the intervening screens. Select a destinationfrom the drop down menu and you will be brought directly to that menu orscreen.Figure 1-1. The NAV MenuThermo ScientificNITON XL3 Analyzer User’s Guide1-1
ApplicationsThe Tools MenuThe Tools MenuThe Tools Menu enables you to perform common data-related tasks such asprinting and averaging. Select a task from the drop down menu to initiatethat task.Figure 1-2. The Tools MenuThe Tools Menu, like the NAV Menu, uses context sensitive menus. Thefollowing is the most common menu set.PrintBacklightAvg Forward1-2NITON XL3 Analyzer User’s GuideEnables you to print the sample analysis to the optional printer.Enables you to turn backlighting on and off.Enables you to average different readings together from this analysisforward. Select Avg Forward to initiate future sample averaging. AvgForward will set up an automatic personal averaging protocol to be followeduntil your analyzer is shut down, or this feature is disabled. To begin, selectthe number of readings you want to average from the virtual numerickeypad. Your analyzer will calculate an average reading after that number oftests, and continue this pattern until stopped. For example, if you select 3on the virtual keypad, the analyzer will automatically calculate, average, andstore a reading for every three tests you take, storing the individual readingsalong the way.Thermo Scientific
ApplicationsThe Tools MenuAvg BackEnables you to average different readings together from this analysisbackward. Select Avg Back to initiate backwards sample averaging. AvgBack will take a number of readings you select and average their analyticalresults. The range is counted from the last reading backward by the numberof readings selected. If your last reading was #15, selecting 3 would averagereadings #13, 14, and 15. The average is calculated, displayed, and storedinto memory as the next sequential reading number.The range number is selected using a virtual keypad on your analyzer similarto the keypad used for login. Select the digits in the range number from thekeypad, then select the “E” key to enter the number. “C” will clear all, and“ “ will clear the last digit entered. The average will automatically bedisplayed.Figure 1-3. The Virtual Numeric Keypad for AveragingNote You cannot average readings taken with different element lists - or withdifferent filter settings if the settings have different element lists - with eitherAvg Back or Avg Forward. Alloy and Mining modes each use the sameelement lists with the different filter settings, so averaging works whenswitching between filter settings when in either of these modes. Thin Filmand Bulk modes both use different element lists for different filter settings,and readings with different filter settings cannot be averaged when usingeither of these modes. You can never average readings taken in differentmodes.Thermo ScientificNITON XL3 Analyzer User’s Guide1-3
ApplicationsThe Tools MenuNote The Tools Menu is only available when viewing readings, and themenu is only accessible through the touch screen interface or NDTr.Stop Avg Fwd/BackAvg Back and Avg Forward are toggles. The option on the Tools Menuchanges to its opposite when selected. To stop averaging, select Stop AvgFwd or Stop Avg Back from the Tools Menu as appropriate.Figure 1-4. The Tools Menu - Averaging Toggles1-4NITON XL3 Analyzer User’s GuideThermo Scientific
ApplicationsExample AveragingExample AveragingFigure 1-5. Averaging example: 3 readingsThermo ScientificNITON XL3 Analyzer User’s Guide1-5
ApplicationsLive Spectrum FeedLive Spectrum FeedThe Tools Menu may contain a toggle option to display live spectra assample analysis occurs.Figure 1-6. The Tools Menu showing the Spectra On/Off ToggleActivating andDeactivating the LiveSpectrumFrom the Tools Menu, select Spectra : On to turn the Spectrun feed on.Once the spectrum is displayed, selecting Spectra : Off from the Tools Menuwill stop the live spectrum display.Figure 1-7. Test Screen Showing Live Spectrum1-6NITON XL3 Analyzer User’s GuideThermo Scientific
RoHS ComplianceRoHS ComplianceRoHS OperatingProcedurePlease review the Standard Operating Procedures (SOP) included with youranalyzer. The SOP includes the most current instructions for RoHS andWEEE analysis with your NITON analyzer.If you have had your analyzer for some time, the most recent RoHSStandard Operating Procedures for NITON analyers are available fromThermo Scientific upon request. For more information on this document,please contact Thermo Scientific’s Customer Service Department in theUnited States, Toll free, at (800) 875-1578, or outside the United States at 1-978-670-7460, or your authorized NITON Analyzer Service Center.#2#1#3Pass:Inconclusive:Fail:Compliant for all RoHSElements.The results for Br, Hg, andCr are not yet c
ii NITON XL3 Analyzer User’s Guide Thermo Scientific The NITON XRF Analyzer Overview The NITON XL3 Analyzer is a single unit, hand held, high performance portable x-ray fluorescence (XRF) elemental analyzer. Figure 0-1. Analyzer Overview The Control Panel The control panel is
ii NITON XL3 Analyzer User’s Guide Thermo Scientific The NITON XRF Analyzer Overview The NITON XL3 Analyzer is a single unit, hand held, high performance portable x-ray fluorescence (XRF) elemental analyzer. Figure 0-1. Analyzer Overview The Control Panel The control panel is
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