THE MOST ADVANCED SYSTEM FOR MEASUREMENT OF CATALYTIC . - Micromeritics

THE MOSTADVANCED SYSTEMFOR MEASUREMENT OFCATALYTICACTIVITYMicroactivityEffi

MICROACTIVITY EFFIThe Microactivity Effi is a compact and advancedmodular and completely automated laboratorysystem for measurement of catalytic activity andselectivity.It is a world Reference Reactor used by scientistsat Research Centers and Universities worldwide.

The standard unit can be adaptedfor different catalytic tests throughdifferent configurations and options.Real time results with very high levelof accuracy and reproducibility.Programming of series of experimentwith data acquisition and graphicscapabilities.Up to 1100 ºC, depending on thematerial of reactors.Up to 200 bar as optional.3STANDARD SPECIFICATIONS3 x high precision mass flow controllers with digital communications.Preinstallation of liquid feed line.1 SS316 tubular reactor, 9.1 mm ID with easy loading of up to 3.3 cc catalyst. Thermocoupleplaced directly in catalyst bed.Maximum working pressure up to 100 0.1 bar based on micrometric servo-controlled valvedesign. PED 2014/68/UE, high-pressure certification.Maximum working temperature up to 1100 1 ºC (depending on reactor material, SS316 asstandard. 9,1 mm ID x 300 mm length, 20 μm porous plate.All layout inside hot box made with hot air convector. Maximum temperature up to 200 1 ºC.Automatic six-port reactor bypass valve.High pressure Liquid/Gas separator (L1) with capacitive level sensor and very low dead volume(less than 1 cc), allowing real time results without accumulation. Level control valve (LCV) basedon micrometric servo-controlled valve.Independent safety levels separate from PC. User-defined functions for alarms.PC with user-friendly software with real time supervision and program recipes.Microactivity Effi

01 MICROACTIVITY EFFITOUCH SCREENAll parameters canbe easily changed andcontrolled by the PLCtouch screen.4PROCESS@ SOFTWARE AND EXPERIMENT VIEWERProcess@ is a user-friendlyreal-time SCADA softwarebased on LabVIEW and digitalcommunications.Session table for automaticdevices changes. Easyprogramming of conditional linesfor more efficient experiments.Monitoring and data acquisitionfor process and control values.Graphs capabilities.All parameters are saved ina log file for later graphicalrepresentation and datatreatment. Easy export tospreadsheets.Microactivity Effi

REACTOR MATERIAL AND SIZESInside x Outside diameter: 9.1x14.3 mm (Std), 13.1x19.1 mm*, 17.5x25.4 mm*Max. temperature(ºC)Max. pressure(BAR)Max. P (BAR) @500 ºCMax. P (BAR) @650 ºCSS316 (Std)800690214104Hastelloy X*1200617525308Hastelloy C276*1093418364155Inconel 600*121235624336Inconel 625*980827728414SS310*1100441262241Max. P (BAR) @790 ºC10023.8 mm ID reactor available* OptionalStd: standard5Microactivity Effi

01 MICROACTIVITY EFFIOPTIONAL CONFIGURATIONGTL configurationHigh pressure L/L/G separator with very low dead volume (lessthan 1 cc each phase) for separation and collection of 2 nonmiscible liquid products.2 reactors1 Duo configuration2 fixed bed reactors.Possibility to switch betweenreactor 1 or reactor 2 and serialconnection.Optionally a 2nd PCV can make thereactor 1 work at higher pressurethan reactor 2.6Optionally an additional MFC fed toreactor 2 to modify the compositioncoming from reactor 1.2 Twin configuration2 fixed bed reactors, one for reaction for pressures up 100 bar, one for regeneration at atmospheric pressure.1 x MFC for regeneration.Possibility of serial connection.Optionally a 2nd PCV can make both reactors work at the same pressure, avoiding re-pressurization when switchingreactors.Microactivity Effi

3 Parallel configuration (includes serial mode)Complete parallel reactor system.2 MFC per reactor.Independent feed each reactor.Independent working conditions, high pressure, high temperature applications.1 x HP L/G separator (L1) each reactor (total 2).Possibility of serial connection.Automatic bypass valve for L/G separator bypassing, sending all products from reactor 1 to to reactor 2.Optionally an automatic switching valve in the gas outlets for GC/vent selection.7Microactivity Effi

01 MICROACTIVITY EFFIOPTIONAL EQUIPMENTMass flow meter in the gas outletfor mass balance calculations.Automatic six port valvesfor different purposesL/G separator bypassUp/down flow selection.8Fixed bedMinimumfluidizationFluidization PneumatictransportFluidized bed reactorwith differential pressuremeasurement.Wax trap temperature controlledfor heavy hydrocarbons collectionjust at reactor outlet (F-T).Microactivity EffiHigh pressure200 bar operationas an option.

Liquid feedUp to 2 HPLC pumps 0.02 – 5 ml/min. Heatedoption up to 90 ºC for heavy liquids.Also Syringe pump for very low and accurateflow (from 0,01 μL/min).Up to 2 Extra liquid evaporatorstemperature controlled (50 to 450 ºC)for heavier products or higher flow rates.Automatic programmableliquid multisampler withcooling system.Digital scale in theliquid outlet forliquid quantification.Optionally in liquidfeed vessel.Gas feedUp to 6 MFCs, 3 as standard.Easy calibration for other gases.9OPC server option, monitorand data processing intocompany network.Microactivity Effi

MICROACTIVITY EFFI SOLOThe new Microactivity Effi Solo reactor isan introductory catalyst testing equipmentusing the same technology developed forthe Microactivity Effi.

COMPARATIVE TABLEMA EFFI SOLOMA EFFIStandardOptionalStandardOptionalNumber of reactors1-12HP L/G separator (L1)-OptionalIncluded2HP L/L/G separator (L2, i.e. FT)---1Max. 800 ºC withSS316 reactorMax. 1100 ºC withspecial alloysMax. 800 ºC withSS316 reactorMax. 1100 ºC withspecial alloysPressureAtmospheric100 bar100 bar200 barGas feed2 MFCUp to 4 MFC3 MFCUp to 6 MFCLiquid feed-1 HPLC pump-Up to 2 HPLCpump (or syringe)Heated liquid feed and head pump-1-2Scale-1-2Mass flow Meter in the gas outlet-1-2ManualAutomaticAutomaticN/AL/G separator bypass valve---OptionalUp/Down flow selection valve---Optional9.1mm IDSmaller (7.9mmand 5.1mm ID)9.1mm IDSmaller and bigger(5.1, 7.9, 13.1, 17.5and 23.8mm ID)Quartz reactor-Optional-OptionalSpecial alloys-Optional-OptionalWax trap---2Fluidized bed reactor---OptionalLiquid Multisampler---2TemperatureReactor bypass valveReactor size (metallic)11Microactivity Effi

THE MOSTADVANCED SYSTEMFOR MEASUREMENT OFCATALYTICACTIVITYCONTACTProcess Integral Development S. L.C/ Francisco Gervás 11Pol. Ind. Alcobendas28108 Alcobendas (Madrid) - SPAINTel. : 34 914 840 183 - Fax : 34 916 620 141pid@micromeritics.comwww.pidengtech.com

COMPARATIVE TABLE. www.pidengtech.com CONTACT Process Integral Development S. L. C/ Francisco Gervás 11 Pol. Ind. Alcobendas 28108 Alcobendas (Madrid) - SPAIN Tel. : 34 914 840 183 - Fax : 34 916 620 141 pid@micromeritics.com ADVANCED SYSTEM CATALYTIC ACTIVITY FOR MEASUREMENT OF THE MOST.